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NASA NTRS1989

Fracture toughness of SiC/Al metal matrix composite

An experimental study was conducted to evaluate fracture toughness of SiC/Al metal matrix composite (MMC). The material was a 12.7 mm thick extrusion of 6061-T6 aluminum alloy with 40 v/o SiC particulates. Specimen configuration and test procedure conformed to ASTM E399 Standard for compact specimens. It was found that special procedures were necessary to obtain fatigue cracks of controlled lengths in the preparation of precracked specimens for the MMC material. Fatigue loading with both minimum and maximum loads in compression was used to start the precrack. The initial precracking would stop by self-arrest. Afterwards, the precrack could be safely extended to the desired length by additional cyclic tensile loading. Test results met practically all the E399 criteria for the calculation of plane strain fracture toughness of the material. A valid K sub IC value of the SiC/Al composite was established as K sub IC = 8.9 MPa square root of m. The threshold stress intensity under which crack would cease to grow in the material was estimated as delta K sub th = 2MPa square root of m for R = 0.09 using the fatigue precracking data. Fractographic examinations show that failure occurred by the micromechanism involved with plastic deformation although the specimens broke by brittle fracture. The effect of precracking by cyclic loading in compression on fracture toughness is included in the discussion.

Flom, Yury↗

NASA NTRS1989

Fracture toughness of SiC/Al metal matrix composite

Flom, Yury↗

NASA NTRS1979

Comparison tests and experimental compliance calibration of the proposed standard round compact plane strain fracture toughness specimen

Standard round specimen fracture test results compared satisfactorily with results from standard rectangular compact specimens machined from the same material. The location of the loading pin holes was found to provide adequate strength in the load bearing region for plane strain fracture toughness testing. Excellent agreement was found between the stress intensity coefficient values obtained from compliance measurements and the analytic solution proposed for inclusion in the standard test method. Load displacement measurements were made using long armed displacement gages and hollow loading cylinders. Gage points registered on the loading hole surfaces through small holes in the walls of the loading cylinders.

Fisher, D. M.↗

DOE OSTI2022

Fracture toughness of schist, amphibolite, and rhyolite from the Sanford Underground Research Facility (SURF), Lead, South Dakota

The Cracked Chevron Notched Brazilian Disc (CCNBD) method was selected for Mode I fracture toughness tests on Poorman schist, Yates amphibolite, and rhyolite dikes from the EGS Collab site at the SURF in Lead, South Dakota. The effects of lithology, anisotropy, and loading rate were investigated. Fracture toughness was greatest in amphibolite, with schist and rhyolite having similar toughness values ($K$ amphibolite > $K$ rhyolite ≈ $K$ schist ). The effects of anisotropy on fracture toughness were investigated in the foliated schist samples. Schist samples were prepared in three geometries (divider, arrester, and short transverse) which controlled how the fracture would propagate relative to foliations. The divider geometry was strongest and short transverse geometry was the weakest ($K$ divider > $K$ arrester > $K$ shorttransverse ). Fracture toughness was observed to decrease with decreasing loading rate. Optical and SEM microscopy revealed that for the short transverse geometry, fractures tended to propagate along grain boundaries, whereas in arrester and divider geometries fractures tended to propagate through grains. In foliated samples, the tortuosity of the fracture observed in thin section was greater in arrester and divider geometries than in short transverse geometries.

58 GEOSCIENCES↗

NASA NTRS1989

Fracture toughness of polycrystalline ceramics in combined mode I and mode II loading

The present investigation of the fracture of alumina and zirconia polycrystalline ceramic specimens of precracked-disk type, in diametral compression, evaluated fracture toughness in pure mode I, combined mode I/mode II, and pure mode II, depending on the alignment of the center crack relative to the loading diameter. The mixed-mode fracture-toughness envelope thus obtained exhibits significant deviation to higher fracture toughness in mode II, relative to the predictions of linear elastic fracture mechanics theory. Crack-surface resistance due to grain-interlocking and abrasion are identified as the primary sources of increased fracture resistance in mode II loading of the polycrystalline ceramics.

