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At least 73 records · Page 4

Ultrasonic and mechanical characterizations of fatigue states of graphite epoxy composite laminates

Eight-ply (0, + or - 45, 0)s laminates of Hercules AS/3501-6 graphite epoxy composite are fabricated using various cure pressures ranging from 0.52 to 0.86 MPa and cure temperatures ranging from 150 C to 200 C. In general, the minimum composite void volume fraction is obtained at a cure temperature of 175 C and a cure pressure of 0.86 MPa, or at 200 C and 0.86 MPa. The ultrasonic attenuation at 4 MHz was found to correlate with the composite void volume fraction. Composite specimens were tested in flexural fatigue. Beyond 10,000 fatigue cycles, the ultrasonic attenuation at 4 MHz was found to increase and the flexural stiffness was found to decrease. The ultrasonic attenuation at 4 MHz of the as-fabricated composite can be correlated with the number of fatigue cycles to failure.

Williams, J. H., Jr.↗

Ultrasonic and mechanical characterizations of fatigue states of graphite epoxy composite laminates

Results of an exploration of the relationship between ultrasonic attenuation and fatigue survivability of graphite fiber epoxy composites fabricated under different cure conditions are reported. A total of 9 27 x 40 cm eight-ply graphite epoxy laminated specimens were formed, and fatigue tests were run on five partial samples at 73.5 N varying at 30 Hz, with tests ending at a 1.27 cm deflection. A pulsed oscillator generated sinusoidal waves and transducers recorded the passage of the ultrasonic waves for display on oscilloscopes. Cure pressures ranged from 0.52-0.85 MPa and cure temperatures were in the 150-200 C interval. Ultrasonic through-transmission at 4 MHz was performed prior to and during fatigue testing. The minimum void volume fraction occurred at 175 C and 0.86 MPa. The flexural stiffness decreased with the number of fatigue cycles past 10,000, when the attenuation also increased. Correlations were found between the 4.0 MHz signal attenuation and the void volume fraction, and between the number of fatigue cycles to failure and the 4.0 MHz signal attenuation.

Williams, J. H., Jr.↗

Failure mechanism characterization of platinum alloy

This article describes procedures and results of testing performed on a platinum/10-percent rhodium, thin-wall tubular product. The purpose of the testing was to develop exemplar SEM fractographs to be used to characterize failures under various environmental conditions. Conditions evaluated for the platinum alloys included high temperature, hydrogen environment, braze metal contamination, and cyclic loading.

Rosen, J. M.↗

Microstructural, Chemical and Mechanical Characterization of Polymer-Derived Hi-Nicalon Fibers with Surface Coatings

Room temperature tensile strengths of as-received Hi-Nicalon fibers and those having BN/SiC, p-BN/SiC, and p-B(Si)N/SiC surface coatings, deposited by chemical vapor deposition, were measured using an average fiber diameter of 13.5 microns. The Weibull statistical parameters were determined for each fiber. The average tensile strength of uncoated Hi-Nicalon on was 3.19 +/- 0.73 GPa with a Weibull modulus of 5.41. Strength of fibers coated with BN/SiC did not change. However, coat with p-BN/SiC and p-B(Si)N/SiC surface layers showed strength loss of approx. 10 and 35 percent, respectively, compared with as-received fibers. The elemental compositions of the fibers and the coatings were analyzed using scanning Auger microprobe and energy dispersive x-ray spectroscopy. The BN coating was contaminated with a large concentration of carbon and some oxygen. In contrast, p-BN, p-B(Si)N, and SiC coatings did not show any contamination. Microstructural analyses of the fibers and the coatings were done by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and selected area electron diffraction. Hi-Nicalon fiber consists of the P-SIC nanocrystals ranging in size from 1 to 30 nm embedded in an amorphous matrix. TEM analysis of the BN coating revealed four distinct layers with turbostatic structure. The p-BN layer was turbostratic and showed considerable preferred orientation. The p-B(Si)N was glassy and the silicon and boron were uniformly distributed. The silicon carbide coating was polycrystalline with a columnar structure along the growth direction. The p-B(Si)N/SiC coatings were more uniform, less defective and of better quality than the BN/SiC or the p-BN/SiC coatings.

Bansal, Narottam P.↗

Mechanical Characterization of Reactively Brazed Metal-Composite Joints for Heat Rejection Systems

The joining of metal tubes to composite plates is required for heat-rejection components in several space applications. Currently a number of different braze compositions are being evaluated as to their effectiveness. Such tube-plate configurations cannot be represented by traditional methods of testing, e.g., lap joints. The joined region is not between two flat surfaces, but rather between a flat surface and a curved surface. Therefore, several tests have been employed to ascertain the effectiveness of the different braze approaches in tension and in shear that are both simple and representative of the actual system and relatively straightforward in analysis. The results of these "tube tests" will be discussed for the three different braze compositions, Cu-ABA, Ti-Cu-Sil, and Ti-Cu-Ni. In addition, fracture analysis of the failed joints was performed and offers insights into the cause of joint failure and the distinctions which need to be made between the "strength" of a joint versus the "load carrying ability" of a joint.

Morscher, Gregory N.↗