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At least 73 records · Page 4

Deep Reactive Ion Etching (DRIE) of High Aspect Ratio SiC Microstructures using a Time-Multiplexed Etch-Passivate Process

High aspect ratio silicon carbide (SiC) microstructures are needed for microengines and other harsh environment micro-electro-mechanical systems (MEMS). Previously, deep reactive ion etching (DRIE) of low aspect ratio (AR less than or = 1) deep (greater than 100 micron) trenches in SiC has been reported. However, existing DRIE processes for SiC are not well-suited for definition of high aspect ratio features because such simple etch-only processes provide insufficient control over sidewall roughness and slope. Therefore, we have investigated the use of a time-multiplexed etch-passivate (TMEP) process, which alternates etching with polymer passivation of the etch sidewalls. An optimized TMEP process was used to etch high aspect ratio (AR greater than 5) deep (less than 100 micron) trenches in 6H-SiC. Power MEMS structures (micro turbine blades) in 6H-SiC were also fabricated.

Evans, Laura J.↗

Aerodynamic Characteristics of Low-Aspect-Ratio Wings in Close Proximity to the Ground

A wind-tunnel investigation has been conducted to determine the effect of ground proximity on the aerodynamic characteristics of thick highly cambered rectangular wings with aspect ratios of 1. 2, 4, and 6. The results showed that, for these aspect ratios, as the ground war, approached all wings experienced increases in lift-curve slope and reductions in induced drag which resulted in increases in lift-drag ratio. Although an increase in lift-curve slope was obtained for all aspect ratios as the ground was approached, the lift coefficient at an angle of attack of 0 deg for any given aspect ratio remained nearly constant. The experimental results were in general agreement with Wieselsberger's ground-effect theory (NACA Technical Memorandum 77). As the wings approached the ground, there was an increase in static longitudinal stability at positive angles of attack. When operating in ground effect, all the wings had stability of height at positive angles of attack and instability of height at negative angles of attack. Wing-tip fairings on the wings with aspect ratios of 1 and 2 produced small increases in lift-drag ratio in ground effect. End plates extending only below the chord plane on the wing with an aspect ratio of 1 provided increases in lift coefficient and in lift-drag ratio in ground effect.

Fink, Marvin P.↗

Comparison of High Aspect Ratio Cooling Channel Designs for a Rocket Combustion Chamber

An analytical investigation on the effect of high aspect ratio (height/width) cooling channels, considering different coolant channel designs, on hot-gas-side wall temperature and coolant pressure drop for a liquid hydrogen cooled rocket combustion chamber, was performed. Coolant channel design elements considered were: length of combustion chamber in which high aspect ratio cooling was applied, number of coolant channels, and coolant channel shape. Seven coolant channel designs were investigated using a coupling of the Rocket Thermal Evaluation code and the Two-Dimensional Kinetics code. Initially, each coolant channel design was developed, without consideration for fabrication, to reduce the hot-gas-side wall temperature from a given conventional cooling channel baseline. These designs produced hot-gas-side wall temperature reductions up to 22 percent, with coolant pressure drop increases as low as 7.5 percent from the baseline. Fabrication constraints for milled channels were applied to the seven designs. These produced hot-gas-side wall temperature reductions of up to 20 percent, with coolant pressure drop increases as low as 2 percent. Using high aspect ratio cooling channels for the entire length of the combustion chamber had no additional benefit on hot-gas-side wall temperature over using high aspect ratio cooling channels only in the throat region, but increased coolant pressure drop 33 percent. Independent of coolant channel shape, high aspect ratio cooling was able to reduce the hot-gas-side wall temperature by at least 8 percent, with as low as a 2 percent increase in coolant pressure drop. The design with the highest overall benefit to hot-gas-side wall temperature and minimal coolant pressure drop cooling can now be done in relatively short periods of time with multiple iterations.

