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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4

Pulse height response of an optical particle counter to monodisperse aerosols

The pulse height response of a right angle scattering optical particle counter has been investigated using monodisperse aerosols of polystyrene latex spheres, di-octyl phthalate and methylene blue. The results confirm previous measurements for the variation of mean pulse height as a function of particle diameter and show good agreement with the relative response predicted by Mie scattering theory. Measured cumulative pulse height distributions were found to fit reasonably well to a log normal distribution with a minimum geometric standard deviation of about 1.4 for particle diameters greater than about 2 micrometers. The geometric standard deviation was found to increase significantly with decreasing particle diameter.

Wilmoth, R. G.↗

Electrophoresis experiment for space

The Apollo 16 electrophoresis experiment was analyzed, demonstrating that the separation of the two different-size monodisperse latexes did indeed take place, but that the separation was obscured by the pronounced electroosmotic flow of the liquid medium. The results of this experiment, however, were dramatic since it is impossible to carry out a similar separation on earth. It can be stated unequivocally from this experiment that any electrophoretic separation will be enhanced under microgravity conditions. The only question is the degree of this enhancement, which can be expected to vary from one experimental technique to another. The low-electroosmotic-mobility coating (Z6040-MC) developed under this program was found to be suitable for a free-fluid electrophoretic separation such as the experiment designed for the ASTP flight. The problem with this coating, however, is that its permanency is limited because of the slow desorption of the methylcellulose from the coated surface.

Vanderhoff, J. W.↗

Separation of granulocytes from whole blood by leukoadhesion, phase 1

Capillary glass tubes are investigated for the separation and retrieval of large quantities of viable granulocytes and monocytes from whole blood on a continuous basis from a single donor. This effort represented the feasibility demonstration of a three phase program for development of a capillary tube cell separation device. The activity included the analysis and parametric laboratory testing with subscale models required to design a prototype device. Capillary tubes 40 cm long with a nominal 0.030 cm internal diameter yielded the highest total process efficiency. Recovery efficiencies as high as 89% of the adhering cell population were obtained. Granulocyte phagocytosis of latex particles indicated approximately 90% viability. Monocytes recovered from the separation column retained their capability to stimulate human bone marrow colony growth, as demonstrated in an in vitro cell culture assay.

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Fluorescent microspheres

Latex particles with attached antibodies have potential biochemical and environmental applications. Human red blood cells and lymphocytes have been labeled with fluorescent microspheres by either direct or indirect immunological technique. Immunolatex spheres can also be used for detecting and localizing specific cell surface receptors. Hormones and toxins may also be bondable.

Rembaum, A.↗

New works in space

Goods and services that may be furnished by the Space Shuttle are described. A single multibeam antenna array capable of supplying satellite communication for 256 U.S. cities, a disaster warning network, and a TV link to remote areas is discussed. Attention is also given to such materials processing programs as crystal growth (for example, production of mercuric iodide crystals for gamma-ray detectors), eutectic growth of solid-solution crystals such as mercury-cadmium-telluride, manufacture of uniform latex spheres for medical applications, and development of small glass spheres for fusion power applications. In addition to the Space Telescope, a meter-class telescope on the Shuttle and a wide-field survey instrument are under study.

Kingsbury, J. E.↗

Sample stream distortion modeled in continuous-flow electrophoresis

Buoyancy-induced disturbances in an electrophoresis-type chamber were investigated. Five tracer streams (latex) were used to visualize the flows while a nine-thermistor array sensed the temperature field. The internal heating to the chamber was provided by a 400 Hz electrical field. Cooling to the chamber was provided on the front and back faces and, in addition, on both chamber side walls. Disturbances to the symmetric base flow in the chamber occurred in the broad plane of the chamber and resulted from the formation of lateral and axial temperature gradients. The effect of these gradients was to retard or increase local flow velocities at different positions in the chamber cross section, which resulted in lateral secondary flows being induced in the broad plane of the chamber. As the adverse temperature gradients increased in magnitude, the critical Rayleigh number was approached and reverse (separated) flow became apparent, which, subsequently, led to the onset of time variant secondary flows.

