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Differential thermal analysis of a lunar soil simulant, 'Minnesota Lunar Simulant-1' (MLS-1) was performed. The MLS-1 was tested in as-received form (in glass form) and with another silica. The silica addition was seen to depress nucleation events which lead to a better glass former.
Sieve fraction analyses of lunar soils reveal the presence of a fine-grained exotic component enriched in K, Rb, Sr, Ba, and in radiogenic Sr in all soils. The probable source of this exotic component is the areas of high-surficial radioactivity observed by orbital gamma ray spectrometry, such as those at Fra Mauro and Archimedes. If the exotic component is fine-grained KREEP, the origin and distribution of KREEP fragments in the soils are identified. It is suggested that the exotic component represents trace element enriched material located at some depth in the Imbrium area which was surficially deposited during Imbrium excavation.
Volatiles implanted into the lunar regolith by the solar wind are potentially important lunar resources. Wittenberg et al. (1986) have proposed that lunar He-3 could be used as a fuel for terrestrial nuclear fusion reactors. They argue that a fusion scheme involving D and He-3 would be cleaner and more efficient than currently-proposed schemes involving D and T. However, since the terrestrial inventory of He-3 is so small, they suggest that the lunar regolith, with concentrations of the order of parts per billion (by mass) would be an economical source of He-3. Solar-wind implantation is also the primary source of H, C, and N in lunar soil. These elements could also be important, particularly for life support and for propellant production. In a SERC study of the feasibility of obtaining the necessary amount of He-3, Swindle et al. (1990) concluded that the available amount is sufficient for early reactors, at least, but that the mining problems, while not necessarily insurmountable, are prodigious. The volatiles H, C, and N, on the other hand, come in parts per million level abundances. The differences in abundances mean that (1) a comparable amount of H, C, and/or N could be extracted with orders of magnitude smaller operations than required for He-3, and (2) if He-3 extraction ever becomes important, huge quantities of H, C, and N will be produced as by-products.
Recycled lunar soil grains are defined as those soil grains that have been a part of either regolith breccias or agglutinates; thus, mineral grains, rock fragments, older agglutinates, and volcanic glass spherules, if dislodged from an agglutinate or a regolith breccia, would all qualify as recycled grains. This paper shows that it is possible to estimate the proportion of recycled material in lunar soils. Optical data from 12 soils in the Apollo 16 core 64001/2 were collected to estimate the proportion (W) of recycled crystalline grains in each of these soils. The W values show a correspondence with other independently derived parameters and the history of the core soils, indicating that W can be used as a valid soil-evolution parameter.
A critical review of maturity with respect to the abundance of implanted solar wind elements (SWE) in lunar soils indicates: (1) that the Rosiwal Principle has limited applicability in determining implantation of SWE in lunar soils, and (2) that despite a depletion of SWE in agglutinitic glass, agglutinates are enriched in SWE due to the presence of buried surfaces of numerous clasts within agglutinates. A statistical analysis of published data of several Apollo 17 soils indicates that the abundance of carbon and, by analogy, the abundance of other SWE are correlatable with the agglutinate content and the mean grain size of lunar soils. Microscopic examination of more than 5000 grains of agglutinates in polished thin sections reveals a wide range of variability in the mineralogy, grain size distribution, degree of recycling, etc., of the clast population in agglutinates. This indicates that the volume-correlated SWE content of agglutinates may vary and need not be constant.
Two oedometer and three direct shear tests have been performed in vacuum on a 200 g sample of lunar soil from Apollo 12 (12001, 119). The compressibility data have been used to calculate bulk density and shear wave velocity versus depth on the lunar surface. The shear wave velocity was found to increase approximately with the one-fourth power of the depth, and the results suggest that the Apollo 14 Active Seismic Experiment may not have detected the Fra Mauro formation at a depth of 8.5 m, but only naturally consolidated lunar soil. The shear data indicate that the strength of the lunar soil sample is about 65% that of a ground basalt simulant at the same void ratio.
Agglutinitic glass contains much of the reduced Fe in lunar soils, and it contributes to the modification of reflectance spectra from lunar soils. Previous work has shown that agglutinitic glass can be compositionally heterogeneous, but the scale of these heterogeneities is not well known. In addition, few data are available on the characteristics of the inclusions in agglutinitic glass. Here we report on our preliminary transmission electron microscope (TEM) examination of agglutinitic glass fragments from the Apollo 11 soil 10084.
Space weathering effects on lunar soil grains result from both radiation-damaged and deposited layers on grain surfaces. Typically, solar wind irradiation forms an amorphous layer on regolith silicate grains, and induces the formation of surficial metallic Fe in Fe-bearing minerals [1,2]. Impacts into the lunar regolith generate high temperature melts and vapor. The vapor component is largely deposited on the surfaces of lunar soil grains [3] as is a fraction of the melt [4, this work]. Both the vapor-deposits and the deposited melt typically contain nanophase Fe metal particles (npFe0) as abundant inclusions. The development of these rims and the abundance of the npFe0 in lunar regolith, and thus the optical properties, vary with the soil mineralogy and the length of time the soil grains have been exposed to space weathering effects [5]. In this study, we used the density of solar flare particle tracks in soil grains to estimate exposure times for individual grains and then perform nanometer-scale characterization of the rims using transmission electron microscopy (TEM). The work involved study of lunar soil samples with different mineralogy (mare vs. highland) and different exposure times (mature vs. immature).