Wadel, Mary F.↗

Ultra-high aspect ratio pores milled in diamond via laser, ion and electron beam mediated processes

Microfabrication techniques are critical for the rapid prototyping and development of applications for cutting edge materials. Recently diamond has gained considerable interest for quantum photonic, biosensing, inertial confinement fusion and magnetometer applications. In this article, ultra-high aspect ratio milling of diamond micropores by photon, ion and electron based methods is reported. A multiphoton absorption laser ablation approach is revealed to rapidly produce sub-10 μm diameter micropores in diamond with an aspect ratio of 14:1 and a tapered profile at the surface interface. Chemically active, oxygen focused ion beam milling produces high-aspect ratio pores in diamond with an aspect ratio of 65:1 and minimal tapering over the length of the pore, overcoming the physical interaction volume limitations imposed in conventional gallium based focused ion beam milling and laser ablation methods. Oxygen-mediated electron beam induced etching is revealed to negate the limitations imposed by physical sputtering mechanisms utilized in focused ion beam milling via the direct initiation of chemical reactions at the receding surface, producing aspect ratios on the order of 200:1. Numerical simulations reveal the physical basis for the superior aspect-ratio pore milling of the oxygen focused ion beam milling and electron beam induced etching methods. Our results demonstrate direct-write methods for the fabrication of ultra-high aspect micropores in diamond and provide insight into the underlying mechanisms of these physical processes. The three methods demonstrated here can be interchanged for applications based on the desired characteristic aspect ratio and process throughput.

36 MATERIALS SCIENCE↗

One-pot rapid synthesis of high aspect ratio silver nanowires for transparent conductive electrodes

Highlights: • We improved a method of preparation of silver nanowires. • The effects of PVP molecular weight and concentration on the morphology and aspect ratio of AgNWs were investigated. • The preferred orientation growth mechanism of AgNWs was also discussed briefly. • We got transparent conductive films by spin-coating silver nanowires dispersion which is compared to ITO films. • The effects of silver nanowires density and heating time on the sheet resistance and transmittance were investigated. - Abstract: Silver nanowires (AgNWs) with high aspect ratio were rapidly one-pot synthesized by a polyol process in the presence of polyvinylpyrrolidone (PVP) as a stabilizer as well as the anisotropic agent, and the corresponding transparent conductive films were prepared by spin-coating method. The effects of PVP molecular weight and concentration on the morphology and aspect ratio of AgNWs were investigated in detail, and the optoelectrical properties of the transparent conductive films were briefly introduced. The presence of PVP induces the growth of silver directed to form high aspect-ratio nanowires by a high anisotropic mode. Appropriate PVP molecular weight and concentration allows the rapid synthesis of AgNWs with the diameter of about 78.2 nm, the length of 79.52 μm and the aspect ratio as high as 1009.2. The as-prepared AgNWs films possess a transmittance of 81.6% and a sheet resistance of 11.36 Ω/sq. The resultant AgNWs with high aspect ratio can be applied to prepare transparent conductive electrodes.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

High- β equilibrium and ballooning stability of the low aspect ratio CNT stellarator

In the paper, the existence and ballooning-stability of low aspect ratio stellarator equilibria is predicted for the Columbia Neutral Torus (CNT) with the aid of 3D numerical tools. In addition to having a low aspect ratio, CNT is characterized by a low magnetic field and small plasma volume. Also, highly overdense plasmas were recently heated in CNT by means of microwaves. These characteristics suggest that CNT might attain relatively high values of plasma beta and thus be of use in the experimental study of stellarator stability to high-beta instabilities such as ballooning modes. As a first step in that direction, here the ballooning stability limit is found numerically. Depending on the particular magnetic configuration we expect volume-averaged β limits in the range 0.9%–3.0%, and possibly higher, and observe indications of a second region of ballooning stability. As the aspect ratio is reduced, stability is found to increase in some configurations and decrease in others. Energy-balance estimates using stellarator scaling laws indicate that the lower β limit may be attainable with overdense heating at powers of 40 to 100 kW. The present study serves the additional purpose of testing VMEC and other stellarator codes at high values of β and at low aspect ratios. For this reason, the study was carried out both for free boundary, for maximum fidelity to experiment, as well as with a fixed boundary, as a numerical test.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Global gyrokinetic study of shaping effects on electromagnetic modes at NSTX aspect ratio with ad hoc parallel magnetic perturbation effects

