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Diffusion-Limited Kinetics of the Solution-Solid Phase Transition of Molecular Substances
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What Would Gibbs Do If he Were Thinking of Nucleation of Protein Solid Phases
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Dense Liquid Precursor for the Nucleation of Ordered Solid Phases from Solution, Crystal Growth and Design
No abstract available
Fundamental Aspects of Nucleation Theory Revealed in Experiments with Protein Solid Phases
No abstract available
Solvent Entropy Effects in the Formation of Protein Solid Phases
No abstract available
Solvent Entropy Effects in the Formation of Protein Solid Phases
No abstract available
Diffusion-limited Kinetics of the Solution-solid Phase Transition of Molecular Substances
No abstract available
Diffusion-Limited Kinetics of the Solution Solid Phase Transition of Molecular Substances
No abstract available
Solid Phase Gene Extraction Isolates mRNA at High Spatial and Temporal Resolution
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JANNAF 36th Combustion Subcommittee Meeting
Volume 1, the first of three volumes is a compilation of 47 unclassified/unlimited-distribution technical papers presented at the Joint Army-Navy-NASA-Air Force (JANNAF) 36th Combustion Subcommittee held jointly with the 24th Airbreathing Propulsion Subcommittee and 18th Propulsion Systems Hazards Subcommittee. The meeting was held on 18-21 October 1999 at NASA Kennedy Space Center and The DoubleTree Oceanfront Hotel, Cocoa Beach, Florida. Solid phase propellant combustion topics covered in this volume include cookoff phenomena in the pre- and post-ignition phases, solid rocket motor and gun propellant combustion, aluminized composite propellant combustion, combustion modeling and combustion instability and instability measurement techniques.
Solid state image sensor research, phase I
Solid state image sensor in infrared and visible regions
Hydrogen-silicon carbide interactions
A study of the thermochemistry and kinetics of hydrogen environmental attack of silicon carbide was conducted for temperatures in the range from 1100 C to 1400 C. Thermodynamic maps based on the parameters of pressure and oxygen/moisture content were constructed. With increasing moisture levels, four distinct regions of attack were identified. Each region is defined by the thermodynamically stable solid phases. The theoretically stable solid phases of Region 1 are silicon carbide and silicon. Experimental evidence is provided to support this thermodynamic prediction. Silicon carbide is the single stable solid phase in Region 2. Active attack of the silicon carbide in this region occurs by the formation of gases of SiO, CO, CH4, SiH4, and SiH. Analysis of the kinetics of reaction for Region 2 at 1300 C show the attack of the silicon carbide to be controlled by gas phase diffusion of H2O to the sample. Silicon carbide and silica are the stable phases common to Regions 3 and 4. These two regions are characterized by the passive oxidation of silicon carbide and formation of a protective silica layer.
Hydrogen-silicon carbide interactions
A study of the thermochemistry and kinetics of hydrogen environmental attack of silicon carbide was conducted for temperatures in the range from 1100 C to 1400 C. Thermodynamics maps based on the parameters of pressure and oxygen/moisture content were constructed. With increasing moisture levels, four distinct regions of attack were identified. Each region is defined by the thermodynamically stable solid phases. The theoretically stable solid phases of region 1 are silicon carbide and silicon. Experimental evidence is provided to support this thermodynamic prediction. Silicone carbide is the single stable solid phase in region 2. Active attack of the silicon carbide in this region occurs by the formation of gases of SiO, CO, CH4, SiH4 and SiH. Analyses of the kinetics of reaction for region 2 at 1300 C show the attack of the silicon carbide to be controlled by gas phase diffusion of H2O to the sample. Silicon carbide and silica are the stable phases common to regions 3 and 4. These two regions are characterized by the passive oxidation of silicon carbide and formation of a protective silica layer.
Solid state phase detector replaces bulky transformer circuit
Miniature solid state phase detector using MOSFETs is used in a phase lock loop with a sun-bit detector in an integrated data-link circuit. This replaces bulky transformer circuits. It uses an inverter amplifier, a modulator switch, and a buffer amplifier.
Extinguishment of a Diffusion Flame Over a PMMA Cylinder by Depressurization in Low-Gravity
The behavior of flames in low-speed flows in low-gravity is relevant to spacecraft fire safety. Previous work has shown that flames in the presence of low-speed forced flows in low-gravity may be more flammable than in a forced flow of the same magnitude in normal gravity. Additionally, fire suppression plans for the International Space Station include the use of venting (depressurization) as an emergency option for extinguishing fires. This procedure would induce flows in the affected compartment that could temporarily intensify the fire, as was observed in flammability tests of solids conducted on board Skylab. Despite a general Understanding, current knowledge of the combined effects of reduced pressure and forced flow on a burning solid in low-gravity is inadequate for the design of a venting extinguishment system. Previous studies in low-g have examined flammability limits for thermally thin solids. However, there are differences when burning thick materials because the interior solid-phase temperature continuously changes, which affects the percentage of gas-phase heat feedback to the solid-phase. Changes in the heat feedback to the solid-phase can affect the flammability characteristics of the material. In the current work, the extinction of a diffusion flame burning over PMMA (polymethyl methacrylate) cylinders during depressurization with a low-speed cross flow was examined experimentally and via numerical simulations.
Isotope effects in dense solid hydrogen - Phase transition in deuterium at 190 + or - 20 GPa
Raman measurements of solid normal deuterium compressed in a diamond-anvil cell indicate that the material undergoes a structural phase transformation at 190 + or - 20 GPa and 77 K. Spectroscopically, the transition appears analogous to that observed in hydrogen at 145 + or - 5 GPa. The large isotope effect on the transition pressure suggests there is a significant vibrational contribution to the relative stability of the solid phases of hydrogen at very high densities.
Interactions between solidification and compositional convection in mushy layers
Mushy layers are ubiquitous during the solidification of alloys. They are regions of mixed phase wherein solid crystals are bathed in the melt from which they grew. The matrix of crystals forms a porous medium through which the melt can flow, driven either by external forces or by its own buoyancy in a gravitational field. Buoyancy-driven convection of the melt depends both on temperature gradients, which are necessary for solidification, and on compositional gradients, which are generated as certain components of the alloy are preferentially incorporated in the solid phase and the remaining components are expelled into the melt. In fully liquid regions, the combined action of temperature and concentration on the density of the liquid can cause various forms of double-diffusive convection. However, in the interior of mushy regions the temperature and concentration are thermodynamically coupled so only single-diffusive convection can occur. Typically, the effect of composition on the buoyancy of the melt is much greater than the effect of temperature, and thus convection in mushy layers in driven primarily by the computational gradients within them. The rising interstitial liquid is relatively dilute, having come from colder regions of the mushy layer, where the liquidus concentration is lower, and can dissolve the crystal matrix through which it flows. This is the fundamental process by which chimneys are formed. It is a nonlinear process that requires the convective velocities to be sufficiently large, so fully fledged chimneys (narrow channels) might be avoided by means that weaken the flow. Better still would be to prevent convection altogether, since even weak convection will cause lateral, compositional inhomogeneities in castings. This report outlines three studies that examine the onset of convection within mushy layers.