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At least 73 records · Page 4

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NASA NTRS1983

Morphology of ductile metals eroded by a jet of spherical particles impinging at normal incidence

Scanning electron microscopy and energy-dispersive X-ray spectroscopy are used, together with surface profile measurements, in the present morphological study of the erosion of an aluminum alloy and copper by the normal impact of spherical glass erodent particles. The morphology of the damage pattern is a manifestation of the flow pattern of erodent particles, and yields insight into the mechanisms that may be active at different stages of erosion. The simultaneous appearance of radial cracks and concentric rings is reported, together with wave crests which contain an accumulation of metallic flakes. A preliminary analysis is advanced to explain the formation of the various damage patterns observed.

Veerabhadra Rao, P.↗

NASA NTRS1984

Microstructures Associated with Wear

High strain associated with metal wear is discussed and macroscopic and fine microscopic aspects are included. Mechanisms for the production of debris which include extrusion of microfurrows, adhesive transfer, and fragmentation are outlined. The structure of near surface deformation zones, a thin transfer layer, is examined. The similarity among the size of fine wear debris particles, the structure of the transfer layer, and large wear flakes is shown. Differences in microstructure associated with dry wear and lubricated wear are pointed out. Some parallels and differences for classic high strain deformation and wear microstructures are discussed.

Glaeser, W. A.↗

NASA NTRS1984

Effect of substrate chemical pretreatment on the tribological properties of graphite films

Rubbed films of natural flake Madagascar graphite were applied to ASTM A-355(D) steel with chemical surface pretreatments of zinc phosphate, gas nitride, salt nitride, sulfo-nitride, and with mechanical pretreatment (sandblasting). SAE 1045 steel pins were slid against these films using a pin-on-disk tribometer. The results indicate that two different lubricating mechanisms can occur. In the chemical surface pretreatment, the graphite can mix together to form a surface layer of the two constituents and this plasticity flowing layer provides the lubrication. The longest endurance lives and the lowest pin wear rates were obtained with this mechanism. In the other, surface topography appeared to control the mechanism. A rough surface was necessary to serve as a reservoir to supply the graphite to the flat metallic plateaus where it was sheared in very thin films between the plateaus and the sliding pin surface. For this mechanism, chemical pretreatment seemed to do little more than serve as a means for roughening the surface. Mean friction was not significantly influenced by chemical pretreatment, but surface roughness effects were observed.

Fusaro, R. L.↗

NASA NTRS1984

Rapidly Solidified Alloys Made by Chill Block Melt-spinning Processes

Chill block melt-spinning (CBMS) processes are used to make rapidly solidified microcrystalline and amorphous alloy ribbon, flakes, etc. Fundamentals of CBMS processes are discussed in light of recent advances. Special regard is given to ribbon geometric defects (edge serrations, surface asperities, etc.). Photomicrographs of CBMS ribbon solidification microstructures are used to compare local solidification rates, especially in the vicinity of ribbon defects.

Liebermann, H. H.↗

NASA NTRS1984

Erosion of iron-chromium alloys by glass particles

The material loss upon erosion was measured for several iron-chromium alloys. Two types of erodent material were used: spherical glass beads and sharp particles of crushed glass. For erosion with glass beads the erosion resistance (defined as the reciprocal of material loss rate) was linearly dependent on hardness. This is in accordance with the erosion behavior of pure metals, but contrary to the erosion behavior of alloys of constant composition that were subjected to different heat treatments. For erosion with crushed glass, however, no correlation existed between hardness and erosion resistance. Instead, the erosion resistance depended on alloy composition rather than on hardness and increased with the chromium content of the alloy. The difference in erosion behavior for the two types of erodent particles suggested that two different material removal mechanisms were involved. This was confirmed by SEM micrographs of the eroded surfaces, which showed that for erosion with glass beads the mechanism of material removal was deformation-induced flaking of surface layers, or peening, whereas for erosion with crushed glass it was cutting or chopping.