Singh, Dileep↗

NASA NTRS1975

The feasibility of ranking material fracture toughness by ultrasonic attenuation measurements

A preliminary study was conducted to assess the feasibility of ultrasonically ranking material fracture toughness. Specimens of two grades of maraging steel for which fracture toughness values were measured were subjected to ultrasonic probing. The slope of the attenuation coefficient versus frequency curve was empirically correlated with the plane strain fracture toughness value for each grade of steel.

Vary, A.↗

NASA NTRS1975

The feasibility of ranking material fracture toughness by ultrasonic attenuation measurements

A preliminary study was conducted to assess the feasibility of ultrasonically ranking material fracture toughness. Specimens of two grades of maraging steel for which fracture toughness values were measured were subjected to ultrasonic probing. The slope of the attenuation coefficient vs frequency curve was empirically correlated with the plane strain fracture toughness value for each grade of steel.

Vary, A.↗

DOE OSTI2020

Tritium Aging Effects on Fracture Toughness of Stainless Steel Weldments

The long-term embrittlement effects of tritium and decay helium on the structural properties of stainless steels have been studied for years at Savannah River to provide required data for establishing safe operating conditions and lifetimes of pressure vessels used to contain tritium gas. In this study, the fracture toughness properties of the longest-aged tritium-precharged stainless-steel base metals and weldments tested at Savannah River were measured and compared to earlier results. The fracture toughness values were the lowest recorded here for tritium-exposed stainless steel. As-forged and as-welded specimens were thermally precharging with tritium gas at 34.5 MPa and 623 K, then aged for up to 17 years to buildin decay helium prior to testing. ASTM J-Integral fracture mechanics analyses, transmission electron microscopy (TEM), and small angle neutron scattering (SANS) examinations were conducted to characterize the effects of tritium and its radioactive decay product, helium-3. Results show that the fracture toughness values were reduced to less than 2-4% of the as-forged values for specimens with more than 1300 appm helium from tritium decay. The trend of decreasing fracture toughness values with increasing helium content was consistent with earlier observations, and the data show that Type 304L stainless steel is more resistant to tritium-induced cracking than Type 21-6-9 stainless at similar decay helium levels. The fracture toughness properties of long-aged weldments were also affected, but the reductions were not as severe over time because weldments did not retain as much tritium as did the base metals. TEM observations were used to characterize the effects of decay helium bubbles on the deformation substructures, but nanometer-sized helium bubbles were not easily resolved because of high dislocation densities within the forged microstructures. SANS results are presented that suggest the technique can provide information on decay helium bubble size, spacing, and distribution in these steels.

36 MATERIALS SCIENCE↗

NASA NTRS2002

Strength and Fracture Toughness of Solid Oxide Fuel Cell Electrolyte Material Improved

Solid oxide fuel cells (SOFC) are being developed for various applications in the automobile, power-generation, and aeronautics industries. Recently, the NASA Glenn Research Center has been exploring the possibility of using SOFC's for aeropropulsion under its Zero Carbon Dioxide Emission Technology (ZCET) Program. 10-mol% yttriastabilized zirconia (10YSZ) is a very good anionic conductor at high temperatures and is, therefore, used as an oxygen solid electrolyte in SOFC. However, it has a high thermal expansion coefficient, low thermal shock resistance, low fracture toughness, and poor mechanical strength. For aeronautic applications, the thin ceramic electrolyte membrane of the SOFC needs to be strong and tough. Therefore, we have been investigating the possibility of enhancing the strength and fracture toughness of the 10YSZ electrolyte without degrading its electrical conductivity to an appreciable extent. We recently demonstrated that the addition of alumina to zirconia electrolyte increases its strength as well as its fracture toughness. Zirconia-alumina composites containing 0 to 30 mol% of alumina were fabricated by hot pressing. The hot pressing procedure was developed and various hot pressing parameters were optimized, resulting in dense, crackfree panels of composite materials. Cubic zirconia and a-alumina were the only phases detected, indicating that there was no chemical reaction between the constituents during hot pressing at elevated temperatures. Flexure strength sf and fracture toughness K(sub IC) of the various zirconia-alumina composites were measured at room temperature as well as at 1000 C in air. Both properties showed systematic improvement with increased alumina addition at room temperature and at 1000 C. Use of these modified electrolytes with improved strength and fracture toughness should prolong the life and enhance the performance of SOFC in aeronautics and other applications.

