Full Scale Natural Gas Compressor Loop Testing with Blended Hydrogen
Summary of Phase 1 work
03 NATURAL GAS↗
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G3P3 Phase 3 Project Execution Plan. Issue 1
The National Solar Thermal Test Facility (NSTTF) at Sandia National Laboratories New Mexico (SNL/NM) developed this Project Execution Plan (PEP) to document its process for executing, monitoring, controlling and closing-out Phase 3 of the Gen 3 Particle Pilot Plant G3P3. This plan serves as a resource for stakeholders who wish to be knowledgeable of project objectives and how they will be accomplished. The plan is intended to be used by the development partners, principal investigator, and the federal project director. Project objectives are derived from the mission needs statement, and an integrated project team assists in development of the PEP. This plan is a living document and will be updated throughout the project to describe current and future processes and procedures. The scope of the PEP covers: Cost, schedule, and scope Project reporting Staffing plan Quality assurance plan Environment, safety, security, and health This document is a tailored approach for the Facilities Management and Operations Center (FMOC) to meet the project management principles of DOE Order 413.3B, Program and Project Management for the Acquisition of Capital Assets , and DOE G 413.3-15, DOE Guide for Project Execution Plans. This document will elaborate on content as knowledge of the project is gained or refined.
14 SOLAR ENERGY↗
Design Status and Experimental Strategy for Initial Molten Salt Irradiation Experiments in HFIR
The development and deployment of molten salt reactor (MSR) technologies require experimental capabilities that can evaluate molten fuel salt behavior and structural material performance under representative irradiation conditions. Although modeling and separate effects testing provide important insight, there remains a critical lack of in-pile data that capture the coupled effects of neutron irradiation, temperature, salt chemistry, and time. Informed by lessons learned from historical MSR programs and recent international irradiation efforts, this report presents a structured approach to addressing existing gaps in molten salt irradiation testing using the High Flux Isotope Reactor (HFIR). A phased irradiation strategy is presented that incrementally increases experimental complexity while managing cost, risk, and facility constraints. The framework progresses from passive, nonfueled static capsule experiments to fueled, instrumented, and ultimately circulating molten salt systems, providing a pathway for materials screening, mechanistic understanding, and qualification-relevant testing. The report defines a near-term Phase 1 passive capsule concept, associated irradiation conditions, and a conceptual post-irradiation examination strategy. Ongoing modeling, out-of-pile testing, and safety analysis activities are described to support continued capability maturation and to enable future phases of molten salt irradiation testing in support of MSR technology deployment.
22 GENERAL STUDIES OF NUCLEAR REACTORS↗
Knocking out barriers to engineered cell activity
Engineered T cell therapies are revolutionizing cancer treatment by achieving long-lasting remission in blood-related cancers, such as leukemia and lymphoma. These therapies involve removal of patient T cells, “reprogramming” them to attack cancer cells, and then transferring them back into the patient. Targeted gene inactivation (knockout) using CRISPR-Cas9 can enhance T cell activity (1, 2) and has the potential to expand cell therapy applications. Until now, it has been unknown whether CRISPR-Cas9–edited T cells would be tolerated and thrive once reinfused into a human. On page 1001 of this issue, Stadtmauer et al. (3) present data from a phase 1 clinical trial (designed to test safety and feasibility) on the first cancer patients treated with CRISPR-Cas9–modified T cells. The findings represent an important advance in the therapeutic application of gene editing and highlight the potential to accelerate development of cell-based therapies.
60 APPLIED LIFE SCIENCES↗
Sister Rod Destructive Examinations (FY20) Appendix D: Fission Gas, Fuel Burnup and Fuel Isotopic Measurements
This appendix documents the status of the ORNL Phase 1 DE activities related to fission gas sample analysis, fuel burnup analysis, and fuel isotopic analysis of selected sister specimens in Phase 1 of the sister rod test program.
11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
Sister Rod Destructive Examinations (FY2020) Appendix I: SNF Aerosols Released During Rod Fracture
As a part of the DOE NE High Burnup Spent Fuel Data Project, Oak Ridge National Laboratory (ORNL) is performing destructive examinations (DEs) of high burnup (HBU) (>45 GWd/MTU) spent nuclear fuel (SNF) rods from the North Anna Nuclear Power Station operated by Dominion Energy. The SNF rods, called sister rods or sibling rods, are all HBU and include four different kinds of fuel rod cladding: standard Zircaloy-4 (Zirc-4), low-tin Zirc-4, ZIRLO, and M5. This report documents the status of the ORNL Phase 1 DE activities related to the collection of SNF aerosol particles released during fuel rod fracture in four-point bending in Phase 1 of the sister rod test program.
