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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4

Spinoff 2015

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Source record↗

Pretreatment of lubricated surfaces with sputtered cadmium oxide

Cadmium oxide is used with a dry solid lubricant on a surface to improve wear resistance. The surface topography is first altered by photochemical etching to a predetermined pattern. The cadmium oxide is then sputtered onto the altered surface to form an intermediate layer to more tightly hold the dry lubricant, such as graphite.

Fusaro, Robert L.↗

Bearings use dry self-lubricating cage materials

Rolling element bearings in spacecraft mechanical systems use solid lubricant composites of polytetrafluoroethylene in the bearing cage which functions as the lubricant reservoir. The cage spaces the rolling elements equally and provides the lubricant at the bearing load-carrying surface.

Anderson, W. J.↗

Performance of MoS2 Coated Gears Exposed to Humid Air During Storage - (Study Number Two)

This work is a follow-on to a prior study on the effect of exposure to humid air on the durability of a molybdenum disulfide (MoS2) dry film lubricant on spur gears operated in vacuum, motivated by the James Webb Space Telescope (JWST) mission. In this study, MoS2 dry-lubricating films (DFLs) matching JWST specification were applied to test gears. The gear specimens were subjected to a brief run-in period in vacuum prior to their exposure to humid air, mimicking the sequence of mechanism checkout testing, exposure to air during integration, and then storage prior to launch. Test gear exposure times to humid air ranged from 1 hour to 326 days. After exposure, gear durability tests were conducted as an indication of film lifetime. MoS2 DFLs that were exposed to humid air (57% RH) exhibited reduced film durability relative to DFLs that were not exposed. On average, the exposed specimens demonstrated 75% shorter film life. The severity of the reduction in film durability did not correlate with the duration of exposure, i.e., long exposures to humid air were not more impactful to film durability than were short exposures.

MoS2↗

Fundamental aspects of polyimide dry film and composite lubrication: A review

The tribological properties of polyimide dry films and composites are reviewed. Friction coefficients, wear rates, transfer film characteristics, wear surface morphology, and possible wear mechanisms of several different polyimide films, polyimide-bonded solid lubricants, polyimide solid bodies, and polyimide composites are discussed. Such parameters as temperature, type of atmosphere, load, contact stress, and specimen configuration are investigated. Data from an accelerated test device (Pin-on-Disk) are compared to similar data obtained from an end use application test device (plain spherical bearing).

Fusaro, R. L.↗

Properties data for opening the Galileo's partially unfurled main antenna

An investigation was conducted into the friction and wear behavior of both unlubricated and dry-film-lubricated (Tiolube 460) titanium alloy (Ti-6Al-4V) in contact with an uncoated high-nickel-content superalloy (Inconel 718) both in vacuum and in air. The acquisition of friction and wear data for this sliding couple was motivated by the need for input data for the 'antenna stuck ribs model' effort to free Galileo's High Gain Antenna. The results of the investigation indicate that galling occurred in the unlubricated system in vacuum and that the coefficient of friction increased to 1.2. The abnormally high friction (1.45) was observed when relatively large wear debris clogged at the sliding interface. The coefficient of friction for the dry-film-lubricated system in vacuum is 0.04, while the value in air is 0.13. The endurance life of the dry-film lubricant is about three orders of magnitude greater in vacuum than in air. The worn surfaces of the dry-film-lubricated Ti-6Al-4V pin and Inconel 718 disk first run in humid air and then rerun in vacuum was completely different from that of the pin and disk run only in vacuum. When galling occurred in the humid-air and vacuum contact, coefficient of friction rose to 0.32 when sliding in humid air and to 1.4 when sliding in vacuum. The galling was accompanied by severe surface damage and extensive transfer of the Ti-6Al-4V to the Inconel 718, or vice versa. When spalling occurred in the dry-film-lubricated Ti-6Al-4V pin run only in vacuum, the coefficient of friction rose to 0.36 or greater. The wear damage caused by spalling can self-heal when rerun in vacuum - the coefficient of friction decreased to 0.05. The friction and wear data obtained can be used for the 'antenna stuck ribs model' effort to free Galileo's high gain antenna.