Salik, J.↗

NASA NTRS1985

Packaging's Contribution for the Effectiveness of the Space Station's Food Service Operation

Storage limitations will have a major effect on space station food service. For example: foods with low bulk density such as ice cream, bread, cake, standard type potato chips and other low density snacks, flaked cereals, etc., will exacerbate the problem of space limitations; package containers are inherently volume consuming and refuse creating; and the useful observation that the optimum package is no package at all leads to the tentative conclusion that the least amount of packaging per unit of food, consistent with storage, aesthetics, preservation, cleanliness, cost and disposal criteria, is the most practical food package for the space station. A series of trade offs may have to be made to arrive at the most appropriate package design for a particular type of food taking all the criteria into account. Some of these trade offs are: single serve vs. bulk; conventional oven vs. microwave oven; nonmetallic aseptically vs. non-aseptically packaged foods; and comparison of aseptic vs. nonaseptic food packages. The advantages and disadvantages are discussed.

Rausch, B. A.↗

NASA NTRS1984

Microstructures and properties of rapidly solidified alloys

The microstructure and properties of rapidly solidified aluminum alloys were researched. The effects of powder and flake chemistry and morphology and alternative consolidation processing parameters are being conducted. Samples of the powders being utilized were obtained for comprehensive metallurgical characterization. Seven aluminum alloys in the form of thin foils were studied by a variety of techniques including optical metallography, scanning electron microscope, and transmission electron microscope. Details of the microstructural characteristics are presented along with a discussion of the solidification process. A better understanding of the microstructure of the rapidly solidified aluminum alloys prepared by a variety of techniques such as roller quenching, the vacuum atomized procedure, ultrasonically atomized in inert atmospheres, and atomized in flue gas was provided.

Shechtman, D.↗

NASA NTRS1986

Laboratory experiments in a baroclinic annulus with heating and cooling on the horizontal boundaries

Experiments have been performed in a cylindrical annulus with horizontal temperature gradients imposed upon the horizontal boundaries and in which the vertical depth was smaller than the width of the annulus. Qualitative observations were made by the use of small, suspended, reflective flakes in the liquid (water). Four basic regimes of flow were observed: (1) axisymmetric flow, (2) deep cellular convection, (3) boundary layer convective rolls, and (4) baroclinic waves. In some cases there was a mix of baroclinic and convective instabilities present. As a 'mean' interior Richardson number was decreased from a value greater than unity to one less than zero, axisymmetric baroclinic instability of the Solberg type was never observed. Rather, the transition was from non-axisymmetric baroclinic waves, to a mix of baroclinic and convective instability, to irregular cellular convection.

Miller, T. L.↗

NASA NTRS1985

SSM atomic oxygen reactions on Kapton and silverized Teflon

Surface morphology studies using scanning electron microscopy on Kapton and Inconel silver coated Teflon material samples retrieved from the Solar Maximum Mission spacecraft revealed significant changes attributed to orbital atomic oxygen induced reactions. The Kapton recession observed on the aluminized Kapton material samples appeared equivalent in nature with that observed on previous Space Shuttle LEO missions. SSM Teflon taped material samples, coated on the back side with films of Inconel protected silver were observed degraded on both sides. Visibly severe reactions on the back side produced total blackening, generally restricted to areas of tape with a narrow direct view-factor of the external orbital environment. High magnification scanning electron microscope views provided evidence of near total silver reaction, flaking, and subsequent erosion of the underlying Teflon itself. Only three of the extensive S.E.M. photographs illustrating the basic reactions observed are included pending further detailed investigations.

Roger Linton↗

NASA NTRS1986

An evaluation of candidate oxidation resistant materials for space applications in LEO

Ground based testing of materials considered for polyimide (Kapton) solar array blanket protection and graphite-epoxy stroctural member protection was performed in an RF plasma asher. Protective coatings on Kapton from various commercial sources and from NASA Lewis Research Center were exposed to the air plasma; and mass loss per unit area was measured for each sample. All samples evaluated provided some protection to the underlying surface, but metal-oxide-fluoropolymer coatings provided the best protection by exhibiting very little degradation after 47 hr of asher exposure. Mica paint was evaluated as a protective coating for graphite-epoxy structural members. Mica appeared to be resistant to attack by atomic oxygen, but only offered limited protection as a paint. this is believed to be due to the paint vehicle ashing underneath the mica leaving unattached mica flakes lying on the surface. The protective coatings on Kapton evaluated so far are promising but further research on protection of graphite-epoxy support structures is needed.

