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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 703 records · Page 39
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Effects of Sodium and Magnesium Ions on the Photochemically Induced Heterogeneous Formation of Manganese Oxides and Their Structural Evolution

Manganese (Mn) oxides are abundant in aquatic and terrestrial environments, where they play significant roles in redox cycling and biological metabolisms. We recently observed that Mn oxides were homogeneously formed during the abiotic oxidation of Mn 2+ (aq) to Mn(IV) by O 2 •– via nitrate photolysis, at a rate comparable to that of biotic Mn oxide formation. On the other hand, for the heterogeneous formation of Mn oxides, the presence of a substrate can alter the required thermodynamic driving force, which may affect their crystalline phases and further influence the oxidative capability of redox cycling in environmental systems. However, little is known about the photochemically induced heterogeneous formation of Mn oxides on substrates. In this study, we investigated the heterogeneous formation of Mn oxides on a quartz substrate in the presence of two environmentally abundant cations, Na + and Mg 2+ . In contrast to homogeneously generated Mn oxides, the heterogeneously formed Mn oxides displayed faster crystalline phase evolutions and morphological changes over time. Additionally, the coexistence of Na + and Mg 2+ ions greatly affected the initial crystalline phases and the phase evolution, as well as the surface morphologies of the Mn oxides. Finally, these discoveries contribute to our understanding of how various Mn oxides form in nature and provide insights into the processes involved in manufacturing specific Mn oxide crystalline structures for engineering applications.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1992

Users manual for program NYQUIST: Liquid rocket nyquist plots developed for use on a PC computer

The piping in a liquid rocket can assume complex configurations due to multiple tanks, multiple engines, and structures that must be piped around. The capability to handle some of these complex configurations have been incorporated into the NYQUIST code. The capability to modify the input on line has been implemented. The configurations allowed include multiple tanks, multiple engines, and the splitting of a pipe into unequal segments going to different (or the same) engines. This program will handle the following type elements: straight pipes, bends, inline accumulators, tuned stub accumulators, Helmholtz resonators, parallel resonators, pumps, split pipes, multiple tanks, and multiple engines. The code is too large to compile as one program using Microsoft FORTRAN 5; therefore, the code was broken into two segments: NYQUIST1.FOR and NYQUIST2.FOR. These are compiled separately and then linked together. The final run code is not too large (approximately equals 344,000 bytes).

Armstrong, Wilbur C.↗
NASA NTRS1992

Users manual for program SSFREQ intermediate mode stability curves: Developed for use on a PC computer

The piping in a liquid rocket can assume complex configurations due to multiple tanks, multiple engines, and structures that must be piped around. The capability to handle some of these complex configurations have been incorporated into the SSFREQ code. The capability to modify the input on line has been implemented. The configurations allowed include multiple tanks, multiple engines, the splitting of a pipe into equal segments going to different (or the same) engines. This program will handle the following type elements: straight pipes, bends, inline accumulators, tuned stub accumulators, Helmholtz resonators, parallel resonators, pumps, split pipes, multiple tanks, and multiple engines.

Armstrong, Wilbur C.↗
NASA NTRS1992

Users manual for program ADMIT: Admittance and pressure transfer function developed for use on a PC computer

The piping in a liquid rocket can assume complex configurations due to multiple tanks, multiple engines, and structures that must be piped around. The capability to handle some of these complex configurations have been incorporated into the ADMIT code. The capability to modify the input on line has been implemented. The configurations allowed include multiple tanks, multiple engines, the splitting of a pipe into unequal segments going to different (or the same) engines. This program will handle the following type elements: straight pipes, bends, inline accumulators, tuned stub accumulators, Helmholtz resonators, parallel resonators, pumps, split pipes, multiple tanks, and multiple engines.

