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At least 703 records · Page 39

Additive manufacturing of AISI M2 tool steel by binder jetting (BJ): Investigation of microstructural and mechanical properties

The presented research demonstrates for the first time the successful processing of AISI M2 tool steel by binder jetting, a promising additive manufacturing technique capable of producing complex shapes with minimal residual stresses and isotropic properties. The optimal printing parameters were explored by varying processing parameters such as the binder saturation (45 %–105 %), binder set time (0 to 10 s), targeted bed temperature (50–60 °C), oscillator (2600–2750 rpm), recoater (20–28 mm/s), and roller speeds (200–300 rpm). Microstructural characterization and evaluation of mechanical properties of binder jetted parts were performed using x-ray diffraction (XRD), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) to study their chemical composition, powder morphology, microstructure, carbide morphologies, relative density, hardness, compressive strength, and ductility. Two powder sizes (5 and 10 μm) were used, and sintering was performed at varying temperatures (1270, 1280, and 1300 °C) and durations (60 and 120 min), followed by a furnace, air, and water cooling. An optimum hardness of ~970 HV was obtained when parts were sintered at 1270 °C for 60 min, followed by water quenching. Impressive compressive strength of ~ 3580 MPa was observed in the sample sintered at 1280 °C for 60 min duration, followed by air cooling. Furnace-cooled parts showed the highest density of ~95 %, whereas the relative density of air- and water-cooled parts varied between ~91 to 93.50 %, respectively. The microstructure of sintered samples revealed the formation of M 6 C stable carbide, M 2 C metastable carbide, MC as a secondary carbide, and a-Fe matrix, which contributed to the observed increase in mechanical properties.

36 MATERIALS SCIENCE↗

Microstructure and Mechanical Property Improvement in Laser-Welded TC4 Titanium Alloy and 301L Stainless Steel Joints Without Filler Metal

Pulsed laser welding of Ti alloy to stainless steel (SS) has been applied without filler metal. When the laser beam was focused on the Ti alloy–SS interface, large volumes of Ti-Fe intermetallics were formed in the joint. These Ti-Fe intermetallics were highly brittle, causing the joint to crack spontaneously after welding. The brittle coarse Ti-Fe intermetallics seriously deteriorates the joint strength of Ti alloy and SS; therefore, it is necessary to control the quantities and distributions of brittle Ti-Fe intermetallics in the joint. The amount of melted base materials was controlled by changing laser offset to control the melted proportion and thus control the quantity and distribution of brittle Ti-Fe intermetallics in weld. When laser beam was on the SS side, melting amount of Ti alloy in weld was decreased. When laser beam was on the Ti alloy side, melting amount of SS in weld was decreased. When the laser offset was 0.35 mm away from SS side, the sample realizes the effective connection between Ti alloy and SS. A compound layer was formed at the SS side with the main microstructure of β-Ti and TiFe{sub 2}. The joint fractured at the compound layer with the maximum tensile strength of 182 MPa. Microstructures and mechanical properties of joints were improved by changing laser offset.

36 MATERIALS SCIENCE↗

Microstructural Evolution and Properties of 24CrNiMoY Alloy Steel Fabricated by Selective Laser Melting

24CrNiMoY alloy steel samples were fabricated by selective laser melting (SLM), and a phase transformation model was established to study the alloy steel microstructural evolution. Meanwhile, microhardness and tensile properties of 24CrNiMoY alloy steel prepared by different laser energy densities (E{sub v}) were investigated. Results indicate that the microstructural evolution of 24CrNiMoY alloy steel is consistent with the phase transformation model. The main microstructure changed from martensite to bainite with the increase in thermal cycle numbers. In addition, a suitable E{sub v} plays an important role in refining the bainite structure and improving the alloy steel properties. When the E{sub v} decreases from 210 to 140 J/mm{sup 3}, the bainite lath width reduces from 1.7 to 0.6 μm. Simultaneously, the relative density, tensile strength and microhardness of the fabricated samples increase first and decrease later. 24CrNiMoY alloy steel sample prepared by 160 J/mm{sup 3} has fine mechanical properties: The tensile strength is 850 MPa and microhardness is 360 HV{sub 0.2}.