Plasma shaping may have a stronger effect on global turbulence in tight-aspect-ratio tokamaks than in conventional-aspect-ratio tokamaks due to the higher toroidicity and more acute poloidal asymmetry in the magnetic field. In addition, previous local gyrokinetic studies have shown that it is necessary to include parallel magnetic field perturbations in order to accurately compute growth rates of electromagnetic modes in tight-aspect-ratio tokamaks. In this work, the effects of elongation and triangularity on global, ion-scale, linear electromagnetic modes are studied at National Spherical Torus Experiment (NSTX) aspect ratio and high plasma β using the global gyrokinetic particle-in-cell code XGC. The effects of compressional magnetic perturbations are approximated via a well-known modification to the particle drifts that was developed for flux-tube simulations [Joiner et al., Phys. Plasmas 17, 072104 (2010)], without proof of its validity in a global simulation, with the gyrokinetic codes GENE and GEM being used for local verification and global cross-verification. Magnetic equilibria are re-constructed for each distinct plasma profile that is used. Coulomb collision effects are not considered. Within the limitations imposed by the present study, it is found that linear growth rates of electromagnetic modes (collisionless microtearing modes and kinetic ballooning modes) are significantly reduced in a high-elongation and high-triangularity NSTX-like geometry compared to a circular NSTX-like geometry. For example, growth rates of kinetic ballooning modes at high- β are reduced to the level of that of collisionless trapped electron modes.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Experimental study of low aspect ratio compressor blading

The effects of low aspect ratio blading on aerodynamic performance were examined. Four individual transonic compressor stages, representative of the inlet stage of an advanced high pressure ratio core compressor, are discussed. The flow phenomena for the four stages are investigated. Comparisons of blade element parameters are presented for the two different aspect ratio configurations. Blade loading levels are compared for the near stall conditions and comparisons are made of loss and diffusion factors over the operating range of incidence angles.

Reid, L.↗

Convergence acceleration of implicit schemes in the presence of high aspect ratio grid cells

The performance of Navier-Stokes codes are influenced by several phenomena. For example, the robustness of the code may be compromised by the lack of grid resolution, by a need for more precise initial conditions or because all or part of the flowfield lies outside the flow regime in which the algorithm converges efficiently. A primary example of the latter effect is the presence of extended low Mach number and/or low Reynolds number regions which cause convergence deterioration of time marching algorithms. Recent research into this problem by several workers including the present authors has largely negated this difficulty through the introduction of time-derivative preconditioning. In the present paper, we employ the preconditioned algorithm to address convergence difficulties arising from sensitivity to grid stretching and high aspect ratio grid cells. Strong grid stretching is particularly characteristic of turbulent flow calculations where the grid must be refined very tightly in the dimension normal to the wall, without a similar refinement in the tangential direction. High aspect ratio grid cells also arise in problems that involve high aspect ratio domains such as combustor coolant channels. In both situations, the high aspect ratio cells can lead to extreme deterioration in convergence. It is the purpose of the present paper to address the reasons for this adverse response to grid stretching and to suggest methods for enhancing convergence under such circumstances. Numerical algorithms typically possess a maximum allowable or optimum value for the time step size, expressed in non-dimensional terms as a CFL number or vonNeumann number (VNN). In the presence of high aspect ratio cells, the smallest dimension of the grid cell controls the time step size causing it to be extremely small, which in turn results in the deterioration of convergence behavior. For explicit schemes, this time step limitation cannot be exceeded without violating stability restrictions of the scheme. On the other hand, for implicit schemes, which are typically unconditionally stable, there appears to be room for improvement through careful tailoring of the time step definition based on results of linear stability analyses. In the present paper, we focus on the central-differenced alternating direction implicit (ADI) scheme. The understanding garnered from this analyses can then be applied to other implicit schemes. In order to systematically study the effects of aspect ratio and the methods of mitigating the associated problems, we use a two pronged approach. We use stability analyses as a tool for predicting numerical convergence behavior and numerical experiments on simple model problems to verify predicted trends. Based on these analyses, we determine that efficient convergence may be obtained at all aspect ratios by getting a combination of things right. Primary among these are the proper definition of the time step size, proper selection of viscous preconditioner and the precise treatment of boundary conditions. These algorithmic improvements are then applied to a variety of test cases to demonstrate uniform convergence at all aspect ratios.

