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DOE OSTI2023

Epitaxial growth of oriented CoO films by radio-frequency sputtering deposition

Rock-salt CoO is a p-type semiconductor and its Neel temperature is close to room temperature. CoO-based compounds are known as promising systems for renewable energy harvest with high efficiency. CoO with catalytic and exchange bias properties can be widely used for industrial applications. In this paper, we report high-quality stable CoO(111) and (100) films epitaxially grown on c-cut (0001) and r-cut ($10\bar1$2) alpha-Al 2 O 3 substrates, respectively, using radio-frequency sputtering deposition. X-ray diffraction (XRD) measurements revealed that the CoO films had a rock-salt structure (Fm3m) with lattice constants of 4.2477 Å and 4.2617 Å for film grown on (0001) and ($10\bar1$2) α-Al 2 O 3 substrates, respectively. CoO films with the best crystal quality were grown at a substrate temperature of similar to ~700°C. XRD measurements of CoO(111) films indicated a lack of structural residual strain, whereas CoO(100) films had substantial amounts of structural strain. X-ray reflectivity (XRR) and transmission electron microscopy measurements showed neither oxygen vacancy nor defects in both CoO(111) and (100) films. Further, XRR revealed that the mean electron density of the CoO films was nearly identical to a pure CoO and that the films were considerably stable under the atmosphere.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Atomic Layer Deposition Niobium Nitride Films for High-Q Resonators

Niobium nitride (NbN) is a useful material for fabricating detectors because of its high critical temperature and relatively high kinetic inductance. In particular, NbN can be used to fabricate nanowire detectors and mm-wave transmission lines. When deposited, NbN is usually sputtered, leaving room for concern about uniformity at small thicknesses. In this work, we present atomic layer deposition niobium nitride (ALD NbN) as an alternative technique that allows for precision control of deposition parameters such as film thickness, stage temperature, and nitrogen composition. Atomic-scale control over film thickness admits a high degree of uniformity for films 4–30 nm thick; control over deposition temperature gives rise to growth rate changes, which can be used to optimize film thickness and critical temperature. In order to charac- terize ALD NbN in the radio-frequency regime, we construct single-layer micro- wave resonators and test their performance as a function of stage temperature and input power. ALD processes can admit high resonator quality factors, with ≥ 43% of resonators above Q i = 10 6 , which in turn increase detector multiplexing capabilities. i Furthermore, we find critical temperatures in the range of 7.5–10.9 K that vary as a function of cycle count and deposition temperature.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2022

Autonomous Wireless Technology Detection in Seamless IoT Applications

The ever-increasing use of Internet of Things (IoT) devices results in the implementation of multiple wireless technologies that would not only cater their data rate requirements but also support various applications. To optimize the energy efficiency and security of the wireless transmission, it is imperative to identify the wireless technologies in various IoT implementations. Many of the existing approaches are based on measuring only the receiving signal strength indicator (RSSI). However, such approaches may not work well because of transmit power control and complex channel variations among different wireless technologies. In this article, we propose an autonomous wireless detection scheme that considers multiple distinguishable physical (PHY)-layer settings for real-time identification of wireless technologies for real-time applications. Specifically, the proposed scheme relies on the PHY-layer measurements of the targeted spectrum. Transmission settings, such as bandwidth, carrier frequency, and RSSI are estimated from the raw in-phase and quadrature-phase (I/Q) measurements. In addition, a symbol-level extraction scheme is implemented to extract unique features of modulation settings. These aforementioned features are applied to a machine learning process to identify the received wireless technologies. Compared with raw I/Q measurements, the extracted features are much simplified and, thus, the machine learning classifier can be designed with a simple structure for fast processing on IoT nodes. Finally, the proposed schemes are primarily evaluated theoretically, followed by implementing them on a USRP software-defined radio (SDR)-based hardware testbed. The evaluation results demonstrate high accuracy in the real-time detection of different wireless technologies for seamless IoT applications.

