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At least 649 records · Page 36

Effect of Hf Additions to Pt Aluminide Bond Coats on EB-PVD TBC Life

Small Hf additions were incorporated into a Pt aluminide coating during chemical vapor deposition (CVD) on single crystal RENE N5 substrates. Standard yttria-stabilized zirconia top coats were subsequently deposited onto the coated substrates by electron beam-physical vapor deposition (EB-PVD). The coated substrates underwent accelerated thermal cycle testing in a furnace at a temperature in excess of 1121 C (2050 F) (45 minute hot exposure, 15 minute cool to approximately 121 C (250 F)) until the thermal barrier coating (TBC) failed by spallation. Incorporating Hf in the bond coat increased the TBC life by slightly more than three times that of a baseline coating without added Hf. Scanning electron microscopy of the spalled surfaces indicated that the presence of the Hf increased the adherence of the thermally grown alumina to the Pt aluminide bond coat. The presence of oxide pegs growing into the coating from the thermally grown alumina may also partially account for the improved TBC life by creating a near-surface layer with a graded coefficient of thermal expansion.

Nesbitt, James↗

Metallographic cooling rates of L-group ordinary chondrites

Shock metamorphism appears to be a ubiquitous feature in L-group ordinary chondrites. Brecciation and heterogeneous melting obscure much of the early history of this meteorite group and have caused confusion as to whether L chondrites have undergone thermal metamorphism within onion-shell or rubble-pile parent bodies. Employing the most recent shock criteria, we have examined 55 Antarctic and 24 non-Antarctic L chondrites in order to identify those which have been least affected by post-accretional shock. Six low-shock samples (those with shock grade less than S4) of petrographic types L3-L5 were selected from both populations and metallographic cooling rates were obtained following the technique of Willis and Goldstein. All non-Antarctic L6 chondrites inspected were too heavily shocked to be included in this group. However, 4 shocked L6 chondrites were analyzed in order to determine what effects shock may impose on metallographic cooling rates. Metallographic cooling rates were derived by analyzing the cores of taenite grains and then measuring the distance to the nearest grain edge. Taenites were identified using backscatter imaging on a Cameca SX-50 electron microprobe. Using backscatter we were able to locate homogeneous, rust-free, nearly spherical grains. M-shaped profiles taken from grain traverses were also used to help locate the central portions of selected grains. All points which contained phosphorus above detection limits were discarded. Plots of cooling-rate data are summarized and data from the high-shock samples are presented. The lack of coherency of cooling rates for individual samples is indicative of heterogeneous cooling following shock. The data confirms the statement expressed by numerous workers that extreme care must be taken when selecting samples of L chondrites for cooling-rate studies. Data for the 6 non-Antarctic low-shock samples are also presented. The samples display a general trend in cooling rates. The lowest metamorphic grade yielded the slowest cooling rates and an increase in grade follows an increase in cooling rate. This is the opposite relationship to that predicted by the onion-shell model.

Bennett, Marvin E.↗

Characterizing Cometary Electrons with Kappa Distributions

The Rosetta spacecraft has escorted comet 67P/Churyumov-Gerasimenko since 6 August 2014 and has offered an unprecedented opportunity to study plasma physics in the coma. We have used this opportunity to make the first characterization of cometary electrons with kappa distributions. Two three-dimensional kappa functions were fit to the observations, which we interpret as two populations of dense and warm (density 10 cubic centimeters, temperature 2 times 10 (sup 5) degrees Kelvin, invariant kappa index 10 to 1000), and rarefied and hot (density equals 0.005 cubic centimeters, temperature 5 times 10 (sup 5) degrees Kelvin, invariant kappa index equals 1 to 10) electrons. We fit the observations on 30 October 2014 when Rosetta was 20 kilometers from 67P, and 3 Astronomical Units from the Sun. We repeated the analysis on 15 August 2015 when Rosetta was 300 kilometers from the comet and 1.3 Astronomical Units from the Sun. Comparing the measurements on both days gives the first comparison of the cometary electron environment between a nearly inactive comet far from the Sun and an active comet near perihelion. We find that the warm population density increased by a factor of 3, while the temperature cooled by a factor of 2, and the invariant kappa index was unaffected. We find that the hot population density increased by a factor of 10, while the temperature and invariant kappa index were unchanged. We conclude that the hot population is likely the solar wind halo electrons in the coma. The warm population is likely of cometary origin, but its mechanism for production is not known.