Miyoshi, Kazuhisa↗

Vitrolube NPI-1220 Solid Lubricant Performance After Ultraviolet and Salt Fog Test Exposures

Vitrolube NPI-1220 is a ceramic-bonded solid lubricant produced by National Process Industries, Inc. (NPI) that uses molybdenum disulfide (MoS2) and graphite as lubricating pigments. It is applied to many space flight components, including nickel-alloy and stainless-steel components. Various applications, such as the powered nut and bolt assemblies in the international space station (ISS) (Illi, 1999), the Space Launch System (SLS) sliding bellows, and the SLS ball strut tie-rod assembly (BSTRA) use Vitrolube. No engineering data exists regarding possible Vitrolube degradation after extended exposure to coastal environments encountered by flight hardware on test stands or launch pads. Such environments include ultraviolet (UV) ray, high humidity, and salt exposures. In this study, nickel-alloy disks coated with Vitrolube by NPI, are exposed to controlled UV ray and ‘salt fog’ environments in facilities at Marshall Space Flight Center (MSFC). The exposed disks are run in tribological pin-on-disk tests to quantify any difference in coating lubricity and/or wear compared to coated disks that were not exposed to those environments.

Tribology↗

Torque vs. induced load of A-286, and MP35N nuts and bolts with cadmium, dry film, and cetyl alcohol lubricants

Data for specific joint design, utilizing various combinations of bolt, nut and lubricants in typical structure of the shuttle booster rocket is obtained. Requirements of the structure performance criteria were to withstand temperatures of 260 C (500 F) and to provide a nut lubricant which would be compatible with sealants used in the joint. Cadmium plating and dry film lubricant meeting the requirements of MIL-L-8937 were the lubricants specified. In a follow up effort, cadmium plating and cetyl alcohol were further specified The materials for the bolt and nut combinations were MP35N and A-286. These materials demand a lubricant to be used to prevent galling of the thread when tightened and also to help reduce the scatter of clamping load in application.

Crispell, C.↗

International Space Station Powered Bolt Nut Anomaly and Failure Analysis Summary

A key mechanism used in the on-orbit assembly of the International Space Station (ISS) pressurized elements is the Common Berthing Mechanism (CBM). The mechanism that effects the structural connection of the CBM halves is the Powered Bolt Assembly. There are sixteen Powered Bolt Assemblies per CBM. The CBM has a bolt which engages a self aligning Powered Bolt Nut (PBN) on the mating interface; see Figure 1. The Powered Bolt Assemblies are preloaded to approximately 19 kilo pounds (KIPs) prior to pressurization of the CBM. The PBNs mentioned below, manufactured in 2009, will be used on ISS future missions. An on orbit functional failure of this hardware would be unacceptable and in some instances catastrophic due to the failure of modules to mate and seal the atmosphere, risking loss of crew and ISS functions. The manufacturing processes which create the PBNs need to be strictly controlled. Functional (torque vs. tension) acceptance test failures will be the result of processes not being strictly followed. Without the proper knowledge of thread tolerances, fabrication techniques, and dry film lubricant application processes, PBNs will be, and have been manufactured improperly. The knowledge gained from acceptance test failures and the resolution of those failures, thread fabrication techniques and thread dry film lubrication processes can be applied to many aerospace mechanisms to enhance their performance. Test data and manufactured PBN thread geometry will be discussed for both failed and successfully accepted PBNs.

Sievers, Daniel E.↗

International Space Station Powered Bolt Nut Anomaly and Failure Analysis Summary