42 ENGINEERING↗

DOE OSTI2026

Digital Grid Twin–Direct Communication Scheme Test Bed for Assessing Relay-to-Relay Radio Antenna and Optical Fiber Performance and Misoperations

This study introduces a novel “Digital Grid Twin–Direct Communication Scheme” test bed. This advanced platform evaluates point-to-point communication between transmitter and receiver relays with optical fiber and radio omnidirectional antenna systems, implemented at the Advanced Protection lab in the Grid Research Innovation and Development Center at Oak Ridge National Laboratory. The increased diversity of energy sources has led to more protective relay misoperations. In North America, microgrid protection schemes now use point-to-point communication along distribution lines between relays to implement advanced logic in nonradial grids that include both high- and low-inertia generators. This trend challenges utilities to minimize misoperations while ensuring rapid fault clearance and accurate selectivity coordination between primary and backup relays. This study assesses relay-to-relay communication schemes by introducing an advanced testing platform based on a digital grid twin protection test bed using a synchronized time source system. The platform evaluates the communication system using radio antennas or optical fiber links by integrating protective relays that operate breakers within the digital twin and record relay events and communication signals. In the experiments, transmitter and receiver relays were configured with inverse time overcurrent and breaker trip detection logic to assess the total time of the communication protection schemes based on the sum of the relay protection element operating time, radio latency, propagation delay, baud rate delay, and relay processing time. These delays were derived from recorded relay events and communication signals from the interface of a real-time simulator set as a digital grid twin. The test bed successfully simulated various electrical faults along a distribution line while ensuring effective and reliable point-to-point communication between transmitter and receiver relays. The radio antenna communication system exhibited latency because of the radio. This latency depends on the baud rate setting and type of radio application; in general, the higher the baud rate, the lower the radio latency. The measured radio latency (for Mirrored Bits with an encryption card at 9,600 bps) was about 9–10 ms. Additionally, calculated propagation delay per mile for radio antennas and optical fiber was 5.36 µs/mi and 8.04 µs/mi, respectively. Optical fiber communication did not demonstrate radio latency. Instead, the protection element operating time depends mainly on the protection logic function set in the relay, and the relay processing time depends on the processing rate of the relay in samples per power system cycle.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2021

Searching for Interstellar Quantum Communications

The modern search for extraterrestrial intelligence began with the seminal publications of Cocconi & Morrison and Schwartz & Townes, who proposed searching for narrowband signals in the radio spectrum and optical laser pulses. Over the last six decades, more than 100 dedicated search programs have targeted these wavelengths, all with null results. All of these campaigns searched for classical communications, that is, for a significant number of photons above a noise threshold, with the assumption of a pattern encoded in time and/or frequency space. I argue that future searches should also target quantum communications. They are preferred over classical communications with regard to security and information efficiency, and they would have escaped detection in all previous searches. The measurement of Fock state photons or squeezed light would indicate the artificiality of a signal. I show that quantum coherence is feasible over interstellar distances and explain for the first time how astronomers can search for quantum transmissions sent by ETI to Earth using commercially available telescopes and receiver equipment.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2026

Superconducting Material Growth for Radio-Frequency (RF) Cavities

Superconducting radio-frequency (SRF) cavities, usually manufactured from Niobium (Nb), are vital components of modern particle accelerators because of their ability to achieve high acceleration gradients with little power dissipation. Naturally forming Nb surface oxides significantly alter cavity performance by changing surface resistance. A nondestructive characterization of oxide thickness is helpful for relating surface processing treatments to cavity performance. This work develops a protocol to measure Nb oxide thickness using Angle-Resolved X-ray Photoelectron Spectroscopy (ARXPS) while correcting instrumental errors. Using uniform bulk standard samples (Silver, Aluminum oxide, and Germanium), we determined a baseline correction factor to account for analyzer-related intensity evolution as the measurement angle increases. The correction factor was then applied to Nb 3d ARXPS data. Applying the Strohmeier equation to the corrected data yielded a Nb2O5 thickness of 6.04 nm, closely matching the 5.5 (±.05) nm value obtained from cross-sectional transmission electron microscopy. Our approach will bring a method to incorporate inherent errors in the thickness measurements using ARXPS and can be broadly applied to improve the accuracy of thickness measurements in a wide range of heterostructures.