Buelow, B. E. O.↗

Jet-Surface Interaction: High Aspect Ratio Nozzle Test, Nozzle Design and Preliminary Data

The Jet-Surface Interaction High Aspect Ratio (JSI-HAR) nozzle test is part of an ongoing effort to measure and predict the noise created when an aircraft engine exhausts close to an airframe surface. The JSI-HAR test is focused on parameters derived from the Turbo-electric Distributed Propulsion (TeDP) concept aircraft which include a high-aspect ratio mailslot exhaust nozzle, internal septa, and an aft deck. The size and mass flow rate limits of the test rig also limited the test nozzle to a 16:1 aspect ratio, half the approximately 32:1 on the TeDP concept. Also, unlike the aircraft, the test nozzle must transition from a single round duct on the High Flow Jet Exit Rig, located in the AeroAcoustic Propulsion Laboratory at the NASA Glenn Research Center, to the rectangular shape at the nozzle exit. A parametric nozzle design method was developed to design three low noise round-to-rectangular transitions, with 8:1, 12:1, and 16: aspect ratios, that minimizes flow separations and shocks while providing a flat flow profile at the nozzle exit. These designs validated using the WIND-US CFD code. A preliminary analysis of the test data shows that the actual flow profile is close to that predicted and that the noise results appear consistent with data from previous, smaller scale, tests. The JSI-HAR test is ongoing through October 2015. The results shown in the presentation are intended to provide an overview of the test and a first look at the preliminary results.

Aeroacoustics↗

Microwave synthesis and photocatalytic activities of ZnO bipods with different aspect ratios

Highlights: • We synthesized linked ZnO nanorods by a facile microwave method. • The effect of reaction parameters on ZnO was investigated. • ZnO bipods with different aspect ratios were prepared. • The photocatalytic performance of ZnO bipods was evaluated. - Abstract: Linked ZnO nanorods have been successfully prepared via a facile microwave method without any post-synthesis treatment. The X-ray diffraction (XRD) patterns indicated the precursor had completely transformed into the pure ZnO crystal. The images of field emitting scanning electron microscope (FESEM) and transmission electron microscope (TEM) showed that linked ZnO nanorods consisted predominantly of ZnO bipods. The formation process of the ZnO bipods was clearly discussed. ZnO bipods with different aspect ratios have been obtained by tuning the concentrations of reagents and microwave power. Moreover, the photocatalytic performance of ZnO bipods with different aspect ratios for degradation of methylene blue was systematically evaluated. The results of photocatalytic experiments showed that the photocatalytic activity increased with the aspect ratios of ZnO bipods increased. The reason is that ZnO bipods with larger aspect ratio have higher surface area, which can absorb more MB molecules to react with ·OH radicals.