This paper describes the first phase of the long-term investigation for the construction of concrete lunar bases. In this phase, petrographic and scanning electron microscope examinations showed that the morphology and elemental composition of the lunar soil made it suitable for use as a fine aggregate for concrete. Based on this finding, calcium aluminate cement and distilled water were mixed with the lunar soil to fabricate test specimens. The test specimens consisted of a 1-in cube, a 1/2-in cube, and three 0.12 x 0.58 x 3.15-in beam specimens. Tests were performed on these specimens to determine compressive strength, modulus of rupture, modulus of elasticity, and thermal coefficient of expansion. Based on examination of the material and test results, it is concluded that lunar soil can be used as a fine aggregate for concrete.
An attempt is made to identify those K/Ar techniques which extract the most reliable chronological information from lunar soils and to define the situations in which the best data are obtainable. Results are presented for determinations of the exposure and K/Ar ages of five lunar soil samples, which were performed by applying correlation techniques for a two-component argon structure to stepwise-heated and neutron-irradiated aliquots of grain-sized separates. It is found that ages deduced from Ar-40/surface-correlated Ar-36 vs K-40/surface-correlated Ar-36 and analogous plots of data from grain-sized separates appear to be the best available K/Ar ages of submature to mature lunar soils, that ages deduced from Ar-40 vs Ar-36 and analogous plots which assume a uniform K content can be significantly in error, and that stepwise-heating (Ar-40)-(Ar-39) experiments yield useful information only for simple immature soils where the K-Ar systematics are dominated by a single component.
Current understanding of the chemistry and microstructure of the surfaces of lunar soil grains is dominated by a reference frame derived mainly from electron microscopy observations [e.g. 1,2]. These studies have shown that the outermost 10-100 nm of grain surfaces in mature lunar soil finest fractions have been modified by the combined effects of solar wind exposure, surface deposition of vapors and accretion of impact melt products [1,2]. These processes produce surface-correlated nanophase Feo, host grain amorphization, formation of surface patinas and other complex changes [1,2]. What is less well understood is how these changes are reflected directly at the surface, defined as the outermost 1-5 atomic monolayers, a region not easily chemically characterized by TEM. We are currently employing X-ray Photoelectron Spectroscopy (XPS) to study the surface chemistry of lunar soil samples that have been previously studied by TEM. This work includes modification of the grain surfaces by in situ irradiation with ions at solar wind energies to better understand how irradiated surfaces in lunar grains change their chemistry once exposed to ambient conditions on earth.
Lunar soil and rock program in support of lunar exploration
A method has been developed which will determine hydrogen in sub-milligram samples of lunar soil. It consists of heating the sample in a pyroprobe followed by the gas chromatographic determination of hydrogen using the helium ionization detector. Using a 7 foot, 1/8 OD stainless steel column packed with Carbosieve S, 120/140 mesh, hydrogen was well-separated from the other gases released from lunar soil. Standards of hydrogen in helium were used for calibration. The limit to detection under the conditions used was about 2 ng. The method was linear from 2 ng to 270 ng. The method was checked using some actual lunar samples. Results were typical of those obtained for lunar soils using other methods.
Tranquillity Base lunar soil origin, establishing component nature, size distribution, density, mineralogy, constructional or destructional history
Apollo 11 lunar soil sample derived from basaltic and anorthositic rocks, considering basalt origin by melting due to internal radioactive heating
Boulder tracks from 19 different locations on the Moon, observable in Lunar Orbiter photographs, have been examined. Measurements of the track width indicate that some of the boulders sank considerably deeper than others. It is suggested that lunar surface materials vary from place to place; the state of compaction (density of lunar soil) is probably one of the significant variables. Using bearing capacity theory, modified to be applicable to the rolling boulder problem by theoretical studies and extensive testing, the friction angle of the lunar soil was estimated. Most of the results were between 24 and 47 degrees with an arithmetic average of 37 degrees.
Direct extraction and reaction of the 50 ppm H found in mature lunar soil with a small fraction of the 1 percent ilmenite found in even the most Ti-poor lunar soils is a viable method of producing H2O2 and H2O for propellants and life support. A plant with a mass of approximately 62 metric tons can produce about 8 metric tons of LOX and 1.2 metric tons of LH2 per month. The concept is viable in even Ti-poor regions if the soils have long exposure to solar wind. The plant processes over 29,000 tons of soil with about 50 ppm H per month. The mine that feeds the plant excavates over 8600 sq m per month with a fleet of three front-end loaders and five haulers. Trade studies demonstrate that nuclear power accompanied by a high process plant duty cycle results in a far smaller installation than a solar-powered unit.
Mechanical behavior of lunar fine soils in engineering gravity flow bins