Demonstration and Analysis of Volumetric Additive Manufacturing via Sub-Orbital Spaceflight Testing
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Engineering - Space vehicles and technology↗
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Long-term Dynamical Stability in the Outer Solar System. I. The Regular and Chaotic Evolution of the 34 Largest Trans-Neptunian Objects
We carried out an extensive analysis of the stability of the outer solar system, making use of the frequency analysis technique over short-term integrations of nearly 100,000 test particles, as well as a statistical analysis of 200 1 Gyr long numerical simulations, which consider the mutual perturbations of the giant planets and the 34 largest trans-Neptunian objects (we have called all 34 objects “dwarf planets,” DPs, even if probably only the largest of them are true DPs). From the frequency analysis, we produced statistical diffusion maps for a wide region of the a–e phase-space plane; we also present the average diffusion time for orbits as a function of perihelion. We later turned our attention to the 34 DPs, making an individualized analysis for each of them and producing a first approximation of their future stability. From the 200 distinct realizations of the orbital evolution of the 34 DPs, we classified the sample into three categories, including 17 stable, 11 unstable, and 6 resonant objects; we also found that, statistically, two objects from the sample will leave the trans-Neptunian region within the next gigayear, most likely being ejected from the solar system, but with a nonnegligible probability of going inside the orbit of Neptune, either to collide with a giant planet or even falling to the inner solar system, where our simulations are no longer able to resolve their continuous evolution.
79 ASTRONOMY AND ASTROPHYSICS↗
In-Situ SEM High Strain Rate Testing of Large Diameter Micropillars Followed by TEM and EBSD Postmortem Analysis
Background Dislocation dynamic simulations are intended as a tool to understand and predict the mechanical behavior of metallic materials, but its prediction has never been directly verified by experiments due to differences in specimen strain rate and size. Objective In this work, a comprehensive experimental framework is proposed to attempt direct comparison between experiments and discrete dislocation dynamics (DDD) modelling. Methods By integrating high-throughput sample fabrication and a customized testing apparatus, the sample size and strain rate typically employed in DDD simulations are explored experimentally. Constitutive properties such as stress-strain response are measured, and microstructural information is obtained from transmission electron microscopy (TEM) imaging, electron backscatter diffraction (EBSD), and TEM-based orientation mapping. Results Magnesium and copper were selected, as case studies, to demonstrate the newly developed experimental procedure. Measured stress-strain responses for Mg are consistent with those obtained with a miniaturized Hopkison bar experiments. Furthermore, by exploiting the validated workflow, the effect of strain rate on micropillar heterogeneous deformation and associated dislocation plasticity were revealed. Conclusion The work establishes a methodology for the systematic study of not only metals but also other materials and structures at the microscale and high strain rates.
42 ENGINEERING↗
Evaluation of Additively Manufactured Monolithic SiC and SiC-Matrix Ceramic Matrix Composites for Concentrating Solar Receiver Applications - Fabrication and Testing of Receiver Design Feature Specimens in a Simulating Lab Test via Laser Heating
Increasing operating temperatures of solar receivers is paramount to the efficiency of concentrated solar thermal (CST) and solar power (CSP) systems. Owing to its high temperature stability combined with excellent thermal and optical properties, SiC has been the material of choice for application in high-temperature solar receivers. We report the results of our study of the effective heat transfer characteristics of several candidate SiC structure motifs, or feature geometries, which are fabricated via additive manufacturing. The SiC structure motifs studied include different permutations of three-dimensional periodic lattices and defined shapes. A solar-thermal simulating laboratory test setup is constructed using a 4kW CO2 laser system with beam shaping optics to apply concurrent radiative heating power on one face of 2”-diameter cylindrical feature specimens, representing the structure motifs of interest for receiver element design, while flowing through the sample as heat transfer fluid. Using the test setup, simulative test conditions representative of a concentrated solar flux of up to ~2000 suns could be achieved in the lab tests under varying air flow through the test structure. A simple 1D numerical analysis scheme is developed to extract an effective or compound heat transfer coefficient representative of the test structure under steady-state heat flow conditions. The test results and their use to guide the selection and optimization of SiC material and structure motifs for the receiver element design fabrication are discussed.