Rutledge, Sharon↗

NASA NTRS1985

Thermal barrier coatings for the space shuttle main engine turbine blades

The Space Shuttle Main Engine (SSME) turbopump turbine blades experience extremely severe thermal shocks during start-up and shut-down. For instance, the high pressure fuel turbopump turbine which burns liquid hydrogen operates at approximately 1500 F, but is shut down fuel rich with turbine blades quenced in liquid hydrogen. This thermal shock is a major contributor to blade cracking. The same thermal shock cause the protective ZrO2 thermal barrier coatings to spall or flake off, leaving only the NiCrAlY bond coating which provides only a minimum thermal protection. The turbine blades are therefore life limited to about 3000 sec for want of a good thermal barrier. A suitable thermal barrier coating (TBC) is being developed for the SSME turbine blades. Various TBCs developed for the gas turbine engines were tested in a specially built turbine blade tester. This tester subjects the coated blades to thermal and pressure cycles similar to those during actual operation of the turbine. The coatings were applied using a plasma spraying techniques both under atmospheric conditions and in vacuum. Results are presented. In general vacuum plasma sprayed coatings performed much better than those sprayed under atmospheric conditions. A 50 to 50 blend of Cr2O3 and NiCrAlY, vacuum plasma sprayed on SSME turbopump turbine blades appear to provide significant improvements in coating durability and thermal protection.

Bhat, B. N.↗

NASA NTRS1989

Utilization of non-conventional systems for conversion of biomass to food components

The potential use of micro-algae in yielding useful macronutrients for the CELSS is investigated. Algal proteins were isolated and characterized from green algae (Scenedesmus obliquus) grown under controlled conditions. The RNA and DNA contents were determined, and methodology for reduction of the nucleic acid content to acceptable levels developed. Lipid extraction procedures using supercritical fluids were tailored to removal of undesirable lipids and pigments. Initial steps toward preparation of model foods for potential use in the CELSS were taken. The goal was to fabricate food products which contain isolated algal macronutrients such as proteins and lipids and also some components derived from higher plants including wheat flour, soy flour, potato powder (flakes), soy oil, and corn syrup.

Karel, M.↗

NASA NTRS1989

Comet ejection and dynamics of nonspherical dust particles and meteoroids

This paper generalizes the formalism for calculating the ejection velocity of meteoroids and dust from comets and the forces to which such objects are subject in interplanetary space, including the dust tail of comets. It is found that spheres have the smallest cross section of any geometrical figures of the same valume averaged over random orientations, so for a fixed volume and mass, both the ejection velocity and beta reaches a minimum for bodies of spherical shapes. Flakes in random orientation are ejected near 70 percent of the highest ejection velocity for any orientation. Needles in random orientation escape a comet at nearly 90 percent of their maximum velocities. Randomly oriented cylinders of finite thickness escape at lower velocities that are slightly closer to their maximum velocities. The average beta acting on spin-aligned, perfectly absorbing needles is more than half that acting on a sphere of the same material and radius.

Gustafson, Bo A. S.↗

NASA NTRS1990

The mechanical stability of polyimide films at high pH

Polyimide insulated electrical wire has been widely used in the aerospace industry in commercial, military, and to a lesser degree, general aviation aircraft since the early 1970s. Wiring failures linked to insulation damage have drawn much attention in the media and concerns have developed regarding the long term stability and safety of polyimide insulated electrical wire. The mechanical durability and chemical stability of polyimide insulated wire are affected by hydrolysis, notch propagation, wet and dry arc tracking, topcoat flaking, and degradation due to high pH fluids. Several polyimides were selected for evaluation for resistance to degradation by various aqueous alkaline solutions. The polyimides under evaluation include commercially available films such as KAPTON (tradename), APICAL (tradename), LARC-TPI, and UPILEX (tradename) R and S, as well as a number of experimental films prepared at NASA-Langley. Material properties investigated include viscosity, solubility, moisture absorption, glass transition temperature, dielectric constant, and mechanical properties before and after exposure to various conditions.