Bansal, Narottam P.↗

NASA NTRS1993

Effect of environment on fracture toughness of 96 wt pct alumina

An effort is made to deepen understanding of environmental effects on the fracture toughness of an alumina composition that contains a residual glassy phase, by ascertaining the fracture toughness under atmospheric conditions in such varied environments as air distilled water, silicone oil, and liquid nitrogen. Fracture toughness was determined via the single-edge-precracked beam technique. Weibull strength parameters are compared for polished specimens tested both in air and silicone environments.

Choi, Sung R.↗

NASA NTRS1993

Evaluation of the Fracture Toughness of Nb-40Al-8Cr-1W-1Y-0.05B Intermetallic Material by Indentation Techniques

The fracture toughness of an Nb-40Al-8Cr - 1W-1Y-0.05B intermetallic material was evaluated by indentation techniques at room temperature. Two widely used indentation methods, crack size measurement and indent strength, yielded excellent agreement with a conventional fracture toughness technique using straight-through precracked specimens, despite the occasional formation of poorly configured cracks. However, the modified indentation technique, using dummy indent flaws, resulted in a low fracture toughness compared to that evaluated by the other methods. The material did not exhibit rising R-curve behavior, as evaluated from the indentation strength data. These results indicate that indentation fracture principles are applicable to this brittle intermetallic material without modification of the residual contact stress term originally calibrated for ceramic materials.

Choi, S. R.↗

NASA NTRSDate not supplied

Computational Assessment of the Opening Mode Facesheet-to-Core Fracture Toughness of a Thin-Gage Facesheet Sandwich Structure

The single-cantilevered beam test (SCB) is currently being considered for standardization for measuring the opening mode fracture toughness of sandwich structures subjected to facesheet-to-core separation. At present, the Area method is considered the benchmark method for determining energy required to propagate the crack. This method is problematic since it requires periodic unloading and cannot be evaluated instantaneously. Therefore, a method is needed to accurately and instantaneously calculate opening mode fracture toughness. In previous work, SCB tests with thin-gauge facesheets were performed to compare the J-integral approach to data reduction methods including the Modified Beam Theory (MBT) and the Area method. Large deviations (over 10%) in the calculated fracture toughness were observed between the J-integral and MBT for large displacements. In this study, a simulated SCB experiment using a virtual crackclosure technique was performed to assess the previously observed discrepancies. The predicted load displacement response, the predicted angle at the load application point, and the predicted crack growth results are in good agreement (within 5%) with the corresponding experimental data. Using the predicted load and angles, the predicted J-integral is in good agreement (within 10%) with the experimentally obtained solution. Using the MBT approach, the previously observed deviations in the fracture toughness were determined to be associated with the empirical extrapolation procedure to estimate the crack-root rotation correction from nonlinear compliance curves. The nonlinear compliance is determined to be associated with large displacement effects observed within the predicted and experimental results.

Sandwich Composite↗

NASA NTRS1995

Effects of stitching on fracture toughness of uniweave textile graphite/epoxy laminates

The effects of through-the-thickness stitching on impact damage resistance, impact damage tolerance, and Mode 1 and Mode 2 fracture toughness of textile graphite/epoxy laminates were studied experimentally. Graphite/epoxy laminates were fabricated from AS4 graphite uniweave textiles and 3501-6 epoxy using Resin Transfer Molding. The cloths were stitched with Kevlar(tm) and glass yarns before resin infusion. Delamination was implanted during processing to simulate impact damage. Sublaminate buckling tests were performed in a novel fixture to measure Compression After Impact (CAI) strength of stitched laminates. The results show that CAI strength can be improved up to 400% by through-the-thickness stitching. Double Cantilever Beam tests were performed to study the effect of stitching on Mode 1 fracture toughness G(sub 1c). It was found that G(sub 1c) increased 30 times for a low stitching density of 16 stitches/sq in. Mode 2 fracture toughness was measured by testing the stitched beams in End Notch Flexure tests. Unlike in the unstitiched beams, crack propagation in the stitched beams was steady. The current formulas for ENF tests were not found suitable for determining G(sub 2C) for stitched beams. Hence two new methods were developed - one based on crack area measured from ultrasonic C-scanning and the other based on equivalent crack area measured from the residual stiffness of the specimen. The G(sub 2c) was found to be at least 5-15 times higher for the stitched laminates. The mechanisms by which stitching increases the CAI strength and fracture toughness are discussed.