36 MATERIALS SCIENCE↗

Evolution of microstructures and mechanical properties during solution treatment of a Ti–V–Mo-containing high‑manganese cryogenic steel

Highlights: • High-Mn cryogenic steels are getting the spotlight in the cryogenic market. • The grain size grew slowly and the yield strength remained almost stabilized with an increase of solutionizing temperature. • The Hall–Petch strengthening coefficient for yield strength was small, estimated to be 153 MPa μm{sup 0.5}. • The weakening effect of solutionizing temperature on grain size was attributed to the nano-sized (Ti, V, Mo)C precipitate. - Abstract: The effect of solution treatment on the microstructure and mechanical properties of a high‑manganese (Mn) twin-induced plastic (TWIP) cryogenic steel that was alloyed from elemental titanium (Ti), vanadium (V) and molybdenum (Mo) was investigated by a variety of techniques such as microstructural characterization, room tensile testing and − 196 °C impact testing. The austenite grain size grew slowly with an increase of the solutionizing temperature (ST). The relatively weak effect of the ST on the austenite grain size is attributed to the superior thermal stability and coarsening resistance of the (Ti, V, Mo)C precipitate, which hindered austenite grain growth. An increase in ST improved the low-temperature toughness (LTT) significantly and decreased the strain hardening rate (SHR), but had no significant effect on the yield strength. The Hall–Petch strengthening coefficient for yield strength was small, and was estimated to be 153 MPa μm{sup 0.5}. Undissolved large-sized chromium (Cr) carbide can deteriorate the LTT significantly. Because of its excellent mechanical properties, high-Mn steel that was alloyed by elemental Ti, V and Mo can be used to manufacture storage tanks for liquefied natural gas.

36 MATERIALS SCIENCE↗

A process optimization framework for laser direct energy deposition: Densification, microstructure, and mechanical properties of an Fe-Cr alloy

Laser Direct Energy Deposition (DED) is a metal additive manufacturing technique with the ability to fabricate large and complex parts through deposition of metal powders. However, achieving high-density parts and targeted build heights using DED can be challenging due to the large number of highly sensitive process variables. This work proposes a robust fabrication parameter optimization framework to generate process maps for primary parameters in DED, including laser power, scan speed, mass flow rate, hatch spacing, and layer height. Simple single-track experiments were utilized to map out the parameter space, and a combination of geometric criteria for hatch spacing and layer height were proposed to determine parameter sets that achieve both targeted build heights and mitigate porosity formation. Using this framework, specimens with >99 % density and consistent mechanical properties were successfully fabricated over a wide range of process parameters for an Fe-9wt.%Cr (Fe9Cr) alloy, a surrogate for radiation damage-resistant reduced activation ferritic/martensitic (RAFM) steels. Processing these materials using DED is of particular interest in the development of plasma facing components for nuclear fusion applications. The microstructure and mechanical properties of as-printed Fe9Cr were characterized using optical and electron microscopy, X-ray diffraction, and uniaxial tensile tests. As-printed Fe9Cr displayed ~25 % elongation and ultimate tensile strengths of up to 475 MPa which is comparable to similar wrought alloys. Finally, the proposed framework will allow for accelerated DED parameter optimization for novel alloy systems, as well as open the possibility for local microstructure control while simultaneously mitigating defect formation.

42 ENGINEERING↗

Microstructure and Mechanical Properties of Laves Phase-strengthened Fe-Cr-Zr Alloys

Laves phase-reinforced alloys have shown some preliminary promising performance at room temperatures. This paper aims at evaluating mechanical properties of Laves phase-strengthened alloys at elevated temperatures. Three Fe-Cr-Zr alloys were designed to favor the formation of eutectic microstructures containing Laves and body-centered cubic phases with the aid of thermodynamic calculations. Microstructural characterization was carried out on the alloys in as-processed and aged states using optical microscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction. The effect of thermal aging and alloy composition on microstructure has been discussed based on microstructural characterization results. Mechanical properties have been evaluated by means of Vickers microhardness measurements, tensile testing at temperatures up to 973.15 K (700.15 °C), and creep testing at 873.15 K (600.15 °C) and 260 MPa. Alloys close to the eutectic composition show significantly superior strength and creep resistance compared to P92. Finally, however, their low tensile ductility may limit their applications at relatively low temperatures.