Broiles, T. W.↗

Overview on Current Activities of Conduction-Cooled SRF Accelerators and their Applications

When Nb3Sn was reintroduced to the SRF community as an alternative to pure niobium, one key motivation has been to reduce the cryogenic requirements of new and existing accelerators by shifting from 2 K to 4 K operation. Meanwhile, a variety of implementations beyond research machines are being explored. The combination of Nb3Sn with conventional cryocoolers, enabling cryogen-free operation, has paved the way for the development of compact, standalone systems suitable for applications far beyond research, such as enhancing the durability of synthetics via crosslinking or sterilizing food and medical equipment, as well as environmental cleanup when it comes to decontaminating liquid and solid waste material. So, while fundamental R&D continues to refine Nb3Sn resonators, exploring improvements such as replacing the niobium substrate with copper, parallel research efforts are investigating how the increased beam power provided by SRF could expand the commercial use of electron beams. This presentation aims to deliver a comprehensive overview of ongoing research efforts to harness the benefits of SRF through Nb3Sn and conduction cooling.

Vennekate, John [Thomas Jefferson National Acceler↗

Photocurrent Nanoscopy of Quantum Hall Bulk

Understanding nanoscale electronic and thermal transport of two-dimensional (2D) electron systems in the quantum Hall regime, particularly in the bulk insulating state, poses considerable challenges. One of the primary difficulties arises from the presence of chiral edge channels, whose transport behavior obscures the investigation of the insulating bulk. Using near-field optical and photocurrent nanoscopy, we probe real-space variations of the optical and thermal dynamics of graphene in the quantum Hall regime without relying on complex sample or electrode geometries. Near the charge-neutrality point, we detect strong optical and photothermal signals from resonant inter-Landau-level (LL) magnetoexciton excitations between the zeroth and ± 1 st LLs, which gradually weaken with increasing doping due to Pauli blocking. Interestingly, at higher doping levels and full-integer LL fillings, photothermal signals reappear across the entire sample over an approximately 10 − μ m scale, indicating unexpectedly long cooling lengths and nonlocal photothermal heating through the insulating bulk. This observation suggests that thermal conductivity persists for the localized states even as electronic transport is suppressed—a clear violation of the Wiedemann-Franz law. Our experiments provide novel insights into nanoscale thermal and electronic transport in incompressible 2D gases, highlighting the roles of magnetoexcitons and chiral edge states in the thermo-optoelectric dynamics of the Dirac quantum Hall state. Published by the American Physical Society 2025

36 MATERIALS SCIENCE↗

In Situ 4D‐STEM Imaging of the Orientation of Lamellar Clusters in Polymer Crystallization

In semi‐crystalline polymeric materials, the initial stages of nucleation and the growth path of crystalline domains can determine the final performance. Here, in this work, we used four‐dimensional scanning transmission electron microscopy (4D‐STEM) imaging to analyze the changes in lamellar orientation in high‐density polyethylene (HDPE) during heating and cooling. This method allowed us to quantitatively detect the formation of lamellae clusters with different in‐plane orientations, which are not visible with traditional methods. Our analysis provided detailed insights into the orientation and size changes of crystalline domains. Additionally, this technique enabled direct observation of lattice structures in hierarchical lamellae and the growth of crystals, confirming the local variability in lamellar orientation. This innovative approach significantly improves our understanding of polymer crystallization, linking changes in morphology and lattice structures at different length scales.