11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
ULTIMATE FY22 Creep Test Facility Report (FY23 ARPA-E Milestone Report)
In the 18-month Phase 1 of this project, a facility was assembled for creep testing of refractory metals at 1300°C. This report focuses on the four creep frames that are operational and using an inert gas system (argon) to limit oxidation of the refractory metal specimens being tested. This report details the operations for the first period of operation including the results and lessons learned for Nb- and Mo-based alloy specimens tested by the ORNL team. For an alloy development program, a particularly unique feature of the ORNL facility is more than 40 years of experience conducting mechanical properties testing on sub-sized test specimens (25 mm long dogbones). Due to proprietary constraints, only one representative set of team data are provided. The primary concern for testing Nb-based alloys is oxygen ingress. Despite several strategies to reliably limit O ingress, including getters and Ar gas purity, the experimentally informed strategy currently being developed is a new load train design intended to better seal the system. Hardware for the new design is currently being fabricated.
36 MATERIALS SCIENCE↗
Soar Survey Scoring
ORNL conducted an experiment to test COTS (commercial off the shelf) SOAR tools. Vendors interested in entering their tool into the experiment were asked to submit information videos about their tool for phase 1 to down-select which tools should make it through to the testing phase. SOC operators were assigned to watch a subset of the videos such that each video was assigned to the same number of operators. After watching all the videos, operators completed surveys which asked them to grade basic aspects about the tool as best as they could based on the provided video, and asked them to rank the order of their interest in the vendors they were assigned to watch videos on. The problem solved was how do we aggregate the results of the surveys and each of the operator's ranked lists into an overall ranking of all the tools. In addition, it was desirable to be able to work on this code before final results were collected from operators, so code to generate fake data was developed to output in the same output as the survey results.
Bridges, Robert↗
Pilot Scale Operation and Testing of Syngas Chemical Looping For Hydrogen Production
The Syngas Chemical looping (SCL) process provides efficient and economic means to utilize the abundant fossil reserve of coal. The main problem associated with coal utilization is the CO 2 emissions resulting from its combustion. Even though CO 2 regulation or carbon tax is currently not in place, its enforcement is expected in the near future. Such a greenhouse gas emission control, if adopted in current power plant systems, will drive the efficiency down and increase the cost of electricity, due to the energy and capital-intensive nature of current CO 2 separation techniques. This highlights the need to develop technologies that present a solution to the rising cost of electricity in the future. The integrated gasification combined cycle (IGCC) presents an improvement to the above predicament, but it is capital intensive due to the extensive unit operations involved. The efficiency for a CO 2 capture incorporated IGCC system is around ~32%, resulting in approximately 45% increase in cost of electricity. This is definitely a better path to traverse than the conventional pulverized coal (PC) power plants as it has improved economics and efficiencies accompanied by product flexibility. The SCL process advances the benefits even further when integrated with the IGCC process. The SCL process removes the expensive WGS system and CO 2 separation columns, thereby saving on capital and operational expenses. This integration results in a 12 – 21% increase in efficiency accompanied by a reduction in cost of electricity by 15 – 28%, over conventional IGCC systems. Therefore, SCL process provides the best route to harness the energy from coal. The overall project objective was to construct and operate a syngas chemical looping pilot scale test unit at the NCCC. The project scope of work was divided into 3 phases. In Phase I, cold flow model studies using a 1:1 scale acrylic test unit constructed at Particulate Solids Research, Inc. (PSRI) was successfully completed confirming robust solid flow control is achievable in the non-mechanical system design. In Phase II, the high pressure, high temperature, chemical looping reactor was successfully designed with all necessary equipment and safety instrumentation/controls specified to allow for fabrication, site construction, and assembly to commence in Phase III. In Phase III, the SCL pilot plant was successfully assembled and all necessary functional checks and pre-startup safety reviews completed. During unit commission over the course of 200 hours of testing, operational issues were observed with premix burner used for system startup. With the grants awarded by the National Energy Laboratory (NETL) and the Ohio Development Services Agency (ODSA) under awards DE-FE0023915 and D-14-18, the SCL pilot unit underwent three auxiliary equipment modifications to resolve all of the startup operational issues encountered. The unit was successfully demonstrated with 300+hr continuous operation. Key results obtained include high syngas conversion of 97.95% with 16.03% oxygen carrier conversion in the moving bed reducer and >99% purity H 2 produced from the moving bed oxidizer.
