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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4

Investigation of mounting discrete chip components for hybrid microelectronic applications.

In the assembly of hybrid microcircuits, passive and active discrete chip components are attached by epoxy cements and by solders. This study was initiated to determine the integrity of such attachments. Alumina substrates were subjected to a group of thermal and mechanical test environments defined by test methods in MIL-STD-883. Lot samples of substrates with assembly variations were subjected to separately applied testing and to serial testing. These test methods were applied sequentially to the same lot of substrates. Epoxy cements were generally satisfactory with respect to separate tests, although sequential tests severely degraded epoxy bond strengths of all types. Bond strengths to unglazed substrates were slightly superior to those of the same components on glazed types. Solder joints were vulnerable to catastrophic failure in several environments, especially temperature cycling and thermal shock. Vibration and impact shock also produced solder joint failures.

Caruso, S. V.↗

Ultraviolet effects on conductive coated coverglasses

Experiments on the International Sun-Earth Explorer required that the outer surface of the spacecraft be conductive. For the solar panels this was accomplished by using solar cell coverglasses coated with indium-oxide and interconnected to ground. This paper presents results of ultraviolet tests performed as part of the overall qualification program for cell assemblies using these coverglasses. The samples were exposed under vacuum at a controlled temperature to 5000 equivalent sun hours. Coverglass transmission curves and cell assembly current-voltage curves were measured before and after the test. Observed degradations were of the order of 1 percent more for conductively coated coverglasses than for coverglasses without conductive coatings.

Bass, J. A.↗

Statistical fatigue of graphite/epoxy angle-ply laminates in shear

A three-parameter fatigue and residual strength degradation model has been proposed to predict statistically the fatigue behavior of composite laminae under axial shear loadings. The fatigue behavior includes the fatigue life and the fatigue damage expressed in terms of the residual strength degradation. An experimental test program using graphite/epoxy /+ or - 45 deg/2s laminates has been conducted to generate statistically meaningful data in order to examine the validity of the theoretical model. It is shown that the correlation between the theoretical predictions and the test results on the statistical distributions of the fatigue life and the residual strength is excellent. Test results on the shear modulus degradation are also presented and discussed in detail in order to provide insight for the establishment of a shear modulus degradation model.

Yang, J. N.↗

Ultraviolet effects on conductive coated coverglasses

Experiments on the International Sun-Earth Explorer required that the outer surface of the spacecraft be conductive. For the solar panels this was accomplished by using solar cell coverglasses coated with indium-oxide and interconnected to ground. This paper presents results of ultraviolet tests performed as part of the overall qualification program for cell assemblies using these coverglasses. The samples were exposed under vacuum at a controlled temperature to 5000 equivalent sun hours. Coverglass transmission curves and cell assembly current-voltage curves were measured before and after the test. Observed degradations were of the order of 1 percent more for conductively coated coverglasses than for coverglasses without conductive coatings.

Bass, J. A.↗

Accelerated life testing and reliability of high K multilayer ceramic capacitors

The reliability of one lot of high K multilayer ceramic capacitors was evaluated using accelerated life testing. The degradation in insulation resistance was characterized as a function of voltage and temperature. The times to failure at a voltage-temperature stress conformed to a lognormal distribution with a standard deviation approximately 0.5.

Minford, W. J.↗

Reliability and engineering sciences area. Materials research: Single junction thin film

A test bench was designed and fabricated for the purpose of improving control of hot-spot test accuracy. Electrochemical corrosion research focused on corrosion mechanisms to which both crystalline and a-Si modules may be subjected in central station applications. A variety of cells and several designs were subjected to accelerated stress tests. Humiditiy degradation rates were determined and key electrochemical failure mechanisms were identified. Software was developed for the prediction of power loss resulting from open circuits in an array field of a-Si modules. Failure analysis was continued on the four ARCO Solar Genesis modules. The interactions of water on the silicon module was examined. An autocatalytic photooxidation model was proposed. The reliability and durability of bonding materials and electrical insulation were also studied.

Source record↗

Application of copper-carbon fiber composites to power semiconductor devices

Copper-carbon composite electrodes are used in a series of power semiconductor devices, i.e., resin molded diodes, button-type diodes, stud-type diodes, power modules, and integrated circuit igniter modules. The properties of these power semiconductor devices compare favorably with those conventional devices using Mo or W electrodes. In thermal fatigue tests, no degradation in the electrical and mechanical characteristics of these devices are observed. The new composite electrode with carbon fibers satisfies all of the major requirements for the electrodes in power semiconductor devices.