Lambert, Nathan [Fermilab]↗

DOE OSTI2026

Superconducting Material Growth for Radio-Frequency (RF) Cavities

Lambert, Nathan [Fermilab]↗

DOE OSTI2024

Modeling Communication Infrastructures of Cyber Physical Systems

This effort explores modeling cyber infrastructure, including communication devices like switches, routers, sensors, and controllers, and physical media attributes like propagation of radio signals, in coordination with power distribution system model layouts. To do this, the project studies real-world configurations to define axioms of how different communication media is deployed with control equipment. These axioms will be used to develop tools to generate realistic cyber infrastructure models from starting power system models. This effort leverages and builds on the co-simulation platform developed by the other RD2C projects. The axioms and tools will be validated and demonstrated with the NS3 simulation tool as part of a co-simulation to show the behavior/impacts of cyber infrastructure on control operations.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2024

Design and optimization of higher order mode couplers for the superconducting cavities of the PERLE energy recovery linac

The Powerful Energy Recovery Linac for Experiments (PERLE) is an energy recovery linac (ERL) facility based on superconducting radio-frequency (SRF) technology to be hosted at the Laboratoire de Physique des 2 Infinis Irène Joliot-Curie (IJCLab) in France. With a target beam power of 10 MW, PERLE aims to demonstrate the high-current, continuous wave, multi-pass operation to validate options for future high-energy machines, such as the 50 GeV ERL proposed for the Large Hadron electron Collider (LHeC) and the Future Circular electron-hadron Collider (FCC-eh), and host dedicated particle physics and nuclear experiments. In high-current ERLs, the regenerative Beam Breakup (BBU), emerging from the beam and cavity Higher Order Modes (HOMs) interaction, is a major concern for their stable operation. Beam-induced HOMs can increase the cavity heat load at cryogenic temperature and cause beam instabilities. HOM couplers are installed in the cavity beam pipes to absorb HOM energy and mitigate these effects. This thesis presents the design and optimization of several coaxial HOM couplers for the 5-cell 801.58 MHz elliptical Nb cavities of the 500 MeV PERLE ERL configuration. The RF transmission of the HOM couplers was optimized to enhance the damping of the most dangerous HOMs. The optimized HOM couplers were integrated into endgroups to simulate their damping performance and thermal behavior. The optimized HOM couplers were 3D-printed in epoxy and copper-coated. Low-power RF measurements were conducted on the produced HOM couplers installed in copper PERLE-type cavities to validate their damping performance and propose several endgroups for the PERLE 5-cell cavity to mitigate HOMs below the BBU instability limits.

Barbagallo, Carmelo↗

DOE OSTI2021

Development and characterization of Nb3Sn/Al2O3 superconducting multilayers for particle accelerators

Abstract Superconducting radio-frequency (SRF) resonator cavities provide extremely high quality factors > 10 10 at 1–2 GHz and 2 K in large linear accelerators of high-energy particles. The maximum accelerating field of SRF cavities is limited by penetration of vortices into the superconductor. Present state-of-the-art Nb cavities can withstand up to 50 MV/m accelerating gradients and magnetic fields of 200–240 mT which destroy the low-dissipative Meissner state. Achieving higher accelerating gradients requires superconductors with higher thermodynamic critical fields, of which Nb 3 Sn has emerged as a leading material for the next generation accelerators. To overcome the problem of low vortex penetration field in Nb 3 Sn, it has been proposed to coat Nb cavities with thin film Nb 3 Sn multilayers with dielectric interlayers. Here, we report the growth and multi-technique characterization of stoichiometric Nb 3 Sn/Al 2 O 3 multilayers with good superconducting and RF properties. We developed an adsorption-controlled growth process by co-sputtering Nb and Sn at high temperatures with a high overpressure of Sn. The cross-sectional scanning electron transmission microscope images show no interdiffusion between Al 2 O 3 and Nb 3 Sn. Low-field RF measurements suggest that our multilayers have quality factor comparable with cavity-grade Nb at 4.2 K. These results provide a materials platform for the development and optimization of high-performance SIS multilayers which could overcome the intrinsic limits of the Nb cavity technology.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2024