A key mechanism used in the on-orbit assembly of the International Space Station (ISS) pressurized elements is the Common Berthing Mechanism. The mechanism that effects the structural connection of the Common Berthing Mechanism halves is the Powered Bolt Assembly. There are sixteen Powered Bolt Assemblies per Common Berthing Mechanism. The Common Berthing Mechanism has a bolt which engages a self aligning Powered Bolt Nut (PBN) on the mating interface (Figure 1). The Powered Bolt Assemblies are preloaded to approximately 84.5 kN (19000 lb) prior to pressurization of the CBM. The PBNs mentioned below, manufactured in 2009, will be used on ISS future missions. An on orbit functional failure of this hardware would be unacceptable and in some instances catastrophic due to the failure of modules to mate and seal the atmosphere, risking loss of crew and ISS functions. The manufacturing processes that create the PBNs need to be strictly controlled. Functional (torque vs. tension) acceptance test failures will be the result of processes not being strictly followed. Without the proper knowledge of thread tolerances, fabrication techniques, and dry film lubricant application processes, PBNs will be, and have been manufactured improperly. The knowledge gained from acceptance test failures and the resolution of those failures, thread fabrication techniques and thread dry film lubrication processes can be applied to many aerospace mechanisms to enhance their performance. Test data and manufactured PBN thread geometry will be discussed for both failed and successfully accepted PBNs.

Sievers, Daniel E.↗

Performance of MoS2 Coated Gears Exposed to Humid Air During Storage

The purpose of this work was to study the effect of exposure to humid air on the durability of a molybdenum disulfide dry film lubricant applied to spur test gears and subsequently tested in vacuum environment. This study was motivated by the James Webb Space Telescope (JWST) Mission. Some moving mechanical assembles of the JWST have been exposed to humid air during storage as a subassembly and after integration into a higher-level assembly. molybdenum disulfide dry film lubricant was applied to steel spur test gears and subsequently tested in vacuum environment. One-half of the gears had essentially zero time exposure to humid air prior to testing, and the other half were exposed to humid air of 57 percent relative humidity for exposure durations up to 77 days prior to testing. All tests were completed at the same constant torque and speed. On average, the film durability, as measured by the number of pinion revolutions, was shorter for gears exposed to humid air compared to those with zero exposure. For the unexposed gears, the durability ranged from 53,300 to 190,300 pinion revolutions with an average value of 100,200 and a median value of 83,500 revolutions. For the exposed gears, the durability ranged from 21,000 to 84,700 pinion revolutions with an average value of 64,900 and a median value of 68,800 revolutions. Using the unexposed gears as a baseline, the exposure reduced the average durability by 35 percent and the median value of durability by 18 percent. Red-brown coloration was noted on some of the gear teeth that had been exposed to humid air. The colored regions appeared as soon as 17 days after exposure to humid air. SEM inspections showed that at least some of these colored areas included material raised above the surrounding molybdenum disulfide film.

gear↗

A Study of Some Factors Affecting Rolling-Contact Fatigue Life

A series of investigations using the fatigue spin rig to study the effect of several factors contributing to rolling contact fatigue life is summarized. Ball specimens of 1/2 and 9/16 inch diameter were tested at maximum theoretical Hertz compressive stresses in the range of 600,000 to 750,000 psi. Life was found to vary inversely with the tenth power of stress. In forging fiber studies, a greater concentration of failures and poorer life were observed where the greatest angle of intersection between the fiber flow lines and the surface occurred. This effect was independent of alloy composition. Higher lubricant viscosity was found to increase fatigue life, Lubricants having the same viscosity but of different base stock produced wide differences in life that correlated with the pressure viscosity coefficient of the lubricant. Higher temperature produced lower fatigue life. Dry powder lubricants produced poor fatigue life at 450 F; failure appearance indicated that the lubricant particles probably acted as minute stress raisers. In metallographic studies, nonmetallic inclusions were found to have a deleterious effect on fatigue life the inclusion size, location, composition, and condition of the matrix being contributing factors; failures were by shear cracking in the subsurface zone of maximum shear stress and eventual propagation into a shallow surface spall. Vacuum melting improved fatigue life, although a general correlation between cleanliness and fatigue life was not found. Life results for ten different bearing materials are presented.

Carter, Thomas L.↗

Friction behavior of silicon in contact with titanium, nickel, silver and copper

Sliding friction experiments are conducted with the semiconductor silicon in contact with the metals titanium, nickel, copper, and silver. Sliding is on the (111) plane of single-crystal silicon in the 112 crystallographic direction both in dry and lubricated (mineral oil) sliding. The friction coefficient in dry sliding is controlled by adhesion and the surface chemical activity of the metal. The more active the metal the stronger the adhesion and the higher the friction. In lubricated sliding the lubricant absorbs to the surfaces and reduces the importance of metal chemical effects. In lubricated sliding, silicon ceases to behave in a brittle manner and undergoes plastic deformation under load.