Armstrong, Wilbur C.↗
DOE OSTI2024

Engineering Terpene Production Pathways in Methylobacterium extorquens AM1

Terpenes are diverse specialized metabolites naturally found within plants and have important roles in inter-species communication, adaptation and interaction with the environment. Their industrial applications span a broad range, including fragrances, flavors, cosmetics, natural colorants to agrochemicals and therapeutics, yet formal chemical synthesis is economically challenging due to structural complexities. Engineering terpene biosynthesis could represent an alternative in microbial biotechnological workhorses, such as Saccharomyces cerevisiae or Escherichi coli, utilizing sugars or complex media as feedstocks. Host species that metabolize renewable and affordable carbon sources may offer unique sustainable biotechnological alternatives. Methylotrophs are bacteria with the capacity to utilize one-carbon feedstocks, such as methanol or formate. They colonize the phyllosphere (above-ground area) of plants, and many accumulate abundant carotenoid pigments. Methylotrophs have the capacity to take up and use a subset of the rare earth elements known as lanthanides. These metals can enhance one-carbon (methylotrophic) metabolism. Here, we investigated whether manipulating the metabolism enables and enhances terpene production. A carotenoid-deficient mutant potentially liberates carbon, which may contribute to bioproduct accumulation. To test this hypothesis, terpene-producing bacterial strains regulated by two distinct promoters were generated. Wildtype Methylobacterium extorquens, ∆Meta1_3665, a methylotrophic mutant lacking the carotenoid pathway, and an E. coli strain were transformed with an exogenous terpene pathway and grown both in the presence and absence of lanthanides. The extraction, and the comparison of analytical profiles, provided evidence that engineered cultured M. extorquens under control of a native, inducible methylotrophic promoter can yield the sesquiterpene patchoulol when supplemented with lanthanide. In contrast, using a moderate-strength constitutive promoter failed to give production. We demonstrated colonization of the phyllosphere with the engineered strains, supporting the future engineering of selected species of the plant microbiome and with promising implications for the synthetic biology of small molecules.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2020

Mixing and detonation structure in a rotating detonation engine with an axial air inlet

High-fidelity simulations of an experimental rotating detonation engine with an axial air inlet were conducted. The system operated with hydrogen as fuel at globally stoichiometric conditions. Instantaneous data showed that the detonation front is highly corrugated, and is considerably weaker than an ideal Chapman–Jouguet wave. Regions of deflagration are present ahead of the wave, caused by mixing with product gases from the previous cycle, as well as the injector recovery process. It is found that as the post-detonation high pressure flow expands, the injectors recover unsteadily, leading to a transient mixing process ahead of the next cycle. The resulting flow structure not only promotes mixing between product and reactant gases, but also increases likelihood of autoignition. These results show that the detonation process is very sensitive to injector design and the transient behavior during the detonation cycle. Phase-averaged statistics and conditionally averaged data are used to understand the overall reaction structure. As a result, comparisons with available experimental data on this configuration show remarkable good agreement of the predicted reacting flow structure.

42 ENGINEERING↗
DOE OSTI2019

Laser ablation of polymers: a review

Laser ablation (LA), which employs a pulsed laser to remove materials from a substrate for generating micro-/nanostructures, has tremendous applications in the fabrication of metals, ceramics, glasses and polymers. It has become a noteworthy approach for achieving various functional structures in engineering, chemistry, biology, medicine and other fields. Polymers are one such class of materials; they can be melted and vaporized at high temperature during the ablation process. A number of polymers have been researched as candidate substrates in LA, and many different structures and patterns have been realized by this method. The current states of research and progress are reviewed from basic concepts to optimal parameters, polymer types and applications. Additionally, the significance of this paper is to provide a basis for follow-up research that leads to the development of superior materials and high-quality production through LA. In this review, we first introduce the basic concept of LA, including mechanism, laser types (millisecond, microsecond, nanosecond, picosecond and femtosecond) and influential parameters (wavelength, repetition rate, fluence and pulse duration). Then, we focus on several commonly used polymer materials and compare them in detail, including the effects of polymer properties, laser parameters and feature designs. Finally, we summarize the applications of various structures fabricated by LA in a variety of areas along with a perspective of the challenges in this research area. Overall, a thorough review of LA of several polymers is presented, which could pave the way for characterization of future novel materials.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Improved genome editing by an engineered CRISPR-Cas12a