14 SOLAR ENERGY↗
Comparative Analysis of Radial and Random Microstructures of Mesophase Pitch Carbon Fibers
Carbon fibers (CF) with radial and random microstructures are produced. Here, these fibers are subjected to identical treatment before being mechanically tested and analyzed with Weibull analysis, with the results revealing a statistically significant difference in tensile strengths of 2.23 GPa for random CF and 1.69 GPa for radial CF. Raman mapping probed the crystalline structure perpendicular to the fiber axis and found a uniform structure, while wide‐angle X‐ray diffraction showed a significant difference of 7.5 Å in the crystallites’ basal lengths parallel to the fiber. Small‐angle X‐ray scattering is completed parallel to the fiber for the first time. A cross‐section Guinier plot of the 1D azimuthal integration is generated assuming symmetric scattering, and the parallel scatterers are found to have a similar length scale to the crystallite's length, validating the testing method. Finally, transmission electron microscopy is completed on the longitudinal cross‐section of each fiber. The radial carbon fiber is found to have a core–shell structure, as evidenced further by fast Fourier transform images. Through all studies, it is shown that the structure developed during mesophase pitch spinning altered the microstructure, thus impacting the mechanical properties, confirming a direct relationship between processing, structure, and properties.
Scherschel, Alexander [Univ. of Virginia, Charlott↗
Neutronics analysis of Full Size Plate–1 Experiment using MC21
Qualification and testing of Low Enriched Uranium fuel is desired so that it can be used in research reactors instead of High Enriched Uranium. The Full Size Plate - 1 (FSP-1) experiment involves irradiating a low enriched metallic fuel in the Advanced Test Reactor to assist in this general qualification. Prior to irradiation, an in-depth neutronics analysis is needed to ensure the safety requirements of the Advanced Test Reactor are met. To accomplish this, the MC21 software was used to analyze the FSP-1 experiment, which will allow a test run to be performed with this new fuel in the Advanced Test Reactor Critical facility. By verifying and validating the results of the MC21 software with comparisons to other codes and the preliminary irradiation in the Advanced Test Reactor Critical facility, the FSP-1 experiment will be ready to irradiate using the Advanced Test Reactor. This work is concerned with the neutronics analysis of the FSP-1 experiment using the MC21 software.
11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
Assessment of Different Approaches for Measuring Shear Fracture Appearance in Charpy Tests
In this work, different approaches for establishing shear fracture appearance (SFA) on tested Charpy specimens were assessed and compared, namely (in order of increasing expected accuracy) estimates based on characteristic forces from instrumented Charpy tests, optical measurements using image analysis software, and measurements performed with the aid of a scanning electron microscope. Comparisons between different SFA values for 129 instrumented Charpy tests currently included in the National Institute of Standards and Technology database allowed us to establish the relationships between the different available approaches and formulate recommendations for the revision of the standards ASTM E2298-18, Standard Test Method for Instrumented Impact Testing of Metallic Materials, and ISO 14556:2015, Metallic Materials — Charpy V-Notch Pendulum Impact Test — Instrumented Test Method, which currently provide four empirical correlations that can be used to estimate SFA.
36 MATERIALS SCIENCE↗
Predictive Modeling of NOx Emissions from Lean Direct Injection of Hydrogen and Hydrogen/Natural Gas Blends Using Flame Imaging and Machine Learning
This research paper explores the use of machine learning to relate images of flame structure and luminosity to measured NOx emissions. Images of reactions produced by 16 aero-engine derived injectors for a ground-based turbine operated on a range of fuel compositions, air pressure drops, preheat temperatures and adiabatic flame temperatures were captured and postprocessed. The experimental investigations were conducted under atmospheric conditions, capturing CO, NO and NOx emissions data and OH* chemiluminescence images from 27 test conditions. The injector geometry and test conditions were based on a statistically designed test plan. These results were first analyzed using the traditional analysis approach of analysis of variance (ANOVA). The statistically based test plan yielded 432 data points, leading to a correlation for NOx emissions as a function of injector geometry, test conditions and imaging responses, with 70.2% accuracy. As an alternative approach to predicting emissions using imaging diagnostics as well as injector geometry and test conditions, a random forest machine learning algorithm was also applied to the data and was able to achieve an accuracy of 82.6%. This study offers insights into the factors influencing emissions in ground-based turbines while emphasizing the potential of machine learning algorithms in constructing predictive models for complex systems.
