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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4
All sourcesNASA NTRSDOE OSTI
NASA NTRS2015

Laser Surface Preparation of Epoxy Composites for Secondary Bonding: Optimization of Ablation Depth

Surface preparation has been identified as one of the most critical aspects of attaining predictable and reliable adhesive bonds. Energetic processes such as laser ablation or plasma treatment are amenable to automation and are easily monitored and adjusted for controlled surface preparation. A laser ablation process was developed to accurately remove a targeted depth of resin, approximately 0.1 to 20 micrometers, from a carbon fiber reinforced epoxy composite surface while simultaneously changing surface chemistry and creating micro-roughness. This work demonstrates the application of this process to prepare composite surfaces for bonding without exposing or damaging fibers on the surface. Composite panels were prepared in an autoclave and had a resin layer approximately 10 micrometers thick above the fiber reinforcement. These composite panels were laser surface treated using several conditions, fabricated into bonded panels and hygrothermally aged. Bond performance of aged, experimental specimens was compared with grit blast surface treated specimens using a modified double cantilever beam test that enabled accelerated saturation of the specimen with water. Comparison of bonded specimens will be used to determine how ablation depth may affect average fracture energies and failure modes.

Palmieri, Frank L.↗
NASA NTRS2017

A Review of the Proposed K (sub Isi) Offset-Secant Method for Size-Independent Linear-Elastic Toughness Evaluation

The proposed size-independent linear-elastic fracture toughness, K (sub Isi), for potential inclusion in ASTM E399 targets a consistent 0.5 millimeters crack extension for all specimen sizes through an offset secant that is a function of the specimen ligament length. The K (sub Isi) method also includes an increase in allowable deformation, and the removal of the P (sub max)/P (sub Q) criterion. A finite element study of the K (sub Isi) test method confirms the viability of the increased deformation limit, but has also revealed a few areas of concern. Findings: 1. The deformation limit, b (sub o) greater than or equal to 1.1 times (K (sub I) divided by delta (sub ys) squared) maintains a K-dominant crack tip field with limited plastic contribution to the fracture energy; 2. The three dimensional effects on compliance and the shape of the force versus CMOD (Crack-Mouth Opening Displacement) trace are significant compared to a plane strain assumption; 3. The non-linearity in the force versus CMOD trace at deformations higher than the current limit of 2.5 times (K (sub I) divided by delta (sub ys) squared) is sufficient to introduce error or even "false calls" regarding crack extension when using a constant offset secant line. This issue is more significant for specimens with W (width) greater than or equal to 2 inches; 4. A non-linear plasticity correction factor in the offset secant may improve the viability of the method at deformations between 2.5 times (K (sub I) divided by delta (sub ys) squared) and 1.1 times (K (sub I) divided by delta (sub ys) squared).

James, Mark↗
NASA NTRS2019

Thermally-Induced Healing of Electrically-Insulating Ethylene-Octene Copolymers

We report on electrical insulating materials that not only have sufficient mechanical toughness to survive use conditions, but also possess the ability to undergo thermally induced self-repair when damaged. By controlling the cross-link density, a modified ethylene-octene copolymer (EOC) is able to retain its self-healing abilities while also being used at temperatures greater than the original, unmodified polymer. Specifically, an EOC cross-linked with 0.25 wt% dicumyl peroxide affords a material ability to recover 61% of its critical fracture energy — a value similar to thermoplastic EOC. Furthermore, as shown by dielectric spectroscopy, the cross-linked EOC retains good electrically-insulating properties.

Self-healing↗
NASA NTRS1975

Analysis of liquid metal embrittlement from a bond energy viewpoint

Absorption induced embrittlement of solid metals by certain liquid metals is analyzed through an Engel-Brewer calculation of the solid-liquid interaction energy, and of the effect of the latter in reducing fracture surface energy. The reduction in fracture surface energy is estimated by comparison of the electronic contribution to the solid-liquid interaction energy with solid-solid bond energy for some 40 liquid-solid couples. Regular solution theory is used to estimate mutual solubility as the relative difference in parameter values. Embrittlement can be predicted by using reduction in fracture surface energy and solubility parameter difference as critical variables. The effect of solute additions to the liquid on the degree of embrittlement is interpreted via the same two variables; the principal effect of solutes is to modify solubility relationships at the solid-liquid interface.

Kelley, M. J.↗
NASA NTRS1975

Fracture angle and strain-energy-density-factor of a crack at hole at an arbitrary angle

For both the maximum stress criterion and strain-energy-density-factor (S) theory, fracture angle (the initial angle of crack growth) is predicted by using opening and sliding mode stress intensity factors. These theoretical predictions are consistent with experimental fracture angles. For the S theory, the crack spreads in the direction of the negative fracture angle in a plane for which S is a minimum. This quantity was obtained analytically. The experimental data of the critical S on plexiglass fracture specimens remains essentially constant.