Mishina, H.↗

Lubricant evaluation of the alpha and beta joints, phase 2

A research study was conducted to evaluate dry film lubrication of long life space components such as the alpha and beta joints of the Space Station. The problem addressed in the report pertains to the longevity of sputtered MoS2 or ion plated lead films in a rolling contact environment. A special technique was devised for the experiments, which incorporated a coated ball cyclically loaded against a flat plate. At fixed intervals the surface of the coating was photographed at 100X magnification. By computer scanning the photographs, the rate of coating loss was determined. Experimental variables include load and surface finish of the plate. A theory was developed to analyze the state of stress between ball and flat. The stress condition in the ball apparatus was related to the state of stress under rolling contact conditions. Based on the experiments life appeared to decrease with increasing load and increasing surface roughness. An ion plated lead film gave better life than a sputtered MoS2 film. However, by keeping the interfacial shear stress at a low level, adequate coating life was achieved for either coating. For the lead film, the critical stress was about 0.19 GPa (28 ksi). The study dealt only with mechanical wear. Before a coating is selected for a critical space application, other factors such as reaction with atomic oxygen must also be considered.

Kannel, J. W.↗

NASA interdisciplinary collaboration in tribology. A review of oxidational wear

An in-depth review of oxidational wear of metals is presented. Special emphasis is given to a description of the concept of oxidational wear and the formulation of an Oxidational Wear Theory. The parallelism between the formation of an oxide film for dry contact conditions and the formation of other surface films for a lubricated contact is discussed. The description of oxidational wear is prefaced with a unification of wear modes into two major classes of mild and severe wear including both lubricated and dry contacts. Oxidational wear of metals is a class of mild wear where protective oxide films are formed at real areas of contact and during the time of contact at temperataure T sub c. When the oxide reaches a critical thickness, frequently in the range of 1 to 3 microns, the oxide breaks up and eventually appears as a wear particle. These oxides are preferentially formed on plateaux which alternately carry the load as they reach their critical thickness and are removed. If the system is operated at elevated temperatures, thick oxides can form both out of contact and between the plateaux. Temperature is important in determining the structure of the oxide film present. Spinel oxide (Fe3O4) which forms above 300 C is more protective than the lower temperature rhomobohedral (alpha-Fe2O3) oxide which is abrasive. An Oxidational Wear Theory is derived using a modified Archard wear law expressed in terms of activation energy (Qp) and Arrhenius constant (Ap).

Quinn, T. F. J.↗

Detailed Design of a Magnetically-Geared Actuator for Use in Extremely Cold Lunar Environments

A magnetically-geared actuator is being developed for extremely cold space environments to avoid the wiring and significant efficiency penalty associated with heating grease-lubricated actuators as well as the stringent life and loading constraints imposed by dry film lubricated mechanical gears. This paper describes the detailed design of this actuator, including the impactful requirements, thermal analysis, bearing loads, electromagnetic analysis and the impact of tolerance stack up, and structural analysis.

space mechanisms↗

Detailed Design of a Magnetically-Geared Actuator for use in Extremely Cold Lunar Environments

A magnetically-geared actuator is being developed for extremely cold space environments to avoid the wiring and significant efficiency penalty associated with heating grease-lubricated actuators as well as the stringent life and loading constraints imposed by dry film lubricated mechanical gears. This paper describes the detailed design of this actuator, including the impactful requirements, thermal analysis, bearing loads, electromagnetic analysis and the impact of tolerance stack up, and structural analysis.

space mechanisms↗

Development and Manufacture of A Proof-of-Concept Magnetically-Geared Actuator for Use in Extremely Cold Lunar Environments

A magnetically-geared actuator is being developed for extremely cold space environments to avoid the wiring and significant efficiency penalty associated with heating grease-lubricated actuators as well as the stringent life and loading constraints imposed by dry film lubricated mechanical gears. This paper describes the lessons learned while designing, manufacturing, and assembling a proof-of-concept prototype similar to the preliminary design of the actuator.

lunar surface↗