36 MATERIALS SCIENCE↗

Effect of Zr on microstructures and mechanical properties of an Al-Mg-Si-Cu-Cr alloy prepared by low frequency electromagnetic casting

The Al-1.6Mg-1.2Si-1.1Cu-0.15Cr (all in wt. %) alloys with and without Zr addition prepared by low frequency electromagnetic casting process were investigated by using the optical microscope, scanning electron microscope and transmission electron microscope equipped with energy dispersive analytical X-ray. The effects of Al{sub 3}Zr phases on the microstructures and mechanical properties during solidification, homogenization, hot extrusion and solid solution were studied. The results show that Al{sub 3}Zr phases reduce the grain size by ∼ 29% and promote the formation of an equiaxed grain structure during solidification. Numerous spherical Al{sub 3}Zr dispersoids with 35–60 nm in diameters precipitate during homogenization, and these fine dispersoids change little during subsequent hot extrusion and solid solution. Adding 0.15 wt. % Zr results in no recrystallization after hot extrusion and partial recrystallization after solid solution, while the recrystallized grain size is 400–550 μm in extrusion direction in the Zr-free alloy. In addition, adding 0.15 wt. % Zr can obviously promote Q′ phase precipitation, while the β″ phases are predominant in the alloy without Zr. Adding 0.15 wt. % Zr, the ultimate tensile strength of the T6 treated alloy increases by 45 MPa, while the elongation remains about 16.7%. - Highlights: • Minor Zr can refine as-cast grains of the LFEC Al-Mg-Si-Cu-Cr alloy. • L1{sub 2} Al{sub 3}Zr phases with 35–60 nm in diameter precipitate during homogenization. • L1{sub 2} and DO{sub 22} Al{sub 3}Zr phases result in partial recrystallization after solid solution. • Minor Zr can promote the precipitation of Q′ phases. • Mechanical properties of Al-Mg-Si-Cu-Cr-Zr alloy are higher than those of AA7005.

36 MATERIALS SCIENCE↗

Influence of Mn addition on the microstructure and mechanical properties of a directionally solidified γ-TiAl alloy

Highlights: • Mn addition can significantly improve the yield strength of TiAl alloy. • Introduction of Mn facilitates the operation of twinning-controlled deformation. • Twin-dislocation interactions cause a continuous increase in work hardening rate. - Abstract: TiAl alloys with nominal compositions of Ti-47Al-2Nb-2Cr-(0, 1, 3, 5)Mn were prepared via electromagnetic cold crucible directional solidification (ECCDS), and the influence of Mn addition on the microstructure and mechanical properties of the alloys was investigated. The experimental results showed that the Mn atoms were dissolved within the TiAl alloy, and no Mn compounds were formed. Based on the X-ray diffraction (XRD) analysis results, the peak angle of the Mn-containing sample shifted to a higher value, indicating lattice shrinkage. The Mn addition also increased the volume fraction of the B2 phase. The yield strength of the TiAl alloy monotonically increased as the content of the substitutional-solute Mn atoms increased. The ultimate strengths of the TiAl alloys containing 1 at.%, 3 at.%, and 5 at.% Mn consequently decreased because micro-cracks were preferentially formed in the B2 phase during room-temperature deformation. The introduction of substitutional-solute Mn atoms could result in a reduction of the stacking-fault energy of the γ phase, and facilitate the operation of twinning-controlled plastic-deformation during the intermediate stage of the plastic deformation process. The interaction between the deformation twins and movable dislocations led to a continuous increase in the work-hardening rate.

36 MATERIALS SCIENCE↗

Microstructures and mechanical properties of compositionally complex Co-free FeNiMnCr 18 FCC solid solution alloy

Recently, a structurally-simple but compositionally-complex FeNiCoMnCr high entropy alloy was found to have excellent mechanical properties (e.g., high strength and ductility). To understand the potential of using high entropy alloys as structural materials for advanced nuclear reactor and power plants, it is necessary to have a thorough understanding of their structural stability and mechanical properties degradation under neutron irradiation. Furthermore, this requires us to develop a similar model alloy without Co because material with Co will make post-neutron-irradiation testing difficult due to the production of the 60 Co radioisotope. In order to achieve this goal, a FCC-structured single-phase alloy with a composition of FeNiMnCr 18 was successfully developed. This near-equiatomic FeNiMnCr 18 alloy has good malleability and its microstructure can be controlled by thermomechanical processing. By rolling and annealing, the as-cast elongated-grained-microstructure is replaced by homogeneous equiaxed grains. The mechanical properties (e.g., strength and ductility) of the FeNiMnCr 18 alloy are comparable to those of the equiatomic FeNiCoMnCr high entropy alloy. Both strength and ductility increase with decreasing deformation temperature, with the largest difference occurring between 293 and 77 K. Extensive twin-bands which are bundles of numerous individual twins are observed when it is tensile-fractured at 77 K. No twin bands are detected by EBSD for materials deformed at 293 K and higher. Ultimately the unusual temperature-dependencies of UTS and uniform elongation could be caused by the development of the dense twin substructure, twin-dislocation interactions and the interactions between primary and secondary twinning systems which result in a microstructure refinement and hence cause enhanced strain hardening and postponed necking.