Hsu, Y. C.↗
NASA NTRS1974

The peel test in experimental adhesive fracture mechanics

Several testing methods have been proposed for obtaining critical energy release rate or adhesive fracture energy in bond systems. These tests include blister, cone, lap shear, and peel tests. Peel tests have been used for many years to compare relative strengths of different adhesives, different surface preparation techniques, etc. The present work demonstrates the potential use of the peel test for obtaining adhesive fracture energy values.

Anderson, G. P.↗
NASA NTRS2004

Tensile Creep Fracture of Polycrystalline Near-Stoichiometric NiAl

Tensile creep fracture behavior of polycrystalline near-stoichiometric NiAl has been studied between 700 and 1200 K under initial applied stresses varying between 10 and 200 MPa. The stress exponent for fracture varied between 5.0 and 10.7 while the activation energy for fracture was 250 +/- 22 kJ/mol. The fracture life was inversely proportional to the secondary creep rate in accordance with the Monkman-Grant relation although there was extensive scatter in the data. This observation suggests that the fracture life for near-stoichiometric NiAl was influenced by creep under these stress and temperature conditions. Several different fracture morphologies were observed. Transgranular ductile cleavage fracture occurs at 700 K and at the higher stresses at 800 K. The fracture mode transitions to transgranular creep fracture at 900 and 1000 K and at lower stresses at 800 K, while plastic rupture and grain boundary cavitation occur at 1100 and 1200 K. An experimental fracture mechanism map is constructed for near-stoichiometric NiAl.

Raj, Sai V.↗
NASA NTRS1989

A simplified approach to strain energy release rate computations for interlaminar fracture of composites

A simple approach for the strain energy release rate computations based on the finite element method and a singular fitting model is presented. The model uses the stress and displacement distributions at the delamination front. The method is applied to a mixed-mode double cracked-lap-shear composite configuration. The strain energy release rate components predicted by the model are compared with the finite element crack-closure method. The effect of the mesh size on the stress and displacement distribution is isolated. The strain energy release rates predicted by relatively coarse mesh sizes are in good agreement with the finite element crack closure method.

Armanios, Erian A.↗
NASA NTRS1973

Growth characteristics of a plane crack subjected to three-dimensional loading

The closed form expressions for the stress intensity factors due to concentrated forces applied to the surfaces of a half plane crack in an infinite body are used to generate solutions for distributed loads in this geometry. The stress intensity factors for uniformly distributed loads applied over a rectangular portion of the crack surface are given in closed form. An example of non-uniformly distributed loads which can be treated numerically is also included. In particular, combinations of normal and shear stresses on the crack which simulate the case of loading at an angle to the crack front are considered. The resulting stress intensity factors are combined with the strain energy density fracture criterion for the purpose of predicting the most likely direction of crack propagation. The critical value of the energy density factor can then be used for determining the allowable load on a specimen with a crack front not perpendicular to the tensile axis.

Hartranft, R. J.↗
NASA NTRS2000

Ultrasonic Assessment of Impact-Induced Damage and Microcracking in Polymer Matrix Composites

The main objective of this NASA FAR project is to conduct ultrasonic assessment of impact-induced damage and microcracking in polymer matrix composites at various temperatures. It is believed that the proposed study of impact damage assessment on polymer matrix composites will benefit several NASA's missions and current interests, such as ballistic impact testing of composite fan containment and high strain rate deformation modeling of polymer matrix composites. Currently, impact-induced delamination and fracture in 6061-T6 aluminum/cast acrylic sandwich plates adhered by epoxy were generated in an instrumented drop-weight impact machine. Although only a small dent was produced on the aluminum side when a hemispherical penetrator tup was dropped onto it from a couple of inches, a large ring of delamination at the interface was observed. The delamination damage was often accompanied by severe shattering in the acrylic substratum. Damage patterns in the acrylic layer include radial and ring cracks and, together with delamination at the interface, may cause peeling-off of acrylic material from the sandwich plate. Theory of stress-wave propagation can be used to explain these damage patterns. The impact tests were conducted at various temperatures. The results also show clearly that temperature effect is very important in impact damage. For pure cast acrylic nil-ductile transition (NDT) occurs between 185-195 F Excessive impact energy was dissipated into fracture energy when tested at temperature below this range or through plastic deformation when tested at temperature above the NDT temperature. Results from this study will be used as baseline data for studying fiber-metal laminates, such as GLARE and ARALL for advanced aeronautical and astronautical applications.