01 COAL, LIGNITE, AND PEAT↗
M 3 : a new muon missing momentum experiment to probe (g – 2) μ and dark matter at Fermilab
Here, new light, weakly-coupled particles are commonly invoked to address the persistent $\sim 4\sigma$ anomaly in $(g-2)_\mu$ and serve as mediators between dark and visible matter. If such particles couple predominantly to heavier generations and decay invisibly, much of their best-motivated parameter space is inaccessible with existing experimental techniques. In this paper, we present a new fixed-target, missing-momentum search strategy to probe invisibly decaying particles that couple preferentially to muons. In our setup, a relativistic muon beam impinges on a thick active target. The signal consists of events in which a muon loses a large fraction of its incident momentum inside the target without initiating any detectable electromagnetic or hadronic activity in downstream veto systems. We propose a two-phase experiment, M$^3$ (Muon Missing Momentum), based at Fermilab. Phase 1 with $\sim 10^{10}$ muons on target can test the remaining parameter space for which light invisibly-decaying particles can resolve the $(g-2)_\mu$ anomaly, while Phase 2 with $\sim 10^{13}$ muons on target can test much of the predictive parameter space over which sub-GeV dark matter achieves freeze-out via muon-philic forces, including gauged $U(1)_{L_\mu - L_\tau}$.
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
Radiation Hardened Foam Cold Test Plan – Phase-I: Foam Adhesion, Contamination Fixation, Moisture Stresses, Pipe Cutting, and Thermal Profile Testing
This document outlines the Phase-I test objectives and implementation plan for a down-selective foam fixative technology intended to facilitate activities in support of the Savannah River Site (SRS) F/H labs deactivation and decommissioning (D&D) efforts. It is a collaborative effort between Savannah River National Laboratory (SRNL), Florida International University (FIU), and the SRS F/H labs team intended to test and evaluate the potential of an intumescent, fire-retardant foam in mitigating the release of contamination during dismantling operations on radioactively contaminated piping in legacy facilities. The cold test plan addresses specific requirements highlighted by site and safety personnel and will be executed in FIU’s Outdoor Test and Evaluation Facility using a mock-up that replicates the operational conditions at the proposed hot test location at F/H labs. Results from the cold test plan will inform the hot test at F/H labs, which will use the foam fixative to confine and/or isolate residual contamination within a 3-dimensional void space of Hastelloy C-22 piping designated for removal from the site and transported to a proper disposal facility. Phase-I testing will address eight test objectives: (1) evaluation of the adhesion and bonding properties of foam fixative in piping, (2) evaluation of the adhesion of the foam fixative in piping under varying moisture conditions, (3) determination of the heat profile of the foam fixative during curing, (4) determination of the relationship between pipe diameter and foam fixative quantity, (5) determination of the internal pipe pressure after foam deployment and curing, (6) development of a leak test standard operating procedure to test for the effectiveness of the foam plug, (7) initiation of a literature review to determine if using a hot tap is a viable method to deliver foam into piping, and (8) initiation of a 10-foot mock up test that will be used in Phase-II cold testing. The cold test will be conducted at FIU and all testing activities will comply with SRNL Conduct of R&D Protocols (SRNL-IM-2020-00019).
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
Permanganate Oxidation of Defense Waste Processing Facility (DWPF) Recycle Collection Tank (RCT) Simulants Larger Scale Protocol Runs - Chemical Process Cell (CPC) Nominal and Foamover Conditions
Testing to develop a process to oxidize glycolate and other organic species in non-radioactive waste simulants was requested by Savannah River Remediation (SRR). A Task Technical and Quality Assurance Plan (TTQAP) was written to describe the testing requested by SRR in the development of a process to oxidize glycolate and other organic species that are responsible for hydrogen generation from thermolysis. Scoping studies have been completed as requested by a Technical Assistance Request (TAR) to evaluate the feasibility of using sodium permanganate and Fenton's Reagent (iron catalyzed hydrogen peroxide) for destroying glycolate. The results from these scoping studies were summarized in a report. Six phases of tests with simulants have been planned in developing an oxidation flowsheet for the Recycle Collection Tank (RCT), as shown in Table 1. The first three phases have been completed. The first phase comprised of scoping tests of permanganate and Fenton's reagent. The second phase was a matrix of 23 tests completed to inform a down-select decision by SRR and to complete testing needed to understand the influence of various factors in defining the optimum processing conditions for oxidation of organics. From the results of this testing, oxidation by permanganate was chosen over Fenton's reagent with hydrogen peroxide. The third phase of testing was to demonstrate nominal operation of the permanganate oxidation process under protocols similar to those used in the Defense Waste Processing Facility (DWPF).
