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At least 73 records · Page 4

Pulsed-Current Welding Of Nickel-Based Alloy

Joints as strong (or stronger than) joints made with constant current. Report based on study of pulsed-current versus constant-current gas/tungsten arc welding of butt joints between panels of nickel-based alloy 718. In pulsed-current welding, arc current alternated between high and low value. Enables greater control of freezing and depth of penetration of weld puddle at given heat input. Thicker sections joined. Readily incorporated into automated welding system, with resultant greater uniformity and reproducibility of welds than attained in manual welding.

Gamwell, W. R.↗

The Effect of Laser Scan Strategy on Distortion and Residual Stresses of Arches Made With Selective Laser Melting

The NASA Marshall Space Flight Center (MSFC) is developing Additive Manufacturing (AM) - both in-space AM for on-demand parts, tools, or structures, and on-earth AM for rapid, reduced-cost, small volume production of complex space-flight hardware. Selective Laser Melting (SLM) is an on-earth AM technology that MSFC is using to build Alloy 718 rocket engine components. An understanding of the SLM-718 material properties is required to design, build, and qualify these components for space flight. Residual stresses and are of particular interest for this AM process, since SLM is a series of approximately 100 micron-wide welds, where highly non-linear heating and cooling, severe thermal gradients and repeated thermal cycling can result in high residual stresses within the component. These stresses may cause degraded material properties, and warp or distort the geometry of the SLM component. The distortions can render the component out-of-tolerance when inspected, and even interrupt or halt the build process if the warped material prevents the SLM machine from operating properly. The component must be scrapped and re-designed, which is time consuming and costly. If residual stresses are better understood, and can be predicted, these effects can be mitigated early in the component's design. the compressive residual stresses in the z-direction were highest in the chess sample, followed by island then continuous. This may be due to the binding nature of the segments

Bagg, Stacey D.↗

NASA Engineering and Safety Center Technical Bulletin No. 24-01: Material Compatibility of Common Aerospace Metals in MMH/MON-3

The NESC evaluated material compatibility of some common aerospace metals in monomethylhydrazine (MMH) and nitrogen tetroxide (MON-3). Previous work had identified a lack of quantitative compatibility data for nickel alloy 718, 300 series stainless steel, and titanium Ti-6Al-4V in MMH and MON-3 to support the use of zero-failure-tolerant, thin-walled pressure barriers in these propellants. Static (i.e., not flowing) general corrosion and electrochemistry testing was conducted, evaluating varied processing forms and heat treatment of the metals, water content of propellant, and exposure duration. Corrosion-rate data for all tested product forms, fluids, and durations were on the order of 1 x 10 –6 inch per year rather than the previously documented “less than 1 x 10 –3 inch per year”. The majority of the corrosion products were seen in the first 20 days of exposure, with an overall corrosion rate decreasing with time due to the increased divisor (time). It is therefore recommended that corrosion testing be performed at multiple short-term durations to inform the need for longer-duration testing.

Heather K Hickman↗

Fabrication and Performance of NiCuCoFeMn High Entropy Alloy Nanopastes for Brazing Inconel 718

Overview: High entropy alloys (HEAs) are a class of metallic alloys consisting of 5 plus elemental components and have four core effects - 1. High mixing entropy - 2. Sluggish diffusion kinetics - 3. High lattice distortion - 4. Cocktail effect; Boron-free, silicon-free brazing materials for nickel superalloys to avoid brittle intermetallic and eutectic phase formation; Size-dependent melting point depression can eliminate the need for boron, silicon and other melting point depressants; A Ni-Mn-Fe-Co-Cu HEA with low solidus and liquidus temperatures (1080 °C and 1150 °C) was developed; Low solidus and liquidus temperatures of the HEA combined with the nanoscale melting point depression in this study; Bulk HEA fabricated by induction melting of elemental powders; HEA nanoparticles (NPs) fabricated by ball milling of the HEA micropowder; Inconel 718 was laser brazed in air using the HEA and bulk and NP performances are compared.