08 HYDROGEN↗
Comparative Analysis of Heat Exchangers for High Temperature High Pressure Helium Component Testing
Helium gas loops have been designed and built to gain a better understanding of the gas thermohydraulic phenomena that take place in a helium system. Some of these loops are used for validation and testing of components for high temperature gas-cooled reactors (HTGRs). However, most of them operate at lower pressure and temperature than an HTGR. While these loops can provide valuable information about gas-cooled reactor components, the operating envelope of the experiment is constrained by the maximum operating conditions of the helium loop. In response to the lack of an experimental facility that can provide the infrastructure needed to validate and test components at nominal pressures and temperatures of HTGRS, the HElium Component Testing Out-of-pile Research (HECTOR) facility was designed at Idaho National Laboratory with the assistance of University of Idaho and Walsh Engineering. With the capability to test at temperatures up to 800°C and pressures of 8MPa, HECTOR serves as a critical tool for the advancement of HTGR technology. The facility's primary role is to provide a controlled, high-fidelity environment for the assessment of component resilience and efficiency under nominal HTGR conditions. In the quest to enhance the efficiency and performance of HECTOR, a comparative analysis of three distinct types of heat exchangers—shell and tube, offset strip fin, and printed-circuit—was conducted, focusing primarily on two critical metrics: the required surface area and pressure drop characteristics. The shell and tube heat exchanger, renowned for its robust design and widespread industrial application, was evaluated against the offset strip fin and the cuttingedge printed-circuit heat exchangers, both of which are lauded for their compactness and thermal effectiveness. This comparative study aims to provide detailed insights into the thermal management capabilities of each heat exchanger type under the conditions inherent to HECTOR, thereby facilitating an informed selection for systems demanding high operational integrity and efficiency.
22 GENERAL STUDIES OF NUCLEAR REACTORS↗
Squeeze Film Damper Experimental and Numerical Correlation: Test Setup Description and Parameter Identification of Dry System
The process of characterizing a damper involves both experimental techniques and model simulation. Experiments characterize dynamic behavior of a system through empirical modal analysis using impact and shaker testing. The layout of the test setup is crucial for a low-mass, nonlinear system. Physical arrangement, orientation of the system, and instrumentation affect the results that are discussed in this paper. These results can be used to validate a numerical simulation of the same system. With a validated model, important physical input parameters and modeling techniques can be determined and implemented in future designs. In other words, this modeling can be used with confidence to design alternative dampers that may be difficult, costly, and time-consuming to characterize experimentally.
Cook, Jason↗
Fluorescent amplification for next generation sequencing (FA-NGS) library preparation
BACKGROUND: Next generation sequencing (NGS) has become a universal practice in modern molecular biology. As the throughput of sequencing experiments increases, the preparation of conventional multiplexed libraries becomes more labor intensive. Conventional library preparation typically requires quality control (QC) testing for individual libraries such as amplification success evaluation and quantification, none of which occur until the end of the library preparation process. RESULTS: In this study, we address the need for a more streamlined high-throughput NGS workflow by tethering real-time quantitative PCR (qPCR) to conventional workflows to save time and implement single tube and single reagent QC. We modified two distinct library preparation workflows by replacing PCR and quantification with qPCR using SYBR Green I. qPCR enabled individual library quantification for pooling in a single tube without the need for additional reagents. Additionally, a melting curve analysis was implemented as an intermediate QC test to confirm successful amplification. Sequencing analysis showed comparable percent reads for each indexed library, demonstrating that pooling calculations based on qPCR allow for an even representation of sequencing reads. To aid the modified workflow, a software toolkit was developed and used to generate pooling instructions and analyze qPCR and melting curve data. CONCLUSIONS: We successfully applied fluorescent amplification for next generation sequencing (FA-NGS) library preparation to both plasmids and bacterial genomes. As a result of using qPCR for quantification and proceeding directly to library pooling, the modified library preparation workflow has fewer overall steps. Therefore, we speculate that the FA-NGS workflow has less risk of user error. The melting curve analysis provides the necessary QC test to identify and troubleshoot library failures prior to sequencing. While this study demonstrates the value of FA-NGS for plasmid or gDNA libraries, we speculate that its versatility could lead to successful application across other library types.