36 MATERIALS SCIENCE↗

Microstructure and magnetic properties of MFe{sub 2}O{sub 4} (M = Co, Ni, and Mn) ferrite nanocrystals prepared using colloid mill and hydrothermal method

Three kinds of spinel ferrite nanocrystals, MFe{sub 2}O{sub 4} (M = Co, Ni, and Mn), are synthesized using colloid mill and hydrothermal method. During the synthesis process, a rapid mixing and reduction of cations with sodium borohydride (NaBH{sub 4}) take place in a colloid mill then through a hydrothermal reaction, a slow oxidation and structural transformation of the spinel ferrite nanocrystals occur. The phase purity and crystal lattice parameters are estimated by X-ray diffraction studies. Scanning electron microscopy and transmission electron microscopy images show the morphology and particle size of the as-synthesized ferrite nanocrystals. Raman spectrum reveals active phonon modes at room temperature, and a shifting of the modes implies cation redistribution in the tetrahedral and octahedral sites. Magnetic measurements show that all the obtained samples exhibit higher saturation magnetization (M{sub s}). Meanwhile, experiments demonstrate that the hydrothermal reaction time has significant effects on microstructure, morphologies, and magnetic properties of the as-synthesized ferrite nanocrystals.

36 MATERIALS SCIENCE↗

Effect of non-axisymmetric arc on microstructure, texture and properties of variable polarity plasma arc welded 5A06 Al alloy

Highlights: • Variable polarity plasma arc welding of 5A06 Al alloy was carried out under the condition of non-axisymmetric arc. • Deformation bands formed in the weld joint were due to microstructural inhomogeneities. • Tensile fracture occurred along the deformation bands in the TZ/HAZ fusion boundary on the side of “lower arc”. • The weld zones are harder than the BM due to dislocation sub-structure, deformation bands and ultrafine subgrain. - Abstract: Microstructure, texture and mechanical properties in the weld joint of variable polarity plasma arc welding of 5A06 Al alloy under the condition of non-axisymmetric arc have been investigated. The weld joint are characterized by elongated structure in the base material (BM), the heat affected zone (HAZ) and the transition zone (TZ) and equiaxed structure in the fusion zone (FZ). Microstructure of the weld joint is asymmetrical and inhomogeneous leading to deformation bands. Deformation texture and recrystallization texture were developed in the weld zones. The FZ center was dynamic recrystallized due to severe deformation. Materials in the TZ have undergone dynamic recovery. The weld zones are harder than the BM due to dislocation sub-structure, deformation bands and ultrafine subgrains. Microhardness distribution was homogeneous in the regions without deformation bands. Tensile fracture occurred along the deformation bands on the side of “lower arc” exhibiting ductile fracture, while the BM is less ductile.

36 MATERIALS SCIENCE↗

Effect of temperature on microstructure and mechanical properties of ECAPed (TiB + La2O3)/Ti-6Al-4V composites