Bridges, Denzel↗

Fabrication of Turbine Disk Materials by Additive Manufacturing

Precipitation-strengthened, nickel-based superalloys are widely used in the aerospace and energy industries due to their excellent environmental resistance and outstanding mechanical properties under extreme conditions. Powder-bed additive manufacturing (AM) technologies offer the potential to revolutionize the processing of superalloy turbine components by eliminating the need for extensive inventory or expensive legacy tooling. Like selective laser melting (SLM), electron beam melting (EBM) constructs three-dimensional dense components layer-by-layer by melting and solidification of atomized, pre-alloyed powder feedstock within 50-200 micron layers. While SLM has been more widely used for AM of nickel alloys like 718, EBM offers several distinct advantages, such as less retained residual stress, lower risk of contamination, and faster build rates with multiple-electron-beam configurations. These advantages are particularly attractive for turbine disks, for which excessive residual stress and contamination can shorten disk life during high-temperature operation. In this presentation, we will discuss the feasibility of fabricating disk superalloy components using EBM AM. Originally developed using powder metallurgy forging processing, disk superalloys contain a higher refractory content and precipitate volume fraction than alloy 718, thus making them more prone to thermal cracking during AM. This and other challenges to produce homogeneous builds with desired properties will be presented. In particular, the quality of lab-scale samples fabricated via a design of experiments, in which the beam current, build temperature, and beam velocity were varied, will be summarized. The relationship between processing parameters, microstructure, grain orientation, and mechanical response will be discussed.

oxidation↗

Long-Term Creep of a Thin-Walled Inconel 718 Stirling Power-Convertor Heater Head Assessed

The Department of Energy and NASA have identified Stirling power convertors as candidate power supply systems for long-duration, deep-space science missions. A key element for qualifying the flight hardware is a long-term durability assessment for critical hot section components of the power convertor. One such critical component is the power convertor heater head. The heater head is a high-temperature pressure vessel that transfers heat to the working gas medium of the convertor, which is typically helium. An efficient heater head design is the result of balancing the divergent requirements of thin walls for increased heat transfer versus thick walls to lower the wall stresses and thus improve creep resistance and durability. In the current design, the heater head is fabricated from the Ni-base superalloy Inconel 718 (IN 718, Inco Alloys International, Inc., Huntington, WV). Although IN 718 is a mature alloy system (patented in 1962), there is little long-term (>50,000-hr) creep data available for thin-specimen geometries. Since thin-section properties tend to be inferior to thicker samples, it is necessary to generate creep data using specimens with the same geometry as the actual flight hardware. Therefore, one facet of the overall durability assessment program involves generating relatively short-term creep data using thin specimens at the design temperature of 649 C (1200 F).

Bowman, Randy R.↗

Evaluation of candidate stirling engine heater tube alloys at 820 deg and 860 deg C

Seven commercial alloys were evaluated in Stirling simulator materials rigs. Five iron base alloys (N-155, A-286, Incoloy 800, 19-9DL, and 316 stainless steel), one nickel base alloy (Inconel 718), and one cobalt base alloy (HS-188) were tested in the form of thin wall tubing in a diesel fuel fired test rig. Tubes filled with hydrogen or helium at gas pressure of 21.6 MPa and temperatures of 820 and 860 C were endurance tested for 1000 and 535 hours, respectively. Results showed that under these conditions hydrogen permeated rapidly through the tube walls, thus requiring refilling during each five hour cycle. Helium was readily contained, exhibiting no measurable loss by permeation. Helium filled tubes tested at 860 C all exhibited creep-rupture failures within the 535 hour endurance test. Subsequent tensile test evaluation after removal from the rig indicated reduced room temperature ductility for some hydrogen-filled tubes compared to helium-filled tubes, suggesting possible hydrogen embrittlement in these alloys.