Rhodes, P. H.↗

Development of a special purpose spacecraft interior coating, phase 3

A variety of intumescent coatings based on a fluorocarbon latex resin modified with either an acrylic resin or an epoxy resin were prepared. Several intumescent systems were used for these studies including some based on ammonium polyphosphate and others based on sulfanilamide. The best coatings developed had a high concentration (60-70% by wt.) of intumescent additives and had to be applied thick, approximately 100 mils, in order to have adequate intumescent/fire protection properties.

Gillman, H. D.↗

Development of a special purpose spacecraft coating, phase 4

Coating formulations based on a fluorocarbon resin were evaluated for use on spacecraft exteriors. Formulations modified with an acrylic resin were found to have excellent offgassing properties. A much less expensive process for increasing to solid content of the fluorocarbon latex was developed.

Gillman, H. D.↗

A microprocessor-based one dimensional optical data processor for spatial frequency analysis

A high degree of accuracy was obtained in measuring the spatial frequency spectrum of known samples using an optical data processor based on a microprocessor, which reliably collected intensity versus angle data. Stray light control, system alignment, and angle measurement problems were addressed and solved. The capabilities of the instrument were extended by the addition of appropriate optics to allow the use of different wavelengths of laser radiation and by increasing the travel limits of the rotating arm to + or - 160 degrees. The acquisition, storage, and plotting of data by the computer permits the researcher a free hand in data manipulation such as subtracting background scattering from a diffraction pattern. Tests conducted to verify the operation of the processor using a 25 mm diameter pinhole, a 39.37 line pairs per mm series of multiple slits, and a microscope slide coated with 1.091 mm diameter polystyrene latex spheres are described.

Collier, R. L.↗

Studies with sample conductivity, insertion rates, and particle deflection in a continuous flow electrophoresis system

The continuous flow electrophoresis system makes electrophoresis possible in a free-flowing film of aqueous electrolyte medium. The sample continuously enters the electrolyte at the top of the chamber and is subjected to the action of a lateral dc field. This divides the sample into fractions since each component has a distinctive electrophoretic mobility. Tests were made using monodisperse polystyrene latex microspheres to determine optimum sample conductivity, insertion rates and optimum electric field applications as baseline data for future STS flight experiments. Optimum sample flow rates for the selected samples were determined to be approximately 26 micro-liters/min. Experiments with samples in deionized water yielded best results and voltages in the 20 V/cm to 30 V/cm range were optimum. Deflections of formaldehyde fixed turkey and bovine erythrocytes were determined using the continuous flow electrophoresis system. The effects of particle interactions on sample resolution and migration in the chamber was also evaluated.

Williams, G., Jr.↗

STS-6 sixth Space Shuttle mission. First flight of the Challenger

A prelaunch summary of the sixth Space Shuttle mission is provided. The Challenger orbiter; launching; uprated engines; lighter weight boosters; lightweight tank; external tank reduction; landing; the tracking and data relay satellite system (TDRSS), TDRS-1 deployment; the inertial upper stage (IUS), the spacewalk;electrophoresis, monodisperse latex reactor, night time/day time optical survey of lightning, and getaway special experiments are described.

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Convective and interfacial instabilities during solidification of succinonitrile containing ethanol

Even though slow convective flow is difficult to detect in solidifying metals, it can readily be observed in transparent materials by observing the motion of small neutrally buoyant particles. Succinonitrile, which solidifies with an unfaceted solid/liquid interface and has well characterized physical properties, is considered an excellent material for such studies. For studies of solute-induced convection, ethanol is a useful addition to succinonitrile since it has a lower density and a somewhat similar molecular structure. Samples of high purity and ethanol-doped succinonitrile are unidirectionally solidified in a vertical temperature gradient. Latex mimcrospheres 2 microns in diameter are suspended in the liquid to reveal the convective flow. Convective and morphological stability is observed as a function of solute concentration and growth velocity. These measurements are compared with theoretical calculations that predict the transition from stability to instability as a function of solidification conditions. The predicted transitions occur at low concentrations and solidification velocities; for this reason, extreme care must be taken in order to eliminate the effects of impurities or thermally induced convection.