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
Performance Evaluation of a Single-Phase Grid-Forming Inverter Through Hardware Experiments
This study conducts hardware experiments to assess the performance of a commercial single-phase grid-forming (GFM) inverter using a purely hardware-based approach. We adhere to a testing protocol for the GFM inverter and enhance it by exploring the transient performance of GFM inverters across various grid dynamic events. Quantifiable performance metrics are established for each testing scenario to gain insights into the performance of the single-phase GFM inverters. Based on the comprehensive tests, the following observations are summarized: 1) The performance of the single-phase GFM inverter is satisfactory, and it is capable of being the islanding master for residence homes when the main grid is gone. 2) For frequency response, the inverter is able to stay connected but cannot inject the needed active power to support the grid. This may be improved by the manufacturer by using droop control. 3) The GFM inverter exhibits harmful transients in voltage and frequency during islanding operation, which can be enhanced by maintaining the same operating points before and after the breaker is open.
black start↗
Radiation Hardened Foam Cold Test Plan - Phase II: Foam Characterization Testing and Environmental Chamber Testing of FoamBag Fixative Foam
This document outlines the Phase II test objectives and implementation plan for a down-select foam fixative technology intended to facilitate activities in support of the Savannah River Site (SRS) F/H labs deactivation and decommissioning (D&D) efforts. It is a collaborative effort between Savannah River National Laboratory (SRNL), Florida International University (FIU), and the SRS F/H labs team intended to test and evaluate the potential of a polyurethane resin foam in mitigating the release of contamination during dismantling operations on radioactively contaminated piping in legacy facilities. The cold test plan addresses specific requirements highlighted by site and safety personnel and will be executed at FIU and SRNL test and lab facilities. Results from the cold tests will inform the hot test at F/H labs, which will use the foam fixative to confine and/or isolate residual contamination within a 3-dimensional void space of Hastelloy C-22 piping designated for removal from the area and transported to a designated disposal facility. Phase I testing was previously conducted using Hilti CP620 fixative foam. Results from Phase I testing indicate Hilti CP-620 fixative foam is incompatible with SRS site hot taps as an effective foam delivery method into Hastelloy C-22 piping. Phase II testing will be conducted using FoamBag TM fixative foam as an alternative fixative foam option. Phase II testing will address eight test objectives: (1) evaluation of the adhesion and bonding properties of FoamBag TM in Hastelloy C-22 piping, (2) evaluation of the adhesion of FoamBag TM in piping under various moisture conditions, (3) determination of the heat profile of FoamBag TM during curing, (4) determination of the internal pipe pressure after FoamBag TM deployment and curing, (5) conduct a leak test to determine if FoamBag TM is effective at creating a full seal within piping, (6) headspace testing of FoamBag TM to determine if there are any associated off-gas hazards during FoamBag TM curing, (7) conduct environmental chamber testing of FoamBag TM to understand how environmental parameters impacts FoamBag TM curing, and (8) conduct fire testing to evaluate FoamBag TM fire retardant characteristics.