Towards Construction of a Novel Nanometer-Resolution MeV-STEM for Imaging Thick Frozen Biological Samples

Driven by life-science applications, a mega-electron-volt Scanning Transmission Electron Microscope (MeV-STEM) has been proposed here to image thick frozen biological samples as a conventional Transmission Electron Microscope (TEM) may not be suitable to image samples thicker than 300–500 nm and various volume electron microscopy (EM) techniques either suffering from low resolution, or low speed. The high penetration of inelastic scattering signals of MeV electrons could make the MeV-STEM an appropriate microscope for biological samples as thick as 10 μm or more with a nanoscale resolution, considering the effect of electron energy, beam broadening, and low-dose limit on resolution. The best resolution is inversely related to the sample thickness and changes from 6 nm to 24 nm when the sample thickness increases from 1 μm to 10 μm. To achieve such a resolution in STEM, the imaging electrons must be focused on the specimen with a nm size and an mrad semi-convergence angle. This requires an electron beam emittance of a few picometers, which is ~1000 times smaller than the presently achieved nm emittance, in conjunction with less than 10 -4 energy spread and 1 nA current. We numerically simulated two different approaches that are potentially applicable to build a compact MeV-STEM instrument: (1) DC (Direct Current) gun, aperture, superconducting radio-frequency (SRF) cavities, and STEM column; (2) SRF gun, aperture, SRF cavities, and STEM column. Beam dynamic simulations show promising results, which meet the needs of an MeV-STEM, a few-picometer emittance, less than 10 -4 energy spread, and 0.1–1 nA current from both options. Also, we designed a compact STEM column based on permanent quadrupole quintuplet, not only to demagnify the beam size from 1 μm at the source point to 2 nm at the specimen but also to provide the freedom of changing the magnifications at the specimen and a scanning system to raster the electron beam across the sample with a step size of 2 nm and the repetition rate of 1 MHz. This makes it possible to build a compact MeV-STEM and use it to study thick, large-volume samples in cell biology.

36 MATERIALS SCIENCE↗

DOE OSTI2022

Integration of Wireless Sensor Networks and Battery-free RFID for Advanced Reactors

To address an important need for Nuclear Power Plants (NPPs) to significantly reduce the amount of the required cables for sensor data communications, this Phase I SBIR effort successfully developed and demonstrated a novel low-cost proof-of-concept prototype of a secure wireless sensor network backbone communications system. This system combines commercially available low power, low cost XBEE wireless communications network and passive (battery-free) Radio Frequency Identification (RFID) systems to report individual sensor data and their location through the containment wall for rapid response to anomalies in nuclear facilities. This WIreless Sensing and Locating (WISLO) system network architecture allows non-intrusive wireless collection of sensor data with the sensor’s accurate location information from inside of the instrumentation or containment area with minimal need for power sources. The multi-node sensor data in the containment area is wirelessly transmitted to outside through the metal reinforced concrete walls without the need for any batteries. The WISLO system could be readily used in current reactor fleet and future advanced reactors, as well as in small modular reactors (SMR). The WISLO system is the first dual frequency battery-free trough the wall communications backbone system developed specifically for use in nuclear power plants. It not only can modernize the sensor monitoring practices in the existing reactor fleet, but also offers a secure, low-cost solution to advanced reactors and SMRs by removing cables and issues related to them such as cable integrity, reporting delays, and installation and maintenance costs. The intent is to improve process safety, reliability, efficiency, and cost effectiveness to the monitoring and maintenance process in current and future plants. As we address the next productization and manufacturing capabilities in the next phase, this system will serve the needs of many commercial and government applications in remote monitoring of sensor data that demand battery-free transmission of sensor data such as Internet-of-Things (IOT).