Schaefer, R. J.↗

National Space Transportation Systems Program mission report

The 515-41B National Space Transportation Systems Program Mission Report contains a summary of the major activities and accomplishments of the sixth operational Shuttle flight and fourth flight of the OV-099 vehicle, Challenger. Since this flight was the first to land at Kennedy Space Center, the vehicle was towed directly to the OPF (Orbiter Processing Facility) where preparations for flight STS-41C, scheduled for early April 1984, began immediately. The significant problems that occurred during STS-41B are summarized and a problem tracking list that is a complete list of all problems that occurred during the flight is given. None of the problems will affect the STS 41C flight. The major objectives of flight STS-41B were to successfully deploy the Westar satellite and the Indonesian Communications Satellite-B2 (PALAPA-B2); to evaluate the MMU (Manned Maneuvering Unit) support for EVA (Extravehicular Activities); to exercise the MFR (Manipulator Foot Restraint); to demonstrate a closed loop rendezvous; and to operate the M.R (Monodisperse Latex Reactor), the ACES (Acoustic Containerless Experiment System) and the IEF (Isoelectric Focusing) in cabin experiments; and to obtain photographs with the Cinema 360 Cameras.

Collins, M. A., Jr.↗

Recommendations and calculations concerning physical characteristics of the EEVT apparatus

Several issues arose during the course of preparing for the flight of EEVT on STS-3. Documents concerning the issues are presented in the following order: (1) the possibility of mixing latex spheres with kidney cells as standard electrokinetic markers; (2) tube breakage and the potential for the development of leaks and bubbles; (3) effects of the shape of the sample gate on the electric field and the outward migration of cells; (4) suggestions for reducing electroosmosis by decreasing the diameter of the sample; and (5) predictions of the effects of modified sample dimensions on electroosmotic band spreading.

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Reflectivity of the atmosphere-inhomogeneous surfaces system Laboratory simulation

Theoretical two- and three-dimensional solutions of the radiative transfer equation have been applied to the earth-atmosphere system. Such solutions have not been verified experimentally. A laboratory experiment simulates such a system to test the theory. The atmosphere was simulated by latex spheres suspended in water and the ground by a nonuniform surface, half white and half black. A stable radiation source provided uniform illumination over the hydrosol. The upward radiance along a line orthogonal to the boundary of the two-halves field was recorded for different amounts of the hydrosol. The simulation is a well-defined radiative transfer experiment to test radiative transfer models involving nonuniform surfaces. Good agreement is obtained between the measured and theoretical results.

Mekler, Y.↗

Electrophoresis technology

A new high resolution apparatus designed for space was built as a laboratory prototype. Using a moving wall with a low zeta potential coating, the major sources of flow distortion for an electrophoretic sample stream are removed. Highly resolved fractions, however, will only be produced in space because of the sensitivity of this chamber to buoyancy-induced convection in the laboratory. The second and third flights of the McDonnell Douglas Astronautics Corporation continuous flow electrophoresis system carried samples developed at MSFC intended to evaluate the broad capabilities of free flow electrophoresis in a reduced gravity environment. Biological model materials, hemoglobin and polystyrene latex microspheres, were selected because of their past use as electrophoresis standards and as visible markers for fluid flow due to electroosmosis, spacecraft acceleration or other factors. The dependence of the separation resolution on the properties of the sample and its suspension solution was assessed.

Snyder, R. S.↗

Multiple scattering measurements in laboratory and foggy atmosphere

Multiple scattering affects propagation of light beams in turbid media. Backscattering or forward scattering based measurements of atmospheric parameters are influenced by this effect. Although largely studied theoretically, the effect needs measurements in control of situations due to the large variety of situations of practical importance. The results of laboratory measurements pertaining to the transmission of a collimated light beam (Helium-Neon souce, 10 mW) through suspensions of latex spheres in water are presented and a comparison was made with the predictions of calculation in a foggy atmosphere will also be presented.

Bruscaglioni, P.↗

Processing materials in space - The history and the future

The development of materials processing in space, and some of the Soyuz, Apollo, Skylab, and Shuttle orbital materials experiments are reviewed. Consideration is given to protein crystal growth, electrophoresis, low-gravity isoelectric focusing, phase partitioning, a monodisperse latex reactor, semiconductor crystal growth, solution crystal growth, the triglycine sulfate experiment, vapor crystal growth experiments, the mercuric iodide experiment, electronic and electrooptical materials, organic thin films and crystalline solids, deep undercooling of metals and alloys, magnetic materials, immiscible materials, metal solidification research, reluctant glass-forming materials, and containerless glass formation. The space processing apparatuses and ground facilities, for materials processing are described. Future facilities for commercial research, development, and manufacturing in space are proposed.

Chassay, Roger↗