59 BASIC BIOLOGICAL SCIENCES↗
Hydraulic Response to Thermal Stimulation Efforts at Raft River Based on Stepped Rate Injection Testing
The injection well stimulation project at the Raft River geothermal field tests the effect of long-term cold water injection and high pressure injection on well injectivity, improvements to which could reduce operating costs. The primary data for analysis and interpretation of the injection test are step-rate flow tests run before each new phase of the injection. These tests were analyzed using a combination of standard pump-test analytical solution methods and methods developed expressly for the observed conditions. The stepped rate injection tests, combined with long-term flow and pressure response data suggest that the well is located within a fractured formation of low transmissivity but high storativity. These calculated parameters appeared to increase with pressure during the first injection test and the higher values were reproduced during the second stepped rate test. Calculated transmissivity and storativity are on the order of 4E-5 m cm 2 and 1E-4 m Pa -1 , respectively. The apparent pressure dependence of fitted hydraulic parameters may reflect near-well fracture compliance that increased the effective radius of the wellbore during the first test. While the type curve fit analysis also suggests that the reservoir behaves as a uniformly fractured reservoir with a radial flow regime, the hydraulic parameters indicate that condition may exist only a very limited distance (<10 m) from the well. Longer-term pressure response suggests that flow in the system effectively reaches steady state in a period of less than a day, which may reflect pressure stabilization resulting from pressure-dependent permeability or a region of much higher permeability located with a few meters of the well. The transmissivity estimates obtained from this analysis, converted to approximate fracture density and aperture, provide useful constraints on the distance to which the thermal front may migrate from the well during the cold water injection phase of the stimulation project. We estimate that the cooling front will migrate less than a tenth of a kilometer over an approximately one-year injection period. Here, the effects of that cooling, however, may be substantial, because increases in permeability have maximum effect nearest the well.
cold water injection↗
Methods and compositions for identification of source of microbial contamination in a sample
Herein are described 1058 different bacterial taxa that were unique to either human, grazing mammal, or bird fecal wastes. These identified taxa can serve as specific identifier taxa for these sources in environmental waters. Two field tests in marine waters demonstrate the capacity of phylogenetic microarray analysis to track multiple sources with one test.
Andersen, Gary L.↗
International Benchmarking: A Global Perspective of Workplace Drug and Alcohol Testing
Workplace drug and alcohol testing has been widely implemented in diverse industries and is designed to detect the use of and deter the influence of legal and illegal substances that would impair the ability to perform work that has significant security and safety implications. Across the globe, patterns of drug and alcohol use and abuse and the regulations controlling drug and alcohol use vary by location (e.g., regions, countries, etc.). The prevalence of workplace drug and alcohol testing and protection of individuals’ rights in the workplace similarly tend to exhibit contextual differences. With the advancements in drug-testing technologies and the recent issuance of guidance for additional testing matrices (e.g., oral fluid, hair, etc.) by the U.S. Department of Health and Human Services, gaining a global perspective on the current state of drug and alcohol testing practices and regulations is important for leveraging such advancements to improve the effectiveness of drug and alcohol testing. The U.S. Nuclear Regulatory Commission (NRC) tasked the Pacific Northwest National Laboratory (PNNL) fitness for duty (FFD) team to conduct a benchmarking analysis of international drug and alcohol testing regulations and programs to identify similarities and differences in workplace testing programs and the basis for any differences. The benchmarking study focuses on a policy analysis and benchmarking metrics comparison among different countries and regions. The policy analysis includes the following three types of relevant international and national policies relevant to drug and alcohol testing in the nuclear industry: 1. National drug and alcohol policy 2. Workplace drug and alcohol testing 3. FFD regulations for Nuclear Power Plants The international drug and alcohol benchmarking metrics focusses on the use of blood, breath, urine, hair, and oral fluid in testing; drug and drug metabolite cutoff values; point-of-collection testing devices; roadside testing methodologies; innovations in drug testing; and the extent of availability of such data. Gaining an understanding of workplace drug and alcohol testing in other countries as well as information about new testing methods, matrices, tools, and technologies that other countries have adopted provides NRC with international comparative information regarding the technical basis for such programs and methods as it relates to the protection of worker and public health and safety.