4D-STEM↗

The thermosphere of Titan

The vertical structure of Titan's thermosphere is calculated down to the mesopause as a function of local time based on Voyager 1 occultation data. The thermal time scales that characterize the diurnal behavior of the thermosphere are discussed, the input model atmosphere used to calculate the temperature profile is presented, and the dominant heating and cooling mechanisms in the thermosphere are examined. The temperature profiles obtained by integrating the heat transfer equation with and without electron heating are presented and discussed. The implications that derived exospheric temperatures have for the neutral hydrogen torus are investigated. The diurnal exospheric temperature is unlikely to exceed 225 K, averages between 187 and 197 K, and has a variational amplitude of 28 K or less. The vertical extent of the hydrogen cloud is too large to be explained in terms of simple thermal escape of hydrogen from the exosphere.

Friedson, A. J.↗

Thermal and dynamical effects of pair production on two-temperature accretion flows

The two-temperature criterion for quasi-spherical (ion-pressure supported) accretion onto a black hole, including the effects of electron-positron pair production is studied. For an interesting range of accretion rates, Coulomb interactions between protons and pairs can cool the innermost regions of the accretion flow. The cooled plasma, assumed to possess some angular momentum, will collapse onto the equatorial plane, forming an optically thick annulus. Hysteresis effects involved in the cooling criterion are expected to lead to bistability or time dependence, which may be associated with variability in certain classes of active galactic nuclei (AGNs). Radiation from the annulus may be responsible for the EUV/soft X-ray excess observed in some AGNs.

Begelman, Mitchell C.↗

A Long Look at MCG-5-23-16 with NuSTAR. I. Relativistic Reflection and Coronal Properties

MCG-5-23-16 was targeted in early 2015 with a half mega-second observing campaign using NuSTAR. Here we present the spectral analysis of these data sets along with an earlier observation and study the relativistic reflection and the primary coronal source. The data show strong reflection features in the form of both narrow and broad iron lines plus a Compton reflection hump. A cutoff energy is significantly detected in all exposures. The shape of the reflection spectrum does not change in the two years spanned by the observations, suggesting a stable geometry. A strong positive correlation is found between the cutoff energy and both the hard X-ray flux and spectral index. The measurements imply that the coronal plasma is not at the runaway electron-positron pair limit, and instead contains mostly electrons. The observed variability in the coronal properties is driven by a variable optical depth. A constant heating-to-cooling ratio is measured, implying that there is a feedback mechanism in which a significant fraction of the photons cooling the corona are due to reprocessed hard X-rays.

black hole physics – galaxies: active – galaxi↗

Temperature Mapping Above and Below Air Film-Cooled Thermal Barrier Coatings Using Phosphor Thermometry

Thermal barrier coatings (TBCs) are typically used in conjunction with air film cooling to maximize overall cooling effectiveness and reliability while minimizing sacrifices in engine performance. The effects of thermal barrier coating (TBC) thermal protection and air film cooling effectiveness have usually been studied separately; however, their contributions to combined cooling effectiveness are interdependent and are not simply additive. The combined cooling effectiveness is always less than the sum of the cooling effectiveness of stand-alone TBC protection and stand-alone air film cooling. These diminishing returns arise because adding the thermally insulating TBC between the cooling air and the surface to be cooled reduces the air film cooling effectiveness and because the air film cooling reduces the heat flux through the TBC and therefore reduces the temperature difference sustained across the TBC thickness. Due to these considerations, combined cooling effectiveness must be measured to achieve an optimum balance between TBC thermal protection and air film cooling. In this investigation, temperature mapping above and below air film-cooled TBCs was performed using luminescence lifetime imaging-based phosphor thermometry. Measurements were performed in the NASA GRC Mach 0.3 burner rig on a TBC-coated plate using a scaled-up cooling hole geometry where both the hot mainstream gas temperature and the blowing ratio were varied. Surface temperature maps were obtained from a Cr-doped GdAlO3 thermographic phosphor deposited on the surface of the electron-beam vapor-deposited yttria-stabilized zirconia (YSZ) TBC. From separate plates, temperature maps from the bottom of the TBC were obtained from a thin Er-doped YSZ layer integrated into the TBC below the overlying undoped YSZ. Procedures for temperature and cooling effectiveness mapping above and below the air film-cooled TBC surface are described. Most importantly, these measurements enable mapping the combined cooling effectiveness below the TBC, which is more important than surface cooling effectiveness when there is a barrier coating between the hot mainstream gas and the surface that needs thermal protection. Advantages of the luminescence lifetime imaging method over infrared thermography, as well as its limitations to steady-state conditions are discussed.