Croall, Catharine I.↗

NASA NTRS1991

On charging of snow particles in blizzard

The causes of the charge polarity on the blizzard, which consisted of fractured snow crystals and ice particles, were investigated. As a result, the charging phenomena showed that the characteristics of the blizzard are as follows: (1) In the case of the blizzard with snowfall, the fractured snow particles drifting near the surface of snow field (lower area: height 0.3 m) had positive charge, while those drifting at higher area (height 2 m) from the surface of snow field had negative charge. However, during the series of blizzards two kinds of particles positively and negatively charged were collected in equal amounts in a Faraday Cage. It may be considered that snow crystals with electrically neutral properties were separated into two kinds of snow flakes (charged positively and negatively) by destruction of the snow crystals. (2) In the case of the blizzard which consisted of irregularly formed ice drops (generated by peeling off the hardened snow field), the charge polarity of these ice drops salting over the snow field was particularly controlled by the crystallographic characteristics of the surface of the snow field hardened by the powerful wind pressure.

Shio, Hisashi↗

NASA NTRS1990

Atomic oxygen durability of solar concentrator materials for Space Station Freedom

The findings are reviewed of atomic oxygen exposure testing of candidate solar concentrator materials containing SiO2 and Al2O3 protective coatings for use on Space Station Freedom solar dynamic power modules. Both continuous and iterative atomic oxygen exposure tests were conducted. Iterative air plasma ashing resulted in larger specular reflectance decreases and solar absorptance increases than continuous ashing to the same fluence, and appears to provide a more severe environment than the continuous atomic oxygen exposure that would occur in the low Earth orbit environment. First generation concentrator fabrication techniques produced surface defects including scratches, macroscopic bumps, dendritic regions, porosity, haziness, and pin hole defects. Several of these defects appear to be preferential sites for atomic oxygen attack leading to erosive undercutting. Extensive undercutting and flaking of reflective and protective coatings were found to be promoted through an undercutting tearing propagation process. Atomic oxygen erosion processes and effects on optical performance is presented.

Degroh, Kim K.↗

NASA NTRS1992

Phase transformations in SrAl2Si2O8 glass

Bulk glass of SrAl2Si2O8 composition crystallized at temperatures below 1000 C into hexacelsian, a hexagonal phase which undergoes a reversible, rapid transformation to an orthorhombic phase at 758 C, and at higher temperatures crystallized as celsian, a monoclinic phase. The glass transition temperature and crystallization onset temperature were determined to be 883 C and 1086 C, respectively, from DSC at a heating rate of 20 C/min. Thermal expansion of the various phases and density and bend strengths of cold isostatically pressed glass powder bars, sintered at various temperatures, were measured. The kinetics of the hexacelsian-to-celsian transformation for SrAl2Si2O8 were studied. Hexacelsian flakes were isothermally heat treated at temperatures from 1025-1200 C for various times. Avrami plots were determined by quantitatively measuring the amount of monoclinic celsian formed at various times using x ray diffraction. The Avrami constant was determined to be 1.1, suggesting a diffusionless, one dimensional transformation mechanism. The activation energy was determined from an Arrhenius plot of 1n k vs. 1/T to be 125 kilocal/mole. This value is consistent with a mechanism which transforms the layered hexacelsian structure to a three dimensional framework celsian structure and involves the breaking of Si-O bonds.

Drummond, Charles H., III↗

NASA NTRS1992

Hybrid rocket fuel combustion and regression rate study

The objectives of this study are to develop hybrid fuels (1) with higher regression rates and reduced dependence on fuel grain geometry and (2) that maximize potential specific impulse using low-cost materials. A hybrid slab window motor system was developed to screen candidate fuels - their combustion behavior and regression rate. Combustion behavior diagnostics consisted of video and high speed motion pictures coverage. The mean fuel regression rates were determined by before and after measurements of the fuel slabs. The fuel for this initial investigation consisted of hydroxyl-terminated polybutadiene binder with coal and aluminum fillers. At low oxidizer flux levels (and corresponding fuel regression rates) the filled-binder fuels burn in a layered fashion, forming an aluminum containing binder/coal surface melt that, in turn, forms into filigrees or flakes that are stripped off by the crossflow. This melt process appears to diminish with increasing oxidizer flux level. Heat transfer by radiation is a significant contributor, producing the desired increase in magnitude and reduction in flow dependency (power law exponent) of the fuel regression rate.

Strand, L. D.↗