CRISPR-Cas12a is an RNA-guided, programmable genome editing enzyme found within bacterial adaptive immune pathways. Unlike CRISPR-Cas9, Cas12a uses only a single catalytic site to both cleave target double-stranded DNA (dsDNA) (cis-activity) and indiscriminately degrade single-stranded DNA (ssDNA) (trans-activity). To investigate how the relative potency of cis- versus trans-DNase activity affects Cas12a-mediated genome editing, we first used structure-guided engineering to generate variants of Lachnospiraceae bacterium Cas12a that selectively disrupt trans-activity. The resulting engineered mutant with the biggest differential between cis - and trans -DNase activity in vitro showed minimal genome editing activity in human cells, motivating a second set of experiments using directed evolution to generate additional mutants with robust genome editing activity. Notably, these engineered and evolved mutants had enhanced ability to induce homology-directed repair (HDR) editing by 2–18-fold compared to wild-type Cas12a when using HDR donors containing mismatches with crRNA at the PAM-distal region. Finally, a site-specific reversion mutation produced improved Cas12a (iCas12a) variants with superior genome editing efficiency at genomic sites that are difficult to edit using wild-type Cas12a. This strategy establishes a pipeline for creating improved genome editing tools by combining structural insights with randomization and selection. The available structures of other CRISPR-Cas enzymes will enable this strategy to be applied to improve the efficacy of other genome-editing proteins.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2021

Computational design of microarchitected porous electrodes for redox flow batteries

Porous electrodes are used as the core reactive component across electrochemical technologies. In flowing systems, controlling the fluid distribution, species transport, and reactive environment is critical to attaining high performance. However, conventional electrode materials like felts and papers provide few opportunities for precise engineering of the electrode and its microstructure. To address these limitations, architected electrodes composed of unit cells with spatially varying geometry determined via computational optimization are proposed. Resolved simulation is employed to develop a homogenized description of the constituent unit cells. These effective properties serve as inputs to a continuum model for the electrode when used in the negative half-cell of a vanadium redox flow battery. Porosity distributions minimizing power loss are then determined via computational design optimization to generate architected porosity electrodes. The architected electrodes are compared to bulk, uniform porosity electrodes and found to lead to increased power efficiency across operating flow rates and currents. The design methodology is further used to generate a scaled-up electrode with comparable power efficiency to the bench-scale systems. Finally, the variable porosity architecture and computational design methodology presented here thus offers a novel pathway for automatically generating spatially engineered electrode structures with improved power performance.

25 ENERGY STORAGE↗
NASA NTRS1988

Flow-induced vibrations of the SSME LOX inlet tee vanes

This paper describes the results of a program initiated to identify the cause and the mechanism of 4-kHz vibrations of the Space Shuttle main engine's (SSME's) LOX inlet tee, which were revealed in 17 percent of the SSMEs during ground tests. The results of the engines' inspection, structural analyses, computational fluid dynamics studies, literature reviews, expert consultations, and laboratory testings identified the probable cause of the 4-kHz vibrations being related to the fact that the walls of some tees were thinner than in the mojority of tees, resulting in less stiff structures. The mechanism of the vibrations was identified as vortex shedding in combination with a structural coupling with the thrust cone, which increased the vane mobility, which, in turn, aggravated the fluid coupling with the thrust cone. As a result, the vane mobility was increased, aggravating the fluid coupling with the vanes. An internal modification was developed and was successfully demonstrated on an engine that had previously exhibited a 4-kHz problem.