Highlights: • Dynamic recrystallization resulted in ultrafine grains near TiB interface region. • Tensile strength of ECAPed composites increased by up to 18%. • The average aspect ratio of TiB reduced with increasing ECAP temperature. • Interface debonding of TiB led to crack propagation and low ductility. TiB short fibers and La{sub 2}O{sub 3} particles reinforced titanium matrix composites (TMCs) were successfully equal-channel angular pressed (ECAPed) at 600 °C–900 °C. The effect of ECAP temperature on the microstructure and mechanical properties of the TMCs was investigated. The results indicated that dislocation tangling formed cell structures in matrix at lower ECAP temperature. In contrast, continuous dynamic recrystallization occurred at higher ECAP temperature, and promoted the formation of numerous new ultrafine grains. The average aspect ratio of TiB short fibers decreased with increasing ECAP temperature, which induced interfacial debonding. The tensile strength of TMCs ECAPed at 800 °C was up to 1128 MPa, which was 18% higher than the as-received composites. Interfacial debonding led TiB short fibers in low aspect ratios disabled to bear load, while the formation of ultrafine grains increased the strength of TMCs. The coupling of these two factors resulted in little effect of ECAP temperature on the tensile strength. However, the elongation of ECAPed TMCs generally decreased due to the loss of strain hardening capacity. Stress concentration tended to occur around the tips of TiB short fibers due to the interfacial debonding and cause crack propagation. It led to the premature fracture and low ductility.

36 MATERIALS SCIENCE↗

Uranium-Titanium Alloys: The Effect of Ti Content on Phase Transformations, Microstructures, and Mechanical Properties

This report documents the findings of collaborative research done at Sandia National Laboratory and the Y-12 Development Division during the 1980s. Ongoing progress reports were presented at various U. S. Department of Energy (DOE) meetings throughout the 1980s, but the findings were never integrated into an inclusive final report. This report provides a summary of the key findings and implications of this research. This work was supported by the DOE National Nuclear Security Administration. The effect of titanium content on phase transformations, microstructures, and mechanical properties of uranium-titanium alloys has been investigated in alloys containing 0.3 wt.% to 2.0 wt.% Ti.

36 MATERIALS SCIENCE↗

Influence of Sc content on the microstructure and mechanical properties of cast Al-2Li-2Cu-0.5Mg-0.2Zr alloy

Highlights: • The grain size was continuously reduced with the increasing Sc content. • No evidence for the formation of the Cu-rich and Sc-containing W phase was observed. • Sc addition could promote the precipitation of S′ in the absence of pre-age stretch. • Sc addition would reduce the growth rate of δ′ and δ′-PFZs. • The highest combinations of strength and ductility were obtained in cast Al-Li alloys. - Abstract: In this work, the influence of Sc content on the microstructure and mechanical properties of cast Al-2Li-2Cu-0.5Mg-0.2Zr alloy was investigated. It was found that the grain size of As-cast alloy was significantly reduced in steps with the increase of Sc addition, accompanied by the arising and increasing of cubic primary Al{sub 3}(Sc, Zr) phases. No evidence for the presence of the ternary W (Al{sub 8−x}Cu{sub 4+x}Sc) phase was obtained. The volume fraction of nanoscale Al{sub 3}(Sc, Zr) dispersoids was improved with the increase of Sc content, and the presence of Sc was observed to refine the S′ (Al{sub 2}CuMg) morphology during ageing. The addition of Sc lowered the growth rates of δ′ (Al{sub 3}Li) particles and δ′-Precipitate-free zones (δ′-PFZs) of the base alloy. The tensile property results showed that, with the increasing Sc content and ageing times, the yield strength (YS) and ultimate tensile strength (UTS) were continuously increased, and the highest elongation of 6.0% was obtained in the 0.2Sc-containing alloy aged for 32 h at 175 °C. The results indicated that the optimal Sc addition in cast Al-2Li-2Cu-0.5Mg-0.2Zr alloy was 0.2 wt%.

36 MATERIALS SCIENCE↗

Effect of Hot Isostatic Pressing on the Microstructure and Mechanical Properties of Additively Manufactured Ti Alloys

A previous SAND report, SAND2020-11353 described the basic metallurgical and surface roughness properties of additively manufactured Ti-64 material made using a powder bed fusion process. As part of that work, material was post-processed using a hot isostatic press (HIP) to densify and heat treat the material. This report is meant as an addendum to the original report and to provide specific data on material processed with HIP. The main focus of this report is to show the effects of HIP on the microstructure and mechanical properties of AM Ti-64 and Ti-5553.