cooling effectiveness.↗

MODIS TEB Calibration Algorithm Improvements for Future L1B Collection

Terra and Aqua MODIS have provided continuous global observations for scientific applications for more than 20 and 18 years, respectively. The radiometric calibration of the MODIS thermal emissive bands (TEB) is based on a quadratic approximation of the instrument response. The calibration coefficients look-up tables (LUTs) are updated using the response of the MODIS on-board blackbody (BB)with the response background subtracted by space view. The quarterly on-board BB warm-up and cool-down activity temperature ranges from 270 K to 315 K, and the derived offset has a relatively large uncertainty. Electronic cross-talk, an artifact that affects both instrument calibration and Earth view (EV) radiance retrievals, is corrected based on lunar observations. Calibration assessments using EV observations (e.g. ocean, desert, Antarctic Dome Concordia, and deep convective clouds) provide useful information to evaluate the impact of the Terra safe mode (February 2016) and Aqua MODIS formatter reset (January 2018) events on both MODIS instruments. This study focuses on the TEB radiometric calibration algorithm improvements for future collections based on calibration assessments using EV measurements and analytical modeling. Measurement stability and consistency over specific Earth scenes with a wide temperature range, as well as their brightness temperature (BT) dependency, are used for bias estimations in the calibration coefficients. Calibration coefficients are derived and updated after adjusting the current fitting algorithm. Thereafter, using the test LUTs, their impact on the Level 1B (L1B) data for different EV scenes is analyzed.

MODIS↗

Searching for cluster magnetic fields in the cooling flows of 0745-191, A2029, and A4059

We have performed sensitive polarimetric radio observations with the Very Large Array (VLA) of three galaxies: PKS 0745-191, PKS 1508+059, and PKS 2354-350, embedded in x-ray cooling flow clusters. High sensitivity, multifrequency maps of all three, along with spectral index and Faraday rotation measure (RM) maps of PKS 1508+059 and PKS 2354-350 are presented. For PKS 1508+059 and PKS 2354-350 models of the electron density of the intracluster medium (ICM) have been used to set lower limits of 0.1 and 2.7 microG, respectively, on the magnetic field in the ICM based on the observed RMs. In an x-ray selected sample of cooling flow clusters with an associated radio source, 57% (8/14) are found to have absolute RMs in excess of 800 radians/sq m. This sample includes the three sources of this study and all the other high RM sources found to date at zeta less than 0.4. These facts are consistent with the high RM phenomenon being produced by magnetic fields associated with the relatively dense, hot x-ray gas in cooling flow clusters.

Taylor, Gregory B.↗

Density sensitive C II lines in cool stars of low gravity

It is shown that the relative intensities of emission lines within the multiplet UV 0.01 of C II, around 2325 A, are sensitive to electron density in the range 10 to the 9th to 10 to the 7th per cu cm. The lines therefore offer a valuable method for measuring electron densities in the chromospheres of late-type giants and supergiants. Calculated line ratios are compared with those observed in a range of objects.

Stencel, R. E.↗

Applications of heat pipes to cool PWBS and hybrid microcircuits

Some of the advanced thermal management techniques used to reduce operating junction temperature under extreme environmental temperature conditions are discussed. Heat pipes in actual electronic packaging applications, and those under development, are discussed. Performance characteristics of heat pipes are given, and examples are described of how thermal problems in electronic packaging are solved through the use of heat pipes.

Sekhon, K. S.↗

Difficult Measurements of Materials Systems at Cryogenic Temperatures: Cryo-EELS and Cryo-4D-STEM

Scanning/transmission electron microscopy (S/TEM) in materials science has traditionally been accomplished at room temperature due to their solid state in this temperature range and relative insensitivity to radiolysis damage. Cooling to cryogenic temperatures tended to introduce instabilities such as vibration and drift and can lead to the buildup of carbon contamination or ice reducing contrast. The need to expand TEM experimental techniques into new fields such as quantum and battery materials led to new efforts to reduce these instabilities while achieving temperatures at or well below liquid nitrogen (77 K). Further, developments in detector and spectrometer technology brought new capabilities for high resolution electron energy loss spectroscopy (EELS) and scanning nanodiffraction (4D-STEM). These experimental modalities can require even tighter controls of drift, vibration, and exposure time. Here this presentation will discuss accomplishing difficult experiments at cryogenic temperatures in honor of the late Dr. Lena Kourkoutis who inspired and led many such experiments.

