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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4
All sourcesNASA NTRSDOE OSTI
NASA NTRS1972

Experimental and theoretical aerodynamic heating and flow field analysis of a space shuttle orbiter

The results of work on the McDonnell Douglas delta wing orbiter are summarized and compared to other data and theories where applicable. The tests were conducted in the continuous hypersonic Tunnel B at Mach 8 and in the hypervelocity hotshot Tunnel F at Mach 10.5. Photographic data are used to illustrate the regions of peak heating on the lee-side and to show the vortical nature of the flow. Windward centerline data include measurements of shock angle, surface pressure, flow field pitot pressure and total temperature, and heat transfer rate coefficient distributions. Shock angles, surface pressures, and local Mach number distributions are compared with tangent cone theory over an angle of attack range from 10 to 60 deg. The measured heat transfer rate coefficient distributions are compared to both laminar and turbulent theories and boundary layer transition data are compared to the McDonnell Douglas criteria.

Matthews, R. K.↗
NASA NTRS1996

High Reynolds number analysis of flat plate and separated afterbody flow using non-linear turbulence models

The ability of the three-dimensional Navier-Stokes method, PAB3D, to simulate the effect of Reynolds number variation using non-linear explicit algebraic Reynolds stress turbulence modeling was assessed. Subsonic flat plate boundary-layer flow parameters such as normalized velocity distributions, local and average skin friction, and shape factor were compared with DNS calculations and classical theory at various local Reynolds numbers up to 180 million. Additionally, surface pressure coefficient distributions and integrated drag predictions on an axisymmetric nozzle afterbody were compared with experimental data from 10 to 130 million Reynolds number. The high Reynolds data was obtained from the NASA Langley 0.3m Transonic Cryogenic Tunnel. There was generally good agreement of surface static pressure coefficients between the CFD and measurement. The change in pressure coefficient distributions with varying Reynolds number was similar to the experimental data trends, though slightly over-predicting the effect. The computational sensitivity of viscous modeling and turbulence modeling are shown. Integrated afterbody pressure drag was typically slightly lower than the experimental data. The change in afterbody pressure drag with Reynolds number was small both experimentally and computationally, even though the shape of the distribution was somewhat modified with Reynolds number.

Carlson, John R.↗
NASA NTRS1982

The partitioning of Zr and Nb between diopside and melts in the system diopside-albite-anorthite

The crystal/liquid distribution coefficient for Zr between diopside and melt is measured for six compositions and three temperatures in the diopside field of Di-Ab-An, and the distribution coefficient for Nb is measured for three of these compositions. Nb is found to be excluded from diopside, while D(Zr), which is defined as wt % ZrO2 in crystals/wt % ZrO2 in melt, is variable and ranging from 0.05 to 0.45. D(Zr) is positively correlated with the Al content of both the melt and the pyroxene, and is negatively correlated with temperature. Both D(Zr) and D(Nb) are independent of oxygen fugacity, which implies that neither Zr nor Nb suffer valence changes over a range of oxygen fugacities spanning lunar and terrestrial conditions.

Dunn, T.↗
NASA NTRS1979

Solubility of noble gases in serpentine - Implications for meteoritic noble gas abundances

An investigation of the solubilities of the noble gases from synthesis and solubility studies of the sheet silicate mineral serpentine in carbonaceous chondrites is presented. Hydrothermal synthesis and exchange experiments were made at 340C and 1 kbar with noble gas partial pressures from 2 times 10 to the -8th power to 0.1 atm. The measured distribution coefficients for noble gases are not sufficiently high to account for the trapped noble gases in carbonaceous chondrites by exchange in solar nebula if meteoritic minerals have comparable distribution coefficients. Also, serpentine gains and loses noble gases to approach equilibrium values with the terrestrial atmosphere, indicating that this exposure may have influenced the noble gas abundances in phyllosilicate minerals of these chondrites. The dispersion of K-Ar ages of carbonaceous chondrites could be the result of phyllosilicates approaching equilibrium solubility of atmospheric Ar-40.