36 MATERIALS SCIENCE↗

Effect of Yb Substitution on Microstructure and Superconducting Properties of Y{sub 1−x}Yb{sub x}Ba{sub 2}Cu{sub 3}O{sub 7−δ} Films

The purpose of this study was to improve the critical current density (J{sub c}) of YBa{sub 2}Cu{sub 3}O{sub 7−δ} (YBCO) superconducting films at high magnetic fields. Thin Y{sub 1−x}Yb{sub x}Ba{sub 2}Cu{sub 3}O{sub 7−δ} (Y{sub 1−x}Yb{sub x}BCO) superconducting films on LaAlO{sub 3} substrates were prepared by modified low-fluorine metal organic deposition method (LF-MOD) in order to investigate the effect of Yb substitution on the microstructure and superconducting properties of a YBCO-coated conductor. In this study, single-phased, c-axial-aligned Y{sub 1−x}Yb{sub x}BCO films were obtained. Yb doping had a little effect on the critical temperature (T{sub c}) and transition width (ΔT) values of Y{sub 1−x}Yb{sub x}BCO films. An abnormal phenomenon was observed that the J{sub c} of Y{sub 1−x}Yb{sub x}BCO films at low field was smaller than that of the pure YBCO film, but the J{sub c} of Y{sub 1−x}Yb{sub x}BCO films at high field was much greater than that of the undoped YBCO film. Compared to pure YBCO film, the J{sub c} values of Y{sub 0.75}Yb{sub 0.25}BCO and Y{sub 0.25}Yb{sub 0.75}BCO films were enhanced by a factor of 8 at 8 T, 65 K, which meant that chemical substitution of Yb into the Y site could improve flux pinning significantly under the high magnetic field in Y{sub 1−x}Yb{sub x}BCO coated conductors.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

An integrated study of thermal treatment effects on the microstructure and magnetic properties of Zn-ferrite nanoparticles

The evolution of the magnetic state, crystal structure and microstructure parameters of nanocrystalline zinc–ferrite, tuned by thermal annealing of ~4 nm nanoparticles, was systematically studied by complementary characterization methods. Structural analysis of neutron and synchrotron x-ray radiation data revealed a mixed cation distribution in the nanoparticle samples, with the degree of inversion systematically decreasing from 0.25 in an as-prepared nanocrystalline sample to a non-inverted spinel structure with a normal cation distribution in the bulk counterpart. The results of DC magnetization and Mossbauer spectroscopy experiments indicated a superparamagnetic relaxation in ~4 nm nanoparticles, albeit with different freezing temperatures T f of 27.5 K and 46 K, respectively. The quadrupole splitting parameter decreases with the annealing temperature due to cation redistribution between the tetrahedral and octahedral sites of the spinel structure and the associated defects. DC magnetization measurements indicated the existence of significant interparticle interactions among nanoparticles (‘superspins’). Additional confirmation for the presence of interparticle interactions was found from the fit of the T f (H) dependence to the AT line, from which a value of the anisotropy constant of K eff = 5.6 × 10 5 erg cm -3 was deduced. Further evidence for strong interparticle interactions was found from AC susceptibility measurements, where the frequency dependence of the freezing temperature T f (ƒ) was satisfactory described by both Vogel–Fulcher and dynamic scaling theory, both applicable for interacting systems. The parameters obtained from these fits suggest collective freezing of magnetic moments at T f .

Antic, Bratislav↗

Impact of initial temper of base metal on microstructure and mechanical properties of friction stir welded AA 7055 alloy

Highlights: • Friction stir welded 7055-T4 alloy exhibits higher tensile properties than T6 alloy. • Friction stir welded 7055-T4 alloy exhibits more uniform hardness distribution. • Some regions in heat affected zone have higher hardness than base metal in T4-joint. • Effect of initial temper on precipitate evolution in different zones is discussed. AA 7055-T6 and AA 7055-T4 aluminium alloy sheets were friction stir welded to investigate the impact of initial base metal temper on microstructure, hardness and tensile properties of the joints. In the joint of alloy in T6 temper (T6-joint), the hardness of the weld zone is lower than that of base metal; in the joint of alloy in T4 temper (T4-joint), however, some regions in the heat affected zone exhibit higher hardness than base metal. The weld nugget zone in T6-joint exhibits slightly lower hardness compared with that in T4-joint. The hardness minima is slightly higher in T4-joint than in T6-joint. T4-joint exhibits higher yield strength, ultimate tensile strength and elongation compared with T6-joint. Based on microstructure examination by transmission electron microscopy, the impact of initial precipitate state on precipitation behavior in the weld nugget zone, thermo-mechanically affected zone and heat affected zone during friction stir welding and mechanical properties of the joints is discussed.

36 MATERIALS SCIENCE↗