Kuniya, Keiichi↗

Thermal conductivity, electrical conductivity and specific heat of copper-carbon fiber composite

We have developed a new copper-carbon fiber composite which possesses properties of copper, i.e., excellent thermal and electrical conductivities, in combination with a property of carbon fiber, i.e., a small thermal expansion coefficient. The composite properties can be controlled by the amount, type and orientation of the carbon fibers they contain. Therefore, this composite is considered to be useful as an electrical material. The effects of volume and arrangement of fibers on the thermal conductivity, electrical conductivity and specific heat of the composite were studied. The results obtained were as follows: (1) The thermal and electrical conductivities of the composite became smaller as the volume of carbon fibers increased, and they were also influenced by the fiber arrangement. (2) The above conductivities could be calculated by careful application of the “rule of mixtures” for composites. (3) The specific heat of the composite was dependent not on the fiber arrangement but on the fiber volume. (4) In thermal fatigue tests, no degradation in electrical conductivity was observed.

Keiichi Kuniya↗

The effect of temperature cycling typical of low earth orbit satellites on thin films of YBa2Cu3O(7-x)

The refrigeration of superconductors in space poses a challenging problem. The problem could be less severe if superconducting materials would not have to be cooled when not in use. Thin films of the YBa2Cu3O(7-x) (YBCO) superconductor were subjected to thermal cycling, which was carried out to simulate a large number of eclipses of a low earth orbit satellite. Electrical measurements were performed to find the effect of the temperature cycling. Thin films of YBCO were formed by coevaporation of Y, BaF2, and Cu and postannealing in wet oxygen at 850 C for 3.5 h. The substrates used were (100) SrTiO3, polycrystalline alumina, and oxidized silicon; the last two have an evaporated zirconia layer. Processing and microstructure studies of these types of films have been published. THe zero resistance transition temperatures of the samples used in this study were 91, 82, and 86 K, respectively. The samples were characterized by four point probe electrical measurements as a function of temperature. The parameters measured were: the zero resistance transition temperature, the 10 to 90 percent transition width, and the room temperature resistance, normalized to that measured before temperature cycling. The results for two samples are presented. Each sample had a cumulative exposure. Cycling in atmospheric pressure nitrogen was performed at a rate of about 60 cycles per day, whereas in vacuum the rate was only about 10 cycles per day. The results indicate only little or no changes in the parameters measured. Degradation of superconducting thin films of YBCO has been reported due to storage in nitrogen. It is believed that the relatively good performance of films after temperature cycling is related to the fact that BaF2 was used as an evaporation source. The latest result on extended temperature cycling indicates significant degradation. Further tests of extended cycling will be carried out to provide additional data and to clarify this preliminary finding.

Mogro-Campero, A.↗

Effects of dust accumulation and removal on radiators surfaces on Mars

Tests were carried out to assess the impact of wind blown dust accumulation and abrasion on radiator surfaces on Mars. High emittance arc-textured copper and niobium-1 percent-zirconium samples were subjected to basaltic dust laden wind at Martian pressure (1000 Pa) at speeds varying from 19 to 97 m/s in the Martian Surface Wind Tunnel. The effect of accumulated dust was also observed by pre-dusting some of the samples before the test. Radiator degradation was determined by measuring the change in the emittance after dust was deposited and/or removed. The principle mode of degradation was abrasion. Arc textured Nb-1 percent-Zr proved to be more susceptible to degradation than Cu, and pre-dusting appeared to have lessened the abrasion.

Gaier, James R.↗

Effects of dust accumulation and removal on radiator surfaces on Mars

Tests were carried out to assess the impact of wind blown dust accumulation and abrasion on radiator surfaces on Mars. High emittance arc-textured copper and niobium-1 percent-zirconium samples were subjected to basaltic dust laden wind at Martian pressure (1000 Pa) at speeds varying from 19 to 97 m/s in the Martian Surface Wind Tunnel. The effect of accumulated dust was also observed by pre-dusting some of the samples before the test. Radiator degradation was determined by measuring the change in the emittance after dust was deposited and/or removed. The principle mode of degradation was abrasion. Arc textured Nb-1 percent-Zr proved to be more susceptible to degradation than Cu, and pre-dusting appeared to have lessened the abrasion.

Gaier, James R.↗

Design and performance oof space station photovoltaic radiators

The design and performance of the Space Station Freedom Photovoltaic (PV) Power Module Thermal Control System radiators is presented. The PV Radiator is of a single phase pumped loop design using liquid ammonia as the coolant. Key design features are described, including the base structure, deployment mechanism, radiator panels, and two independent coolant loops. The basis for a specific mass of 7.8 kg/sqm is discussed, and methods of lowering this number for future systems are briefly described. Key performance paramters are also addressed. A summary of test results and analysis is presented to illustrate the survivability of the radiator in the micrometeoroid and orbital debris environment. A design criterion of 95% probability of no penetration of both fluid loops over a 10 year period is shown to be met. Methods of increasing the radiator survivability even further are presented. Thermal performance is also discussed, including a comparison of modeling predictions with existing test results. Degradation in thermal performance due to exposure to atomic oxygen and ultraviolet radiation in the low Earth orbit environment is presented. The structural criteria to which the radiator is designed are also briefly addressed. Finally, potential design improvements are discussed.