Misencik, J. A.↗

Measurement of Damping of Composite Materials for Turbomachinery Applications

The scientific community has felt that ceramic matrix composite (CMC) materials possess more material damping than the superalloys used in the production of rocket engine turbomachinery turbine-end components. The purpose of this NASA/MFSC study is to quantify the damping in CMC's as compared to a typical super-alloy, Inconel 718. It was observed through testing of beam coupons and disk specimens that the CMC's do indeed possess more material damping than the baselined alloy Inconel 718.

Harris, D. L.↗

Mechanical properties of Inconel 718 and Nickel 201 alloys after thermal histories simulating brazing and high temperature service

An experimental investigation was made to evaluate two nickel base alloys (Nickel-201 and Inconel-718) in three heat treated conditions. These conditions were: (1) annealed; (2) after thermal exposure simulating a braze cycle; and (3) after a thermal exposure simulating a braze cycle plus one operational lifetime of high temperature service. For the Nickel-201, two different braze cycle temperatures were evaluated. A braze cycle utilizing a lower braze temperature resulted in less grain growth for Nickel-201 than the standard braze cycle used for joining Nickel-201 to Inconel-718. It was determined, however, that Nickel-201, was marginal for temperatures investigated due to large grain growth. After the thermal exposures described above, the mechanical properties of Nickel-201 were degraded, whereas similar exposure on Inconel-718 actually strengthened the material compared with the annealed condition. The investigation included tensile tests at both room temperature and elevated temperatures, stress-rupture tests, and metallographic examination.

James, W. F.↗

Near-Threshold Fatigue Crack Growth Behavior of Fine-Grain Nickel-Based Alloys

Constant-Kmax fatigue crack growth tests were performed on two finegrain nickel-base alloys Inconel 718 (DA) and Ren 95 to determine if these alloys exhibit near-threshold time-dependent crack growth behavior observed for fine-grain aluminum alloys in room-temperature laboratory air. Test results showed that increases in K(sub max) values resulted in increased crack growth rates, but no evidence of time-dependent crack growth was observed for either nickel-base alloy at room temperature.

Newman, John A.↗

Material variability as measured by low temperature electrical resistivity.

Low temperature electrical resistivity was used to determine the material variability (1) between different manufacturers, (2) between different heats from the same manufacturer, and (3) within a given heat for Al 2024, Al-5% Mg alloys, Inconel 718, A286 stainless, and AISI 316. Generally, the coefficient of variation for solution annealed alloys ranged from 1.2 to 14% between manufacturers, 0.8 to 5.1% between heats, and 0.1 to 1.6% within a heat with stainless steels at the low ends and Al 2024 at the high ends. The variability is increased if the material is in a precipitation-hardened condition. A statistical analysis suggests that the variability within a heat is non-normal.

Clark, A. F.↗

Embrittlement of nickel-, cobalt-, and iron-base superalloys by exposure to hydrogen

Five nickel-base alloys (Inconel 718, Udimet 700, Rene 41, Hastelloy X, and TD-NiCr), one cobalt-base alloy (L-605), and an iron-base alloy (A-286) were exposed in hydrogen at 0.1 MN/sq m (15 psi) at several temperatures in the range from 430 to 980 C for as long as 1000 hours. These alloys were embrittled to varying degrees by such exposures in hydrogen. Embrittlement was found to be: (1) sensitive to strain rate, (2) reversible, (3) caused by large concentrations of absorbed hydrogen, and (4) not associated with any detectable microstructural changes in the alloys. These observations are consistent with a mechanism of internal reversible hydrogen embrittlement.