Zaikowski, A.↗
NASA NTRS1986

Comparison of experimental surface pressures with theoretical predictions on twin two-dimensional convergent-divergent nozzles

A three-dimensional subsonic aerodynamic panel code (VSAERO) was used to predict the effects of upper and lower external nozzle flap geometry on the external afterbody/nozzle pressure coefficient distributions and external nozzle drag of nonaxisymmetric convergent-divergent exhaust nozzles having parallel external sidewalls installed on a generic twin-engine high performance aircraft model. Nozzle static pressure coefficient distributions along the upper and lower surfaces near the model centerline and near the outer edges (corner) of the two surfaces were calculated, and nozzle drag was predicted using these surface pressure distributions. A comparison between the theoretical predictions and experimental wind tunnel data is made to evaluate the utility of the code in calculating the flow about these types of non-axisymmetric afterbody configurations. For free-stream Mach numbers of 0.60 and 0.90, the conditions where the flows were attached on the boattails yielded the best comparison between the theoretical predictions and the experimental data. For the Boattail terminal angles of greater than 15 deg., the experimental data for M = 0.60 and 0.90 indicated areas of separated flow, so the theoretical predictions failed to match the experimental data. Even though calculations of regions of separated flows are within the capabilities of the theoretical method, acceptable solutions were not obtained.

Carlson, J. R.↗
DOE OSTI2019

Magnesian calcite solid solution thermodynamics inferred from authigenic deep-sea carbonate

Magnesian calcite is perhaps the most well studied solid solution in the geosciences due to the widespread use of marine carbonates to reconstruct paleoenvironment. Despite decades of research, the low temperature thermodynamic properties of magnesian calcite in seawater are poorly constrained, largely because very slow reaction kinetics prevent the direct measurement of equilibrium distribution coefficients ($K_d^{Mg}$) for anhydrous Mg-bearing minerals. In this study, we use the Mg content of authigenic calcite formed in deep-sea marine carbonate sediments to determine the dependence of $K_d^{Mg}$ on temperature and aqueous Mg/Ca between ~2 and 25 °C. We find that the solid activity coefficient of magnesite in Mg-calcite is strongly temperature dependent in this range, leading to predicted exsolution of Mg at low temperatures. At the temperatures typical of ocean bottom water, equilibrium Mg distribution coefficients are at least an order of magnitude lower than values inferred from inorganic calcite growth experiments. Moreover, the equilibrium temperature dependence of $K_d^{Mg}$ agrees well with field-based paleotemperature calibrations determined for low-Mg benthic and planktonic foraminifera at temperatures <20 °C. Partitioning of Mg in foraminiferal tests is expected to be highly dependent on the Mg/Ca ratio in the calcifying fluid, so ignoring secular variations in seawater Mg/Ca can lead to significant underestimation of paleotemperatures.

58 GEOSCIENCES↗
NASA NTRS1996

High Reynolds number analysis of an axisymmetric afterbody with flow separation

The ability of a three-dimensional Navier-Stokes method, PAB3D, to predict nozzle afterbody flow at high Reynolds number was assessed. Predicted surface pressure coefficient distributions and integrated afterbody drag are compared with experimental data obtained from the NASA-Langley 0.3 m Transonic Cryogenic Tunnel. Predicted afterbody surface pressures matched experimental data fairly closely. The change in the pressure coefficient distribution with Reynolds number was slightly over-predicted. Integrated afterbody drag was typically high compared to the experimental data. The change in afterbody pressure drag with Reynolds number was fairly small. The predicted point of flow separation on the nozzle was slightly downstream of that observed from oilflow data at low Reynolds numbers and had a very slight Reynolds number dependence, moving slightly further downstream as Reynolds number increased.

Carlson, John R.↗
NASA NTRS1986

Experiments on supersonic turbulent flow development in a square duct

The nature of supersonic, turbulent, adiabatic-wall flow in a square duct is investigated experimentally over a development length of x/D between 0 and 20 for a uniform flow, Mach 3.9 condition at the duct inlet. Initial discussion centers on the duct configuration itself, which was designed specifically to minimize wave effects and nozzle-induced distortion in the flow. Total pressure contours and local skin friction coefficient distributions are presented which show that the flow develops in a manner similar to that observed for the incompressible case. In particular, undulations exist in total pressure contours within the cross plane and in transverse skin friction coefficient distributions, which are indicative of the presence of a well-defined secondary flow superimposed upon the primary flow. The results are analyzed to show that local law-of-the-wall behavior extends well into the corner region, which implies that wall functions conventionally applied in two-equation type turbulence models, when suitably defined for compressible flow, may also be applied to supersonic streamwise corner flows.