Liaw, Benjamin↗
NASA NTRS2000

Impact Delamination and Fracture in Aluminum/Acrylic Sandwich Plates

Impact-induced delamination and fracture in 6061-T6 aluminum/cast acrylic sandwich plates adhered by epoxy were generated in an instrumented drop-weight impact machine. Although only a small dent was produced on the aluminum side when a hemispherical penetrator tup was dropped onto it from a couple of inches, a large ring of delamination at the interface was observed. The delamination damage was often accompanied by severe shattering in the acrylic substratum. Damage patterns in the acrylic layer include radial and ring cracks and, together with delamination at the interface, may cause peeling-off of acrylic material from the sandwich plate. Theory of stress-wave propagation can be used to explain these damage patterns. The impact tests were conducted at various temperatures. The results also show clearly that temperature effect is very important in impact damage. For pure cast acrylic nil-ductile transition (NDT) occurs between 185-195 F. Excessive impact energy was dissipated into fracture energy when tested at temperature below this range or through plastic deformation when tested at temperature above the NDT temperature. Results from this study will be used as baseline data for studying fiber-metal laminates, such as GLARE and ARALL for advanced aeronautical and astronautical applications.

Liaw, Benjamin↗
NASA NTRS1974

Three-dimensional growth characteristics of a plane crack subjected to concentrated forces

A combination of longitudinal shear and normal forces acting on a half-plane crack is shown to lead to predictions of crack growth qualitatively similar to those obtained by Knauss (1970) for crack propagation in antiplane shear. The presented results, based on the strain-energy-density fracture criterion, predict the direction of growth and the load which initiates it.

Hartranft, R. J.↗
NASA NTRS1977

Weldability of high toughness Fe-12% Ni alloys containing Ti, Al or Nb

Three exceptionally high-toughness Fe-12%Ni alloys designed for cryogenic service were welded using the GTA welding process. Evaluation of weldability included equivalent energy (KIed) fracture toughness tests, transverse-weld tensile tests at -196 and 25 C and weld crack sensitivity tests. The Fe-12%Ni-0.25%Ti alloy proved extremely weldable for cryogenic applications, having weld and HAZ properties comparable with those of the wrought base alloy. The Fe-12%Ni-0.5%Al had good weld properties only after the weld joint was heat treated. The Fe-12%Ni-0.25%Nb alloy was not considered weldable for cryogenic use because of its poor weld joint properties at -196 C and its susceptibility to hot cracking.

Devletian, J. H.↗
NASA NTRS1983

Strength and fracture toughness of reaction-bonded Si3N4

Fracture strength and fracture toughness measurements were made on reaction-bonded Si3N4 materials with a range of alpha/beta ratios. The results do not indicate any clear relation between the modulus of rupture and the alpha/beta ratio over the range 1.5-9. Values for the modulus of rupture range from 219 to 290 MN per sq m, with an overall average of 238 MN per sq m. The notched beam fracture toughness is found to be constant over the range of microstructures produced, indicating that of the various microstructural features (e.g., alpha/beta ratio and pore size and distribution) no single element has a controlling influence over fracture toughness and the fracture surface energy.

Danforth, S. C.↗
NASA NTRS1991

Reliability analysis of structural ceramics subjected to biaxial flexure

The reliability of alumina disks subjected to biaxial flexure is predicted on the basis of statistical fracture theory using a critical strain energy release rate fracture criterion. Results on a sintered silicon nitride are consistent with reliability predictions based on pore-initiated penny-shaped cracks with preferred orientation normal to the maximum principal stress. Assumptions with regard to flaw types and their orientations in each ceramic can be justified by fractography. It is shown that there are no universal guidelines for selecting fracture criteria or assuming flaw orientations in reliability analyses.

Chao, Luen-Yuan↗
NASA NTRS1992

Prediction of thermal cycling induced matrix cracking

Thermal fatigue has been observed to cause matrix cracking in laminated composite materials. A method is presented to predict transverse matrix cracks in composite laminates subjected to cyclic thermal load. Shear lag stress approximations and a simple energy-based fracture criteria are used to predict crack densities as a function of temperature. Prediction of crack densities as a function of thermal cycling is accomplished by assuming that fatigue degrades the material's inherent resistance to cracking. The method is implemented as a computer program. A simple experiment provides data on progressive cracking of a laminate with decreasing temperature. Existing data on thermal fatigue is also used. Correlations of the analytical predictions to the data are very good. A parametric study using the analytical method is presented which provides insight into material behavior under cyclical thermal loads.

Mcmanus, Hugh L.↗