O'Connor, G. M.↗
NASA NTRS2009

Structural Dynamic Behavior of Wind Turbines

The structural dynamicist s areas of responsibility require interaction with most other members of the wind turbine project team. These responsibilities are to predict structural loads and deflections that will occur over the lifetime of the machine, ensure favorable dynamic responses through appropriate design and operational procedures, evaluate potential design improvements for their impact on dynamic loads and stability, and correlate load and control test data with design predictions. Load prediction has been a major concern in wind turbine designs to date, and it is perhaps the single most important task faced by the structural dynamics engineer. However, even if we were able to predict all loads perfectly, this in itself would not lead to an economic system. Reduction of dynamic loads, not merely a "design to loads" policy, is required to achieve a cost-effective design. The two processes of load prediction and structural design are highly interactive: loads and deflections must be known before designers and stress analysts can perform structural sizing, which in turn influences the loads through changes in stiffness and mass. Structural design identifies "hot spots" (local areas of high stress) that would benefit most from dynamic load alleviation. Convergence of this cycle leads to a turbine structure that is neither under-designed (which may result in structural failure), nor over-designed (which will lead to excessive weight and cost).

Thresher, Robert W.↗
NASA NTRS1993

Structural design and analysis of a Mach zero to five turbo-ramjet system

The paper discusses the structural design and analysis of a Mach zero to five turbo-ramjet propulsion system for a Mach five waverider-derived cruise vehicle. The level of analysis detail necessary for a credible conceptual design is shown. The results of a finite-element failure mode sizing analysis for the engine primary structure is presented. The importance of engine/airframe integration is also discussed.

Spoth, Kevin A.↗
DOE OSTI2023

Structural analysis of wild-type and Val120Thr mutant Candida boidinii formate dehydrogenase by X-ray crystallography

Candida boidinii NAD + -dependent formate dehydrogenase (CbFDH) has gained significant attention for its potential application in the production of biofuels and various industrial chemicals from inorganic carbon dioxide. The present study reports the atomic X-ray crystal structures of wild-type CbFDH at cryogenic and ambient temperatures, as well as that of the Val120Thr mutant at cryogenic temperature, determined at the Turkish Light Source ‘Turkish DeLight’. The structures reveal new hydrogen bonds between Thr120 and water molecules in the active site of the mutant CbFDH, suggesting increased stability of the active site and more efficient electron transfer during the reaction. Further experimental data is needed to test these hypotheses. Collectively, these findings provide invaluable insights into future protein-engineering efforts that could potentially enhance the efficiency and effectiveness of CbFDH.

59 BASIC BIOLOGICAL SCIENCES↗
NASA NTRS1992

Briefing notes on propulsion stability codes ADMIT, NYQUIST, and SSFREQ

The piping in a liquid rocket can assume complex configurations due to multiple tanks, multiple engines, and structures that piping must go around. The capability to handle some of these complex configurations have been incorporated into the Low Frequency Code (ADMIT), the Nyquist Code (NYQUIST), and the Intermediate Frequency code (SSFREQ). The capability to modify the input on line has been implemented. The configurations allowed include multiple tanks, multiple engines, and the splitting of a pipe into unequal segments going to different (or the same) engines. Straight pipes, bends, inline accumulators, tuned stubs, Helmholtz resonators, parallel resonators, and pumps are the types of piping that may be used. The three codes require the computation of admittance looking toward the tank. Therefore, they all have a number of similar routines for reading in the tank, piping, and engine descriptions. They also have similar routines for computing the admittance looking toward the tank. ADMIT uses only one type of feedline, either a LOX or FUEL line. NYQUIST can use no feedlines, one feedline (either LOX or FUEL), or two feedlines (both LOX and FUEL). SSFREQ requires both feedlines to be present (LOX and FUEL). The common features of the three codes are discussed first, with two sample runs described. Then each of the three codes are discussed along with the sample runs. Several on-line variations are suggested for the second sample run. Input descriptions and the input for the sample runs are given in the appendices.