Gessner, F. B.↗
NASA NTRS1985

Characteristics of heat exchange in the region of injection into a supersonic high-temperature flow

An experimental investigation of the local heat transfer coefficient distribution during gas injection into the supersonic-flow portion of a Laval nozzle is discussed. The controlling dimensionless parameters of the investigated process are presented in terms of a generalized relation for the maximum value of the heat transfer coefficient in the nozzle cross section behind the injection hole. Data on the heat transfer coefficient variation along the nozzle length as a function of gas injection rate are also presented, along with the heat transfer coefficient distribution over a cross section of the nozzle.

Bakirov, F. G.↗
NASA NTRS1978

Partitioning of transition metals between diopside and coexisting silicate liquids. I - Nickel, cobalt, and manganese

Distribution coefficients have been found for the partitioning of Ni, Co, and Mn between calcium-rich clinopyroxenes and coexisting silicate liquids. Values are found for the 1110-1360 C temperature range. The breakdown of Henry's Law was not observed. The measured clinopyroxene/liquid distribution coefficients ranged from 1.5-14.0 for Ni, 0.5-2.0 for Co, and 0.3-1.2 for Mn. Analyses of pyroxenes grown from charges differing in the amounts of transition metals indicate that Ni and Co occupy the M1 site of diopside and that Mn occupies the M1 and M2 sites. Equilibrium constants were found in terms of the activities of the components in the liquid and solid phases. These activities are based on the mole fractions. An activity/concentration model was used for the liquid phase in order to explain the variations in the clinopyroxene/liquid coefficients due to bulk composition.

Lindstrom, D. J.↗
NASA NTRS1999

Trapped Melt in IIIAB Irons: Solid/Liquid Elemental Partitioning During the Fractionation of the IIIAB Magma

Group IIIAB, the largest iron-meteorite group, shows compositional trends (including a three-order-of-magnitude It concentration range) indicating that it formed by fractional crystallization of a metallic magma. Because about 200 irons are available, and all degrees of crystallization are well represented, IIIAB offers an excellent set of samples for the study of crystallization at all depths of the asteroidal core. On log-log Ir-Au, and Ir-As diagrams IIIAB forms a broad band; the breadth represents real meteorite-to-meteorite variations, far outside experimental or sampling uncertainties. A successful model must explain the width of this band; I suggest that it mainly resulted from the trapping of parental magma within the crystallizing solid. Because S is essentially insoluble in metal, the abundance of FeS is a measure of the fraction of trapped liquid. The trapped-melt model is supported by the observation that irons having higher S contents plot closer to the inferred composition of the magmatic parental liquid. The lowest S values are found in the irons occupying the left envelope of the IIIAB Ir-Au or Ir-As compositional fields, thus it is this set of irons that should be interpreted as the solid products of a fractionating magma. This simplifies the modeling of the crystallization process and allows inferences regarding the distribution ratios for other elements in the evolved IIIAB system. The large (multiton) Cape York irons show wide variations in their trapped-melt fractions; their compositions seem best understood in terms of a low initial S content of the IIIAB magma, about 20 mg/g. The inferred initial IIIAB distribution coefficient for Ir, 4.6, is much higher than published values based on laboratory studies of low-S systems; I suggest that low-S (and low-P) partition-ratio measurements tend to err in the direction of unity. In IIIAB distribution coefficients for Au, As, and Ni were still < 1 when the most evolved IIIAB irons formed, another indication of a low initial S content.