98 NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL P↗
Analysis of Uncertainty Impacts on Emissions and Fuel Economy Evaluation for Chassis Dynamometer Testing
This study illustrates a methodology for quantifying the uncertainties encountered in the measurement of tailpipe emissions and in the fuel consumption measurements for light-duty conventional vehicles tested on a four-wheel drive chassis dynamometer. The study leverages high-fidelity experimental data collected over three standard drive cycles, UDDS, HWY and US06, intended to simulate a wide range of operating conditions. Here, a method is developed to estimate the measurement uncertainties in fuel consumption for a test cycle, which occur due to the accumulation of measurement uncertainties propagated through the system. The uncertainty determination model uses statistical analysis and standard propagation techniques to evaluate and combine the uncertainties introduced from various sources (including the vehicle, chassis dynamometer, driver, and instrumentation). The analysis also examines three different experimental methods for determining the fuel consumption: 1) carbon mass balance, 2) volumetric fuel scale and 3) gravimetric fuel scale, and takes into consideration the properties of the instrumentation used. The results show that the most significant influence on the determination of the emissions comes from the concentration measurement, and similarly the biggest impact on the total fuel consumption uncertainty comes from the uncertainty in the determination of the carbon dioxide mass, due to the large presence of this pollutant in the overall emissions. It was found that the fuel consumption uncertainties are in the range of ±1-2% for all three methods analyzed, with the lowest values being obtained for measurements performed using the gravimetric method for all three drive cycles considered.
33 ADVANCED PROPULSION SYSTEMS↗
Cytrics Repository Of Analysis Tools And Engineering Resources
Cybersecurity Testing for Resilient Industrial Control Systems (CyTRICS) is a DOE-funded project that works with vendors to evaluate the cybersecurity of equipment used in US critical infrastructure. In the process of testing systems, CyTRICS researchers often develop custom tools. The tools in this repository were developed during multiple CyTRICS tests to assist with the testing process. They help solve problems encountered by CyTRICS researchers and address uncommon testing subjects for which limited tooling is available. They are useful to other researchers working on similar systems and architectures.
Laird, SutterE↗
Cross-Code Verification of Neutronics Analysis Tools at INL Applied for 238 Pu Production in the Advanced Test Reactor
Here, analyses are completed for experiments prior to experiment irradiation in the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL). Various codes are used to qualify all experiments planned for insertion in the reactor, thereby ensuring that all safety and programmatic requirements are satisfied preirradiation. Among the common experiment analysis tools at INL are MCNP5 coupled to ORIGEN2 (MOPY) and MC21. MOPY uses MCNP5 for transport calculations along with calculations for fluxes and select reaction rates, and then ORIGEN2 handles the step-by-step and postirradiation depletion. MC21 handles all in-reactor transport and step-by-step, during-irradiation, depletion calculations, and then ORIGEN (SCALE 6.2.3) is used for decay and dose calculations postirradiation. The MOPY results, along with those obtained via two variations of the MC21 model, were compared in terms of 238 Pu production in the ATR’s H10 position. For the MOPY model, the MC21 model utilizing the HELIOS-based fission product (FP) library, and the MC21 model utilizing the expanded 1300 FP library, the during-cycle irradiation in-core heating results were sufficiently equivalent; however, the MOPY model and the MC21 model with the HELIOS library showed some differences relating to the respective FP libraries. Ultimately, the MC21 model with a 1300 FP library produced the most consistent results throughout the cycle, whereas the MC21 model that utilized the (smaller) HELIOS library was able to handle during-irradiation analysis but lacked certain short-lived FPs that significantly contributed to the total decay heat at shutdown. MOPY, on the other hand, was found to overpredict fission gas production, as a result of limitations in the ORIGEN2 code.
ATR↗
Representation and Impact of Water Head on Power System Planning and Operation
Representing water head information in power system model files, can provide a more realistic model of the system and thereby inform operation and planning personnel in the decision-making process. This article describes a procedure for modifying the power system model files (steady-state and dynamic) to represent water head information. Additionally, the impact of representing the water head on power system reliability studies including contingency analysis, cascading failure analysis and dynamic frequency response analysis has been investigated, using the modified power system models. This paper considers the detailed Western Electricity Coordination Council model during summer and winter conditions as the test system for the impact analysis. Results show that under reduced water head: 1) the number of critical voltage and branch flow violations increases; 2) chances of cascading failure and island formation increases; and 3) frequency nadir decreases as compared to those of the base cases where the water head information is not represented.
13 - HYDRO ENERGY↗