36 MATERIALS SCIENCE↗

Algorithms for high aspect ratio oriented triangulations

Grid generation plays an integral part in the solution of computational fluid dynamics problems for aerodynamics applications. A major difficulty with standard structured grid generation, which produces quadrilateral (or hexahedral) elements with implicit connectivity, has been the requirement for a great deal of human intervention in developing grids around complex configurations. This has led to investigations into unstructured grids with explicit connectivities, which are primarily composed of triangular (or tetrahedral) elements, although other subdivisions of convex cells may be used. The existence of large gradients in the solution of aerodynamic problems may be exploited to reduce the computational effort by using high aspect ratio elements in high gradient regions. However, the heuristic approaches currently in use do not adequately address this need for high aspect ratio unstructured grids. High aspect ratio triangulations very often produce the large angles that are to be avoided. Point generation techniques based on contour or front generation are judged to be the most promising in terms of being able to handle complicated multiple body objects, with this technique lending itself well to adaptivity. The eventual goal encompasses several phases: first, a partitioning phase, in which the Voronoi diagram of a set of points and line segments (the input set) will be generated to partition the input domain; second, a contour generation phase in which body-conforming contours are used to subdivide the partition further as well as introduce the foundation for aspect ratio control, and; third, a Steiner triangulation phase in which points are added to the partition to enable triangulation while controlling angle bounds and aspect ratio. This provides a combination of the advancing front/contour techniques and refinement. By using a front, aspect ratio can be better controlled. By using refinement, bounds on angles can be maintained, while attempting to minimize the number of Steiner points.

Posenau, Mary-Anne K.↗

Experimental study of low aspect ratio compressor blading

The paper presents a study of low aspect blading for the inlet stages of a high pressure ratio, high-speed core compressor. The basic overall design variables were stage pressure ratio and blade aspect ratio; these four stages represent two levels of total pressure ratio, two levels of rotor blade aspect ratio, and two levels of stator vane aspect ratios. Comparisons of the overall performance, radial distributions of performance parameters, diffusion factors at the near-stall conditions, blade element data, and the axial distribution of rotor tip static pressures yielded the following results: (1) higher peak pressure ratio, high stage and rotor efficiencies, and greater stall margin were obtained with the lower aspect ratio blading, (2) the lower aspect ratio blading showed improved performance over the entire blade span, and (3) the lower aspect ratio rotors operated at higher diffusion factors and higher incidence angles over the entire blade span.

Reid, L.↗

Investigation at low speeds of the effect of aspect ratio and sweep on rolling stability derivatives of untapered wings

A low scale wind tunnel investigation was conducted in rolling flow to determine the effects of aspect ratio and sweep (when varied independently) on the rolling stability derivatives for a series of untapered wings. Test results indicate that when the aspect ratio was held constant, an increase in the sweepback angle caused a significant reduction in the damping in roll at low lift coefficients for only the higher aspect ratios that were tested. This result was in agreement with available swept wing theory which indicated no effect of sweep for aspect ratios near zero. The result of the linear theory that the damping in roll is independent of lift coefficient and that the yawing moment and lateral force due to rolling are directly proportional to the lift coefficient was found to be valid for only a very limited lift coefficient range when the wings were highly swept. For such wings, the damping was found to increase in magnitude and the yawing moment due to rolling, to change from negative to positive at moderate lift coefficients. The effect of wing tip suction, not acounted for by present theory, was found to be very important with regard to the yawing moment due to rolling, particularly for low aspect ratio swept wings. An empirical means of correcting present theory for the effect of tip suction is suggested.

Goodman, Alex↗

Design and Analyses of High Aspect Ratio Nozzles for Distributed Propulsion Acoustic Measurements

A series of three convergent, round-to-rectangular high aspect ratio (HAR) nozzles were designed for acoustic testing at the NASA Glenn Research Center Nozzle Acoustic Test Rig (NATR). The HAR nozzles had exit area aspect ratios of 8:1, 12:1, and 16:1. The nozzles were designed to mimic a distributed propulsion system array with a slot nozzle. The nozzle designs were screened using Reynolds-Averaged Navier-Stokes (RANS) simulations. In addition to meeting the geometric constraints required for testing in the NATR, the HAR nozzles were designed to be free of flow features that would produce unwanted noise (e.g., flow separations) and to have uniform flow at the nozzle exit. Multiple methods were used to generate HAR nozzle designs. The final HAR nozzle designs were generated in segments using a computer code that parameterized each segment. RANS screening simulations showed that intermediate nozzle designs suffered flow separation, a normal shockwave at the nozzle exit (caused by an aerodynamic throat produced by boundary layer growth), and non-uniform flow at the nozzle exit. The RANS simulations showed that the final HAR nozzle designs were free of flow separations, but were not entirely successful at producing a fully uniform flow at the nozzle exit. The final designs suffered a pair of counter-rotating vortices along the outboard walls of the nozzle. The 16:1 aspect ratio HAR nozzle had the least uniform flow at the exit plane; the 8:1 aspect ratio HAR nozzles had a fairly uniform flow at the nozzle exit plane.