Wasson, John T.↗
DOE OSTI2018

Precious Metal Distributions in Direct Nickel Matte Smelting with Low-Cu Mattes

Base metal (Cu, Fe, and Ni) and trace element (Ag, Au, Co, Pd, and Pt) distributions between low-iron nickel mattes with [Ni]:[Cu] = 4 (w/w) have been studied at 1623 K to 1723 K (1350 °C to 1450 °C). We equilibrated small slag–matte samples with CO–CO{sub 2}–SO{sub 2}–Ar atmospheres in pre-selected P{sub S{sub 2}}–P{sub O{sub 2}} points, maintaining silica saturation by fused silica crucibles. The slags studied contained about 0 to 8.5 wt pct MgO. The matte–slag distribution coefficients L{sup m/s}[Me] were obtained from assays by electron probe X-ray microanalysis for the matte and by laser ablation-ICP-mass spectrometry for the slag. The measured L{sup m/s}[Me] values were clearly dependent on iron concentration of the matte and on MgO concentration of the slag, with values on the order of 10{sup 4}, 10{sup 5}, and 10{sup 4} for gold, platinum, and palladium, respectively, in the 5 wt pct iron in matte experiments. The obtained data for silver were scattered, due to volatilization, resulting in depletion of most silver and its escape from matte to gas phase during the 3-hour equilibration period. The matte-to-slag distribution coefficient for silver was estimated to be L{sup m/s}[Ag] = 100 to 400. We also measured the distributions of the base metals Cu and Ni in the same conditions as the trace elements.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Radionuclide Risk Coefficient Uncertainty Distributions for Use in Performance Assessments - 19156

Traditionally, radiation dose has been used as the regulatory criterion for decision making in performance assessments (PAs), despite the concept of cancer risk arguably being a more easily understood endpoint than dose for the public, and a preferable metric for decision analysis. However, the United States Environmental Protection Agency (EPA) has developed risk parameters for use in risk assessments and PAs in the form of radionuclide-specific risk coefficients, or RCs, which are published in various Federal Guidance Reports (FGRs). RCs are employed as scalars to convert environmental radionuclide exposure (via ingestion, inhalation, and external exposure) estimates to incremental lifetime cancer risk (ILCR). ILCR is the additional cancer risk averaged over a lifetime, over-and-above all-cause cancer risk, associated with carcinogen exposure. Uncertainties associated with RCs are discussed in FGR 13 and in a joint report published by EPA and Oak Ridge National Laboratory, but statistical distributions for the RCs were not directly developed. The uncertainty assessments in the EPA/ONRL report were based on dosimetric modeling and elicitation of nine experts. From these sources, five uncertainty categories were defined based on ratios of the 5. and 95. quantiles of uncertainty. Thus, the representations of uncertainty defined by EPA/ORNL are not distributions in a traditional sense. Furthermore, the authors only addressed uncertainty in RCs for inhalation and ingestion pathways. We develop a methodology for assigning statistical distributions to EPA's published mortality RC values (i.e. to estimate the probability of dying from radiation-induced cancers) for the inhalation (slow, medium, and fast absorption types), ingestion (water, food, and soil), and external exposure pathways associated with all cancer types. We employed the same dosimetric concepts and assumptions as EPA/ORNL, including cancer risk (dose-response) distributional information from a previous expert elicitation, which was also employed by EPA/ORNL in their work. We assumed that uncertainty in RCs can be described by lognormal distributions based on the modeling conducted previously by EPA/ORNL, and that point estimates tabulated in FGR 13 represent median values of the distributions. We also extended EPA/ORNL's uncertainty ratios to statistical distributions for external exposure RCs. The results are a set of radionuclide-specific distributions that are applicable in PAs that focus on cancer mortality. These distributions are currently and will subsequently be employed in PAs at various sites, in addition to the required regulatory dose limits. Quantification of ILCRs and associated uncertainty in PAs will provide regulators and the public with additional information for good decision making. Future directions include further refinement of the distributions and development of statistical distributions for morbidity RCs, which are used to estimate the probability of developing, but not necessarily dying as a result of, radiation-induced cancer. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2023