White, K. Alan↗

Assessment of The Compatibility of Composite Materials With High-Test Hydrogen Peroxide

The compatibility of composite materials with high-test hydrogen peroxide (HTP) was assessed using various chemical and mechanical techniques. Methods included classical schemes combining concentration assay with accelerated aging by means of a heated water bath. Exothermic reactivity was observed using Isothermal Microcalorimetry. Mechanical Properties testing determined degradation of the composite material. Photoacoustic Infrared Spectroscopy was used to monitor chemical alteration of the resin matrix. Other materials were examined including some polymers and metals.

Gostowski, Rudy↗

Use of Cumulative Degradation Factor Prediction and Life Test Result of the Thruster Gimbal Assembly Actuator for the Dawn Flight Project

The Dawn Ion Propulsion System is the ninth project in NASA s Discovery Program. The Dawn spacecraft is being developed to enable the scientific investigation of the two heaviest main-belt asteroids, Vesta and Ceres. Dawn is the first mission to orbit two extraterrestrial bodies, and the first to orbit a main-belt asteroid. The mission is enabled by the onboard Ion Propulsion System (IPS) to provide the post-launch delta-V. The three Ion Engines of the IPS are mounted on Thruster Gimbal Assembly (TGA), with only one engine operating at a time for this 10-year mission. The three TGAs weigh 14.6 kg.

Lo, C. John↗

Thermal environment effects on strength and impact properties of boron-aluminum composites

Thermal effects on fracture strength and impact energy were studied in 50 volume percent unidirectional composites of 143 and 203 micron boron fibers in 6061 and 1100 aluminum matrices. For 6061 matrix composites, strength was maintained to approximately 400 C in the cyclic tests and higher than 400 C in the static tests. For the 1100 matrix composites, strength degradation appeared near 260 C after cycling and higher than 260 C in static heating. This composite strength degradation is explained by a fiber degradation mechanism resulting from a boron-aluminum interface reaction. The impact energy absorption degraded significantly only above 400 C for both matrix alloys. Thus, while impact loss for the 6061 composite correlates with the fiber strength loss, other energy absorption processes appear to extend the impact resistance of the 1100 matrix composites to temperatures beyond where its strength is degraded. Interrupted impact tests on as-received and thermally cycled composites define the range of load over which the fibers break in the impact event.

Grimes, H. H.↗

What is “First Ply Failure” in a Unidirectionally Loaded Quasi-Isotropic Composite (and does it exist)?

This study presents experimental results of unidirectional tension tests on quasi-isotropic laminates to observe so called “first ply failure” (FPF). The modulus of the laminates was measured throughout the test to observe any ply degradation. Quasi-isotropic (QI) laminates were tested since this is the most common layup sequence of a laminate in industry and FPF, if it exists to any practical extent, should be observed. The authors are unaware of any claim that only bi-axial loads are needed to cause FPF, thus uniaxial testing was performed since this is much simpler than bi-axial testing. Laminates can be engineered to cause anomalies (“knees” or abrupt change in modulus) in a stress-strain curve (such as sandwiching multiple 90° plies between a couple of 0° plies) but such laminates should never be used in practice. The search for FPF was examined in simple 8 ply QI laminates by stopping tension tests at various levels post predicted FPF and examining the specimen for “ply failure” and ascertaining its effect (if any) on the modulus of the laminate. The ultimate strength values were found for some specimens. Results showed that for 8 ply QI laminates, no FPF of note was found and challenges the whole notion of FPF and thus “progressive failure”.

First ply failure↗

Colloid thruster technology

A program is described for attaining control, reproducibility, and predictability of operation for the annular colloid emitter. A thruster of an improved design was used for a 1000 hour test. The thruster was operated with a neutralizer for 1023 hours at 15 kV with an average thrust of 25 micropound and specific impulse of 1160 sec. The performance was stable, and the beam was vectored periodically. The clean condition of the emitter edge at the end of the test coupled with no degradation in performance during the test indicated that the lifetime could be extrapolated by at least an order of magnitude over the test time.

Perel, J.↗

Test Vehicle Forebody Wake Effects on CPAS Parachutes

Parachute drag performance has been reconstructed for a large number of Capsule Parachute Assembly System (CPAS) flight tests. This allows for determining forebody wake effects indirectly through statistical means. When data are available in a "clean" wake, such as behind a slender test vehicle, the relative degradation in performance for other test vehicles can be computed as a Pressure Recovery Fraction (PRF). All four CPAS parachute types were evaluated: Forward Bay Cover Parachutes (FBCPs), Drogues, Pilots, and Mains. Many tests used the missile-shaped Parachute Compartment Drop Test Vehicle (PCDTV) to obtain data at high airspeeds. Other tests used the Orion "boilerplate" Parachute Test Vehicle (PTV) to evaluate parachute performance in a representative heatshield wake. Drag data from both vehicles are normalized to a "capsule" forebody equivalent for Orion simulations. A separate database of PCDTV-specific performance is maintained to accurately predict flight tests. Data are shared among analogous parachutes whenever possible to maximize statistical significance.

Ray, Eric S.↗