Sankar, Bhavani V.↗

NASA NTRS1982

Interrelation of material microstructure, ultrasonic factors, and fracture toughness of two phase titanium alloy

The pivotal role of an alpha-beta phase microstructure in governing fracture toughness in a titanium alloy, Ti-662, is demonstrated. The interrelation of microstructure and fracture toughness is demonstrated using ultrasonic measurement techniques originally developed for nondestructive evaluation and material property characterization. It is shown that the findings determined from ultrasonic measurements agree with conclusions based on metallurgical, metallographic, and fractographic observations concerning the importance of alpha-beta morphology in controlling fracture toughness in two phase titanium alloys.

Vary, A.↗

DOE OSTI2021

High temperature fracture toughness of single-layer CrAlN and CrAlSiN hard coatings

Hardness and toughness are among of the most important physical properties of hard coatings and it is important to analyze them at temperatures present during coating applications. CrAlN and CrAlSiN are hard coating materials frequently used in high temperature applications. Here, while both possess high oxidation resistance and thermal stability, they differ in their microstructure. In this work, the fracture toughness of magnetron-sputtered single-layer CrAlN and CrAlSiN hard coatings was determined up to 700 °C by in-situ scanning electron microscopy micro-cantilever deflection tests. The results show a decreasing trend of the fracture toughness with increasing temperature. While both coatings' fracture toughness trends are similar up to 400 °C, they diverge at higher temperatures. In general, the evolution of the fracture toughness with increasing temperature shows similarities to the observed changes in hardness in the same temperature range.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Grain Boundary and Lattice Fracture Toughness of UO 2 Measured Using Small-Scale Mechanics

Small-scale mechanical testing has been used to isolate the properties of individual grain boundaries and regions of the lattice in undoped UO 2 polycrystals. Notched microcantilever specimens were prepared by focused ion beam milling and tested in bending. Fracture toughness values were calculated from finite element analysis of the sample geometry at fracture load using the J-integral method. Lattice and grain boundary fracture toughness values of 1.17 ± 0.16 MPa m 1/2 and 1.08 ± 0.08 MPa m 1/2 , respectively, were obtained. The similarity between the lattice and grain boundary fracture toughness values is consistent with the preference for transgranular room-temperature fracture in UO 2 . The grain boundary and lattice fracture toughness values also agree well with the toughness of dense polycrystals, which suggests that microstructural-scale toughening mechanisms are limited in such samples.

36 MATERIALS SCIENCE↗

NASA NTRS1986

Concepts for interrelating ultrasnic attenuation, microstrucutre and fracture toughness in polycrystalline solids

Conceptual models are advanced for explaining and predicting empirical correlations found between ultrasonic measurements and fracture toughness of polycrystalline solids. The models lead to insights concerning microstructural factors governing fracture processes and associated stress wave interactions. Analysis of the empirical correlations suggested by the models indicate that, in addition to grain size and shape, grain boundary reflections, elastic anisotropy, and dislocation damping are factors that underly both fracture toughness and ultrasonic attenuation. One outcome is that ultrasonic attenuation can predict the size of crack blunting or process zones that develop in the vicinity active cracks in metals. This forms a basis for ultrasonic ranking according to variations in fracture toughness.

Vary, A.↗

NASA NTRS1988

Concepts for interrelating ultrasonic attenuation, microstructure, and fracture toughness in polycrystalline solids

Conceptual models are advanced for explaining and predicting empirical correlations found between ultrasonic measurements and fracture toughness of polycrystalline solids. The models lead to insights concerning microstructural factors governing fracture processes and associated stress wave interactions. Analysis of the empirical correlations suggested by the models indicate that, in addition to grain size and shape, grain boundary reflections, elastic anisotropy, and dislocation damping are factors that underlie both fracture toughness and ultrasonic attenuation. One outcome is that ultrasonic attenuation can predict the size of crack blunting or process zones that develop in the vicinity of active cracks in metals. This forms a basis for ultrasonic ranking according to variations in fracture toughness.

Vary, A.↗