Aerodynamic Rotor Design for a 25 MW Offshore Downwind Turbine

Continuously increasing offshore wind turbine scales require rotor designs that maximize power and performance. Downwind rotors offer advantages in lower mass due to reduced potential for tower strike, and is especially true at large scales, e.g., for a 25 MW turbine. In this study, three 25 MW downwind rotors, each with different prescribed lift coefficient distributions were designed (chord, geometry, and twist) and compared to maximize power production at unprecedented scales and Reynolds numbers, including a new approach to optimize rotor tilt and coning based on aeroelastic effects. To achieve this objective the design process was focused on achieving high power coefficients, while maximizing swept area and minimizing blade mass. Maximizing swept area was achieved by prescribing pre-cone and shaft tilt angles to ensure the aeroelastic orientation when the blades point upwards was nearly vertical at nearly rated conditions. Maximizing the power coefficient was achieved by prescribing axial induction factor and lift coefficient distributions which were then used as inputs for an inverse rotor design tool. The resulting rotors were then simulated to compare performance and subsequently optimized for minimum rotor mass. To achieve these goals, a high Reynolds number design space was developed using computational predictions as well as new empirical correlations for flatback airfoil drag and maximum lift. Within this design space, three rotors of small, medium and large chords were considered for clean airfoil conditions (effects of premature transition were also considered but did not significantly modify the design space). The results indicated that the medium chord design provided the best performance, producing the highest power in Region 2 from simulations while resulting in the lowest rotor mass, both of which support minimum LCOE. The methodology developed herein can be used for the design of other extreme-scale (upwind and downwind) turbines.

downwind rotors↗
DOE OSTI2022

Experimental calibration of an Fe3+/Fe2+-in-amphibole oxybarometer and its application to shallow magmatic processes at Shiveluch Volcano, Kamchatka

Abstract Oxygen fugacity is an important but difficult parameter to constrain for primitive arc magmas. In this study, the partitioning behavior of Fe3+/Fe2+ between amphibole and glass synthesized in piston-cylinder and cold-seal apparatus experiments is developed as an oxybarometer, applicable to magmas ranging from basaltic to dacitic composition. The partitioning of Fe2+ is strongly dependent on melt polymerization; the relative compatibility of Fe2+ in amphibole decreases with increasing polymerization. The Fe2+/Mg distribution coefficient between amphibole and melt is a relatively constant value across all compositions and is, on average, 0.27. The amphibole oxybarometer is applied to amphibole in mafic enclaves, cumulates, and basaltic tephra erupted from Shiveluch volcano in Kamchatka with measured Fe3+/FeTotal. An average Fe3+/Fe2+ amphibole-glass distribution coefficient for basalt is used to convert the Fe3+/FeTotal of amphibole in samples from Shiveluch to magmatic oxygen fugacity relative to NNO. The fO2 of primitive melts at the volcano is approximately NNO+2 and is faithfully recorded in amphibole from an amphibole-rich cumulate and the basaltic tephra. Apparently, higher fO2 recorded by amphibole in mafic enclaves likely results from partial dehydrogenation of amphibole during residence in a shallow andesite storage region. We identify three pulses of mafic magma recharge within two weeks of, a month before, and two to three months before the eruption and find that, at each of these times, the host andesite was recharged by at least two magmas at varying stages of differentiation. Application of the amphibole oxybarometer not only gives insight into magmatic fO2 but also potentially details of shallow magmatic processes.

Geochemistry & Geophysics↗
NASA NTRS1982

The effects of C, P, and S on trace element partitioning during solidification in Fe-Ni alloys

Trace and minor element distributions in the iron meteorites are generally ascribed to partitioning during solidification of the parent body core or to partial melting within the parent body. A model involving fractional crystallization is considered. The model cannot account for differences between the measured values for the slopes on the log Ir-log Ni plots and the slopes predicted using experimentally determined distribution coefficients obtained in an investigation conducted by Goldstein and Friel (1978). The model has also other weaknesses. Part of the answer concerning the existing problems was provided by Narayan and Goldstein (1981, 1982). The present investigation is concerned with a further clarification of the effect of the minor elements P, S, and C on the distribution behavior of trace elements. Attention is given to measurements of the distribution coefficients for various elements (Ir, Ge, Ga, Au, Cu, Cr) in the presence of these minor elements.