36 MATERIALS SCIENCE↗

Microelectromechanical System (MEMS) Device Being Developed for Active Cooling and Temperature Control

High-capacity cooling options remain limited for many small-scale applications such as microelectronic components, miniature sensors, and microsystems. A microelectromechanical system (MEMS) using a Stirling thermodynamic cycle to provide cooling or heating directly to a thermally loaded surface is being developed at the NASA Glenn Research Center to meet this need. The device can be used strictly in the cooling mode or can be switched between cooling and heating modes in milliseconds for precise temperature control. Fabrication and assembly employ techniques routinely used in the semiconductor processing industry. Benefits of the MEMS cooler include scalability to fractions of a millimeter, modularity for increased capacity and staging to low temperatures, simple interfaces, limited failure modes, and minimal induced vibration. The MEMS cooler has potential applications across a broad range of industries such as the biomedical, computer, automotive, and aerospace industries. The basic capabilities it provides can be categorized into four key areas: 1) Extended environmental temperature range in harsh environments; 2) Lower operating temperatures for electronics and other components; 3) Precision spatial and temporal thermal control for temperature-sensitive devices; and 4) The enabling of microsystem devices that require active cooling and/or temperature control. The rapidly expanding capabilities of semiconductor processing in general, and microsystems packaging in particular, present a new opportunity to extend Stirling-cycle cooling to the MEMS domain. The comparatively high capacity and efficiency possible with a MEMS Stirling cooler provides a level of active cooling that is impossible at the microscale with current state-of-the-art techniques. The MEMS cooler technology builds on decades of research at Glenn on Stirling-cycle machines, and capitalizes on Glenn s emerging microsystems capabilities.

Beach, Duane E.↗

Operational Testing of 4H-SiC JFET ICs for 60 Days Directly Exposed to Venus Surface Atmospheric Conditions

Prolonged Venus surface missions (lasting months instead of hours) have proven infeasible to date in the absence of a complete suite of electronics able to function for such durations without protection from the planet’s extreme conditions of ~460 °C, ~9.3 MPa (~ 92 Earth atmospheres) chemically reactive environment. Here we report testing data from a successful two-month (60-day) operational demonstration of two 175-transistor 4H-SiC junction field effect transistor (JFET) semiconductor integrated circuits (ICs) directly exposed (no cooling and no protective chip packaging) to a high-fidelity physical and chemical reproduction of Venus surface atmospheric conditions in a test chamber. These results extend the longest reported duration of electronics operation in Venus surface atmospheric conditions almost 3-fold and were accomplished using prototype SiC JFET chips of more than 7-fold increased complexity. The demonstrated advancement marks a significant step towards realization of electronics with sufficient complexity and durability for implementing robotic landers capable of returning months of scientific data from the surface of Venus.

Integrated Circuit↗

Comparison of electron and electronic temperatures in recombining nozzle flow of ionized nitrogen-hydrogen mixture. I, II.

Relaxation of the population distribution of electronic states is studied theoretically for a highly ionized nitrogen-hydrogen mixture expanding through a nozzle wherein the hydrogen content is less than 0.1%. The analysis incorporates quantum-mechanical rate coefficients, and considers the effects of wall cooling and absorption of radiation. Calculations are carried out for a condition produced experimentally. Visible and infrared line radiations from nitrogen and hydrogen were measured with a spectrograph. The geometry and stagnation conditions were those calculated theoretically. The experiment confirms quantitatively the predictions that the electronic excitation temperatures of hydrogen and (3P) core states of nitrogen are higher than the electron temperature, and that (3P) excitation temperatures exhibit maxima within the nozzle.

Park, C.↗