Gray, H. R.↗

Initial Mechanical Testing of Superalloy Lattice Block Structures Conducted

The first mechanical tests of superalloy lattice block structures produced promising results for this exciting new lightweight material system. The testing was performed in-house at NASA Glenn Research Center's Structural Benchmark Test Facility, where small subelement-sized compression and beam specimens were loaded to observe elastic and plastic behavior, component strength levels, and fatigue resistance for hundreds of thousands of load cycles. Current lattice block construction produces a flat panel composed of thin ligaments arranged in a three-dimensional triangulated trusslike structure. Investment casting of lattice block panels has been developed and greatly expands opportunities for using this unique architecture in today's high-performance structures. In addition, advances made in NASA's Ultra-Efficient Engine Technology Program have extended the lattice block concept to superalloy materials. After a series of casting iterations, the nickel-based superalloy Inconel 718 (IN 718, Inco Alloys International, Inc., Huntington, WV) was successfully cast into lattice block panels; this combination offers light weight combined with high strength, high stiffness, and elevated-temperature durability. For tests to evaluate casting quality and configuration merit, small structural compression and bend test specimens were machined from the 5- by 12- by 0.5-in. panels. Linear elastic finite element analyses were completed for several specimen layouts to predict material stresses and deflections under proposed test conditions. The structural specimens were then subjected to room-temperature static and cyclic loads in Glenn's Life Prediction Branch's material test machine. Surprisingly, the test results exceeded analytical predictions: plastic strains greater than 5 percent were obtained, and fatigue lives did not depreciate relative to the base material. These assets were due to the formation of plastic hinges and the redundancies inherent in lattice block construction, which were not considered in the simplified computer models. The fatigue testing proved the value of redundancies since specimen strength was maintained even after the fracture of one or two ligaments. This ongoing test program is planned to continue through high-temperature testing. Also scheduled for testing are IN 718 lattice block panels with integral face sheets, as well as specimens cast from a higher temperature alloy. The initial testing suggests the value of this technology for large panels under low and moderate pressure loadings and for high-risk, damage-tolerant structures. Potential aeropropulsion uses for lattice blocks include turbine-engine actuated panels, exhaust nozzle flaps, and side panel structures.

Krause, David L.↗

Diffusion bonding of IN 718 to VM 350 grade maraging steel

Diffusion bonding studies have been conducted on IN 718, VM 350 and the dissimilar alloy couple, IN 718 to maraging steel. The experimental processing parameters critical to obtaining consistently good diffusion bonds between IN 718 and VM 350 were determined. Interrelationships between temperature, pressure and surface preparation were explored for short bending intervals under vacuum conditions. Successful joining was achieved for a range of bonding cycle temperatures, pressures and surface preparations. The strength of the weaker parent material was used as a criterion for a successful tensile test of the heat treated bond. Studies of VM-350/VM-350 couples in the as-bonded condition showed a greater yielding and failure outside the bond region.

Crosby, S. R.↗

Ammonia-compatible elastomers and alloys

Study examines and reports positive findings from suitability tests of metal alloys, Inconel 718 and Ti-6A1-4V and elastomers, Ethylene propylene terpolymer rubbers, for utilization in storage vessels, fluid lines, and other system components subjected to continuous immersion in liquid anhydrous ammonia.

Bantrell, M. T.↗

Brazed Borsic/aluminum structural panels

A fluxless brazing process has been developed that minimizes degradation of the mechanical properties of Borsic/aluminum composites. The process, which employs 718 aluminum alloy braze, is being used to fabricate full scale Borsic/aluminum-titanium honeycomb-core panels for Mach 3 flight testing on the YF-12 aircraft and ground testing in support of the Supersonic Cruise Aircraft Research (SCAR) Program. The manufacturing development and results of shear tests on full scale panels are presented.

Bales, T. T.↗

Microstructure And Weld Cracking In Inconel 718(R)

Theories on relationship between metallurgy and microfissuring confirmed. Report describes research on effects of microstructure on cracking of heat-affected zones of welds in Inconel 718(R) alloy. In experimental studies, specimens subjected to various combinations of time-varying thermal and mechanical stresses to simulate welding conditions and to identify physical and chemical effects causing microfissuring.

Thompson, R. G.↗

Galvanic Corrosion In (Graphite/Epoxy)/Alloy Couples

Effects of galvanic coupling between graphite/epoxy composite material, G/E, and D6AC steel, 6061-T6 aluminum, and Inconel(R) 718 nickel alloy in salt water described in report. Introductory section summarizes previous corrosion studies of G/E with other alloys. Details of sample preparation presented along with photographs of samples before and after immersion.

Danford, Merlin D.↗