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2024

Foreword: Special Section on Multiphysics Aspects of Power Electronics Packaging—Power Die, Power Module, and Converter Level: Part 2

Power electronics are increasingly being used to condition electricity for a wide array of applications, such as transportation (on land, air, and water), data centers, radio frequency, directed energy, wind, solar, and grid-tied applications. Here, to increase power density, performance, efficiency, and reliability-as well as to reduce cost-innovations and developments are needed in the multiphysics packaging of power electronics at a die, module, and converter level. This includes fundamental R&D related to emerging high-voltage, high-temperature, and high-switching-frequency power electronics, packaging materials, thermal materials and interfaces, fluid-based thermal management technologies, reliability, condition monitoring, and prognostics. Latest developments in this area are published as a Special Section on Multiphysics Aspects of Power Electronics Packaging. The first part was published in the May 2024 issue of the IEEE Transactions on Components, Packaging and Manufacturing Technology (Volume 14, Issue 5). The second part of that Special Section is being published in this issue. A brief summary of the papers included in the second part are given below.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2020

Novel High-Power Microwave Circulator Employing Circularly Polarized Waves

A novel four-port circulator is presented which uses an inline ferromagnetic element to allow for transmission or reflection depending on the sense of the incident circularly polarized wave. This configuration has been shown to reduce the dependency on ferrite anisotropy and support higher power, low rf loss, operation. An analytic analysis of this device is presented here alongside corroborating cold test data of the first prototype. High-power operation was performed at 2.856 GHz, with input power levels up to 8 MW for 3.5 μs in a pressurized nitrogen environment. The results from this research not only demonstrate ability to eliminate the use of greenhouse insulators, such as SF6, but also provide conceptual groundwork for a new class of ultrahigh power (50 MW+) nonreciprocal networks including circulators, isolators, phase shifters, and rf switches.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2024

Precision-controlled ultrafast electron microscope platforms. A case study: Multiple-order coherent phonon dynamics in 1T-TaSe2 probed at 50 fs–10 fm scales

We report on the first detailed beam tests attesting the fundamental principle behind the development of high-current-efficiency ultrafast electron microscope systems where a radio frequency (RF) cavity is incorporated as a condenser lens in the beam delivery system. To allow for the experiment to be carried out with a sufficient resolution to probe the performance at the emittance floor, a new cascade loop RF controller system is developed to reduce the RF noise floor. Temporal resolution at 50 fs in full-width-at-half-maximum and detection sensitivity better than 1% are demonstrated on exfoliated 1T-TaSe2 system under a moderate repetition rate. To benchmark the performance, multi-terahertz edge-mode coherent phonon excitation is employed as the standard candle. The high temporal resolution and the significant visibility to very low dynamical contrast in diffraction signals via high-precision phase-space manipulation give strong support to the working principle for the new high-brightness femtosecond electron microscope systems.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2023

Online Monitoring of Medium Voltage Cable Systems with Spread Spectrum Time Domain and Frequency Domain Reflectometry