acoustic measure↗

Direct fabrication of high aspect-ratio metal oxide nanopatterns via sequential infiltration synthesis in lithographically defined SU-8 templates

Nanopatterning high aspect-ratio metal oxide structures remains challenging for conventional nanofabrication methods based on reactive ion etching due to marginal etch selectivity between target oxides and typical mask materials. Here, the authors report the application of sequential infiltration synthesis (SIS) on lithographically defined SU-8 polymer templates for patterning arbitrarily designed, high aspect-ratio metal oxide nanostructures with sub-50 nm linewidths, smooth vertical profiles, and three-dimensional (3D) morphologies difficult to achieve by the conventional fabrication methods. As examples, various AlOx nanostructures with ∼40 nm linewidths and up to 16 aspect ratios were demonstrated, along with TiOx in-plane nanowire arrays of controlled positional registrations. Detailed scanning and transmission electron microscopy studies revealed nanocrystalline and amorphous internal structures of respective AlOx and TiOx, as well as the swelling and contraction behaviors of polymer templates during the SIS process, which allowed the facile fabrication of high aspect-ratio, sub-50 nm-featured oxide nanopatterns with 3D morphologies. These results confirm the potential of vapor-phase material infiltration in directly nanopatterning complexly structured metal oxides.

Nam, Chang-Yong↗

Global gyrokinetic stability of collisionless microtearing modes in large aspect ratio tokamaks

Linear full radius gyrokinetic calculations show the existence of unstable microtearing modes (MTMs) in purely collisionless, high temperature, large aspect ratio tokamak plasmas. The present study takes into account fully gyrokinetic highly passing ions and electrons. The global 2-D structures of the collisionless mode with full radius coupling of the poloidal modes is obtained and compared with another electromagnetic mode, namely, the Alfvén Ion Temperature Gradient (AITG) mode (or Kinetic Ballooning Mode, KBM) for the same equilibrium profile. Several important characteristics of the modes are brought out and compared, such as a clear signature in the symmetry properties of the two modes, the plasma–β dependence, and radial and poloidal length scales of the electrostatic and magnetic vector potential fluctuations. Extensive parameter scans for this collisionless microtearing mode reveal the scaling of the growth rate with β and the electron temperature gradient η{sub e}. Scans at different β values show an inverse relationship between the η{sub e} threshold and β, leading to a stability diagram, and implying that the mode might exist at moderate to strong temperature gradients for finite β plasmas in large aspect ratio tokamaks. In contrast to small aspect ratio tokamaks where the trapped electron magnetic drift resonance is found to be important, in large aspect ratio tokamaks, a strong destabilization due to the magnetic drift resonance of passing electrons is observed and is identified as a possible collisionless drive mechanism for the collisionless MTM.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Plasma Focused Ion Beam Milling of High-Aspect-Ratio Holes in Diamond

Plasma focused ion beam (PFIB) technology has a great potential for applications requiring rapid micro-machining of high-aspect-ratio features. Here, we use 30-keV Ar, Xe, and O 2 ion beams to study PFIB milling of high-aspect-ratio circular holes in polycrystalline diamond. Our results show that Xe and O 2 ion beams have the highest milling efficiency for low-aspect-ratio and high-aspect-ratio hole milling, respectively. Each ion beam species produces holes with its characteristic shape and wall surface morphology. In conclusion, based on these results, we demonstrate a “hybrid” hole milled in a two-step process with Xe and O 2 ion beams with the geometry and wall morphology attractive for the attachment of a fuel fill tube to the inertial confinement fusion capsule.

ICF targets↗