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
Flexible FlueCO2
Carbon dioxide (CO2) emission reductions remain a significant challenge on the path to clean energy. There are increasing legislative, social, and environmental factors motivating CO2 emissions reduction from power plants with carbon capture and storage (CCS). CCS in natural gas combined cycle (NGCC) power plants is critical to achieve a net-zero carbon electricity grid. Enhanced 45Q tax credits provide new incentives, but currently available technologies are unable to profitably operate in grids with deep variable renewable penetration which require flexible NGCC operation. Luna Labs has developed the FlueCO2 membrane to enable a profitable NGCC-CCS process. The FlueCO2 membrane couples steam transport across the membrane to CO2 transport in the opposite direction, enabling high capture efficiencies and low energy costs even at low CO2 concentrations. The dual-phase membrane can operate in the range of typical flue gas temperatures and pressures and does not require temperature or pressure cycling. Luna Labs’ FlueCO2 technology enables flexible and profitable operation of NGCC plants with lower capital investment and impact on electricity prices. In this Phase 1 project, Luna Labs utilized experimental testing, modeling, process simulation, and standardized costing methodologies to evaluate the techno-economic value of a 650 MW greenfield NGCC plant with FlueCO2 (NGCC-FlueCO2). Key design requirements for operation were established and plant performance under load-leveling conditions was validated through computational fluid dynamics and process modeling. Luna Labs developed a dynamic modeling tool which modeled plant operational modes across a variety of tax structures and electricity pricing scenarios to project the overall Net Present Value (NPV) of the NGCC-FlueCO2. FlueCO2 minimizes the impact of CCS integration on plant operation by integrating directly into the NGCC heat recovery steam generator (HRSG). By tapping into the plant’s low-pressure (LP) steam, operators can divert LP steam to the greenfield NGCC and/or CCS process in response to dynamic markets. Since FlueCO2 will not significantly affect HRSG (or NGCC) operation, CCS only turns off during peak power demand (>$250/MWh). Under baseload conditions, FlueCO2 lowers the capital (37%), energy (36%) and carbon capture (<$40/tonne) costs and can increase the overall plant lifetime NPV by approximately ~$1B in comparison with NGCC solvent-based capture reference cases (NETL Case 31B). Luna Labs has shared its costing tools with several interested partners and customers, which follows a generalizable approach to costing analysis.
Kelly, Jesse↗
Research at UC Berkeley on the SPICE and HeRALD Dark Matter Experiments (Technical Report for DE-SC0022354)
The McKinsey and Pyle groups have taken on the responsibility to complete a number of critical tasks necessary for the successful completion of the TESSERACT project planning phase. In particular: 1) Transition Edge Sensor testing, characterization, and electromagnetic noise mitigation; 2) Design and testing of the athermal phonon detectors along with vibrational noise characterization and mitigation; 3) Testing and characterization of prototype detectors using silica, sapphire, gallium arsenide, and superfluid helium as detector materials. This grant supported efforts of graduate student Roger Romani toward these goals.
47 OTHER INSTRUMENTATION↗
Coalition for Community-Supported Affordable Geothermal Energy Systems (C2SAGES)
The C2SAGES project evaluated the feasibility of a community geothermal system for the planned Windy Ridge affordable housing development in Hinesburg, Vermont. Led by GTI Energy with Vermont Gas Systems, LN Consulting, NREL, and Frontier Energy, the work assessed technical design, energy performance, costs, business models, community engagement, maintenance, workforce development, and permitting. The proposed system was designed to serve 100% of the development’s heating, cooling, and domestic hot water loads. Compared with a baseline using air-source heat pumps and natural gas water heating, the geothermal system was estimated to reduce HVAC and domestic hot water energy use by about 45% to 48%, lower operating and maintenance costs, and reduce 30-year life-cycle costs by 37% for Phase 1 and 10% for Phase 2. Technical testing and modeling indicated that the Windy Ridge site is suitable for a community-scale geothermal system. The project also developed borehole field layouts, piping concepts, pump house designs, controls, maintenance plans, and supporting engineering drawings. The business model analysis found that first cost, ownership structure, and customer affordability remain major deployment challenges. Utility-led maintenance and operation were viewed favorably, but traditional utility cost-recovery models may require subsidy or revised financing structures to be practical for affordable housing. Community engagement highlighted the need for clear public education, transparent financing, reliable long-term maintenance, trained technicians, and the potential to pair geothermal systems with weatherization. Overall, the report concludes that community geothermal is technically feasible and offers meaningful energy, emissions, and life-cycle cost benefits, but broader deployment will depend on workable financing models and workforce readiness.
15 GEOTHERMAL ENERGY↗
Performance Evaluation of a Single-Phase Grid-Forming Inverter Through Hardware Experiments
This study conducts hardware experiments to assess the performance of a commercial single-phase grid-forming (GFM) inverter using a purely hardware-based approach. We adhere to a testing protocol for the GFM inverter and enhance it by exploring the transient performance of GFM inverters across various grid dynamic events. Quantifiable performance metrics are established for each testing scenario to gain insights into the performance of the single-phase GFM inverters. Based on the comprehensive tests, the following observations are summarized: 1) The performance of the single-phase GFM inverter is satisfactory, and it is capable of being the islanding master for residence homes when the main grid is gone. 2) For frequency response, the inverter is able to stay connected but cannot inject the needed active power to support the grid. This may be improved by the manufacturer by using droop control. 3) The GFM inverter exhibits harmful transients in voltage and frequency during islanding operation, which can be enhanced by maintaining the same operating points before and after the breaker is open.
dynamic performance↗