In-service failures of wave energy convertor (WEC) cable systems can have a significant cost and power availability impact. Close parallel research 2019 data showed > 1B£ and 9 Terra-Watt-Hours associated with global off-shore wind (OSW) cable failures (Strang-Moran 2020). OSW is a closely related technology but currently is significantly cheaper than WEC technology. For wave energy to compete, the problem of reliable cable transmission must be mitigated. This project develops isolation technology to allow online high frequency reflectometry testing of medium voltage cables (1 to 10 kV and higher) without arcing or damage to the test instrument. Online spread spectrum time domain reflectometry (SSTDR) testing has been established for low voltage cable systems in the aircraft and rail industry and the ability to detect and locate cable flaws of interest is well understood. Extending reflectometry testing to medium voltage systems could enable detection of cable damage before failures occur thereby allowing repair and replacement of damaged cable segments to be scheduled and managed. The seedling project succeeded to pass and receive high frequency SSTDR signals onto a cable up to 1 kV using a parallel trace isolation circuit board that can be connected onto the test cable. The approach used a novel circuit design for which an invention disclosure has been filed. A proposed sapling project would extend the technology toward the higher operating voltages used by WEC systems, thereby enabling online SSTDR cable monitoring. The goal of the seedling project was to extend the capability of the ARENA cable/motor test bed to address medium voltages and to develop a high pass filter isolation architecture to protect the reflectometry instrument from the low frequency (DC – 60 Hz) line voltage while allowing the high frequency diagnostic signal to pass to and from the test instrument to the live line. Initial efforts focused on passive LCR filter circuits to reduce 60 Hz levels below 10 volts from a 10 kV line while allowing the MHz high frequency chirps to pass onto the cables and for mV signals to be detected. We discovered that the parasitic loss behavior of real high voltage components precluded this approach from working. An alternate approach was adapted for the electric field to couple between two parallel traces on a printed circuit board much like a radio-frequency coupler. The challenge here was and is to have the parallel traces close enough to each other to effectively pass the high frequency chirp onto the live line and receive any reflected signal from any encountered impedance change along the cable. This reflected signal will be in the mV range. The traces however must be far enough apart to not allow arcing on the board. A design with 3 mm spacing was determined to allow the high frequency signal to pass onto the live line and receive the mV signal back into the instrument while reducing the 60 Hz voltage amplitude by >80 dB (more than a factor of 10,000) without allowing arcing from across the parallel traces. This was confirmed by simulation and test.

16 TIDAL AND WAVE POWER↗

DOE OSTI2020

First-principles study and experimental characterization of metal incorporation in germanium telluride

Germanium telluride is a well-known phase change material (PCM) used in non-volatile memory cells and radio frequency switches. Controlling the properties of GeTe for improved PCM device performance has sometimes been achieved by doping and/or alloying with metals, often at concentrations greater than 10 at. % and using non-equilibrium methods. Here, since switching PCMs between the low-resistance crystalline and high-resistance amorphous states requires a heating cycle, the stability of metal-incorporated GeTe (Ge 0.5–x M x Te 0.5 ) films is also critical to practical implementation of these materials in electronic and optoelectronic devices. In this work, we use both density-functional theory and experimental characterization methods to probe the solubility and critical properties of Ge 0.5–x M x Te 0.5 films. Using first-principles calculations, we determine the enthalpy of formation for GeTe with 2.08, 4.17, and 6.25 at. % of Cu, Fe, Mn, Mo, and Ti and show trends between the stability of the Ge 0.5–x M x Te 0.5 systems and the atomic position, composition, and distribution of the metal atoms in the GeTe matrix.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Best Practices for Grid Communications

As the grid evolves, the communications architecture will need to evolve with it. That architecture affords a structured means by which the evolving complexities of the modern electric grid can be managed. This document provides best practices that can be implemented in the grid of today and evolve towards the grid and grid architecture of the future. The evolving grid and its control communications increasingly rely on commercial communications providers and a variety of technologies, from wireless (e.g., 5G, microwave, Wi-Fi) to wireline (fiber, copper) to radio communications (P25, other repeater-based systems), and all these communications systems rely on electric power. A reliable and resilient grid must account for this complex set of interdependencies in its planning activities, especially those involving restoration and recovery. The participation of all relevant parties in both planning and exercising of plans can prevent unexpected conditions that impede the reliable operation and recovery of the grid. Best practices for grid communications include using a Network Management System to document the operational state, define and monitor baselines, detect changes, and accelerate response to abnormalities. If transitioning from SONET to IP/packet-based systems, translating grid requirements into communications requirements for latency, bandwidth and throughput, IP packet delay variation, packet loss, and availability should inform and drive technology planning and selection as well as that communication system’s Quality of Service (QoS) policies and Service Level Agreements (SLAs). Secure and reliable timing is another key component of a reliable and resilient grid that can operate through adverse events. A trusted internal NTP configuration, an integrated and diverse timing delivery system, optimizing the timing architecture based on the transport technologies of the communications system, and using established standards can deliver the level of timing accuracy required by a range of time-sensitive power system applications.

24 POWER TRANSMISSION AND DISTRIBUTION↗