Armstrong, W. C.↗
NASA NTRS2017

NASA's Space Launch System Gains Momentum Toward Integration and Testing

NASA's Space Launch System (SLS) entered a new phase in 2017, completing major structural manufacturing on the core stage and delivering the first flight hardware to NASA's Kennedy Space Center (KSC). The program is now transitioning to integration, assembly and testing in preparation for launch readiness in late 2019. Core stage prime contractor Boeing concluded welding of the major core stage components for Exploration Mission 1 (EM-1) with the liquid hydrogen flight tank, following completion of the engine section, liquid oxygen tank, and forward skirt. Technicians also completed assembly of the bolted intertank, and all sections are currently in hardware integration. The engine section structural test article was shipped to NASA's Marshall Space Flight Center (MSFC) and began testing in 2017. The core stage pathfinder shipped to NASA's Michoud Assembly Facility (MAF). Booster prime contractor Orbital ATK made significant progress casting motor segments for SLS, with several segments finishing processing and in storage. Forward and aft sections of the boosters are being refurbished at KSC. RS-25 prime contractor Aerojet Rocketdyne completed SLS adaptation testing and qualification of four new EM-1 controllers. The four EM-1 engines are ready and waiting for shipment from NASA's Stennis Space Center (SSC) to Michoud Assembly Facility (MAF) for core stage integration in preparation for green run testing at SSC. The EM-1 Interim Cryogenic Propulsion System (ICPS) became the first major piece of SLS to arrive at KSC. Welding is complete on the EM-1 Launch Vehicle Stage Adapter (LVSA) and the flight Orion Stage Adapter (OSA). SLS is critical to U.S. leadership in future human and robotic space exploration, including a presence on the moon in preparation for missions deeper into space. This paper will elaborate on 2017 SLS progress and progress envisioned for 2018.

Askins, Bruce R.↗
NASA NTRS2006

Cryogenic Fracture Toughness Evaluation of an Investment Cast Al-Be Alloy for Structural Applications

Aluminum-Beryllium metal matrix composite materials are useful due to their desirable performance characteristics for aerospace applications. Desirable characteristics of this material includes light-weight, dimensional stability, stiffness, good vibration damping characteristics, low coefficient of thermal expansion, and workability, This material is 3.5 times stiffer and 22% lighter than conventional aluminum alloys. electro-optical systems, advanced sensor and guidance components for flight and satellite systems, components for light-weight high-performance aircraft engines, and structural components for helicopters. Aluminum-beryllium materials are now available in the form of near net shape investment castings. In this materials properties characterization study, the cryogenic tensile and fracture properties of an investment casting alloy, Beralcast 363, were determined. Tensile testing was performed at 21 C (70 F), -73.3 C (-100 F), -195.5 C (-320 F) and -252.8 C (-423 F), and fracture (K(sub lc) and da/dN) testing was performed at -73.3 C (-100 F), -195.5 C (-320 F) and -252.8 C (-423 F). Their use is attractive for weight critical structural applications such as advanced

Gamwell, W. R.↗
NASA NTRS1981

Blade loss transient dynamics analysis, volume 2. Task 2: Theoretical and analytical development. Task 3: Experimental verification

The component element method was used to develop a transient dynamic analysis computer program which is essentially based on modal synthesis combined with a central, finite difference, numerical integration scheme. The methodology leads to a modular or building-block technique that is amenable to computer programming. To verify the analytical method, turbine engine transient response analysis (TETRA), was applied to two blade-out test vehicles that had been previously instrumented and tested. Comparison of the time dependent test data with those predicted by TETRA led to recommendations for refinement or extension of the analytical method to improve its accuracy and overcome its shortcomings. The development of working equations, their discretization, numerical solution scheme, the modular concept of engine modelling, the program logical structure and some illustrated results are discussed. The blade-loss test vehicles (rig full engine), the type of measured data, and the engine structural model are described.

Gallardo, V. C.↗