Willis, J.↗
DOE OSTI2022

Studies toward the Use of Ionic Liquids and Supercritical CO 2 for the Recovery and Separation of Praseodymium from Waste Streams

Waste streams from the incineration of metal-containing materials like such as computer processor boards and batteries may contain critical rare earth elements like praseodymium. Data on the solubility of Pr compounds and on their distribution coefficients in supercritical CO 2 /ionic liquid two-phase systems are important to determine if an ionic liquid/supercritical CO 2 two-phase approach is feasible toward the recovery of a particular metal. This work provides data on the solubility of various praseodymium compounds in butyl-methyl-pyrrolidinium bis(trifluoromethylsulfonyl)imide (BMPyTf2N) ionic liquid and on the distribution coefficients of these praseodymium compounds in the supercritical CO 2 phase of the two-phase BMPyTf2N ionic liquid/supercritical CO 2 system, with and without a tributyl phosphate additive.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2019

Cesium Ion Exchange Testing Using a Three-Column System with Crystalline Silicotitanate and Hanford Tank Waste 241-AP-107

Washington River Protection Solutions (WRPS) is working to support early production of immobilized low-activity waste by feeding Hanford tank supernate from tank farms to the Hanford Waste Treatment and Immobilization Plant (WTP) Low-Activity Waste (LAW) facility. This goal incorporates the design of a Tank-Side Cesium Removal (TSCR) system, which in effect filters tank waste supernate and processes it through a cesium ion exchange medium to remove 137Cs. The 137Cs-depleted product is sent to the WTP for vitrification. Rovira et al. (2018) reported the successful Cs removal from Hanford tank 241-AP-107 waste (hereafter called AP-107) using crystalline silicotitanate (CST) ion exchange media manufactured by Honeywell UOP, LLC (product IONSIVTM R9140-B, Batch 2081000057) in a lead-lag column system. Since that testing, WRPS has changed the column design to a three-column system. WRPS requested a repeated study with AP-107 tank waste using a different batch of IONSIVTM R9140-B, Lot 2002009604, in a three-column format. A small-scale test platform was constructed to demonstrate solids filtration, Cs removal, and LAW vitrification and installed at Pacific Northwest National Laboratory. This report describes the small-scale ion exchange testing system component of the test platform and the processing of approximately 8.55 L of filtered AP-107 supernate using CST, Lot 8056262-999, that passed through a 25-mesh filter. This report also describes the Cs ion exchange batch contact testing to determine the Cs distribution coefficient and the maximum Cs loading capacity in the AP-107 tank waste matrix. Batch contact testing helps to evaluate CST performance on tank waste supernate and is often used prior to processing tank waste through ion exchange columns to assess some performance metrics (e.g., 50% Cs breakthrough). Batch contact tests were performed with the filtered AP-107 tank waste at four Cs concentrations at a phase ratio of 200 (liquid volume to exchanger mass). The distribution coefficient (K d ) at the equilibrium condition of 9.2 µg Cs/mL (AP-107 feed condition) was determined to be 806 mL AP 107/g CST. With a CST bed density of 1.01 g/mL (<25 mesh CST), this K d corresponded to a predicted 50% Cs breakthrough of 814 bed volumes (BVs). The Cs load capacity at the equilibrium feed condition was determined to be 8.3 mg Cs/g dry CST. The three-column format testing was prototypic to the intended TSCR operations, albeit on a small scale with 10-mL CST beds. Flowrate was adjusted to match the CST contact time expected for the full-scale operation, i.e., matched bed volumes per hour (BV/h) flow rate. The feed was processed downflow through the lead column, then through the middle column, and then through the polish column. Loading continued at an average of 1.88 BV/h (1.83 to 2.04 BV/h range) until the entire available AP-107 feed was processed. The Cs-decontaminated product will be provided for vitrification testing. The lead column only reached 45% Cs breakthrough after processing 855 BVs of feed. The 50% Cs breakthrough was extrapolated to occur at ~900 BVs. This extrapolated 50% Cs breakthrough value differed from the batch contact estimate (814 BVs) by 13%. The waste acceptance criteria (WAC) or contract limit for the WTP LAW vitrification facility is 3.18E-5 Ci 137 Cs per mole Na. For the AP-107 tank waste, only 0.127% of the influent 137 Cs concentration may be delivered to the WTP; this required a Cs decontamination factor of 787. The Cs effluent from the middle column reached the WAC after processing 590 BVs. Cs breakthrough from the polish column began at 590 BVs, reaching 6.3E-3 µCi/mL or 4.3E-3% Cs breakthrough after processing 844 BVs of feed.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