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DOE OSTI2020

Fire, dust, air and water: Improving aerosol biogeochemistry interactions in ACME. Final report

Aerosol-biogeochemistry interactions will have important consequences for human health, ecosystem services, and climate feedbacks over the next several decades. In this proposal we seek to link how human activities on land, including direct industrial emissions and landscape fires, impact the atmosphere and the biogeochemistry of the ocean and land. Our overall goal was to complement existing work at DOE labs to improve the capability and performance of the E3SM model in short-term, high-resolution projections of climate. Projections of ocean uptake of anthropogenic carbon are highly dependent on the details of the ocean physical and biogeochemistry parameterizations. Potentially equally important are the estimates of increases in iron and soluble nitrogen deposition in aerosols to the open ocean, but there are substantial uncertainties in these feedbacks. The E3SM land model simulates natural and anthropogenic fires, but improvement is needed to more accurately simulate fire responses to climate variability as well as fire contributions to terrestrial climate feedbacks. This proposal addressed four of the six priorities within the ACME/E3SM call by improving the representation of fire, industrial combustion sources, and desert dust and adding iron and soluble iron to the atmospheric chemistry (1). Our work focused on improving ocean biogeochemistry and the response of the oceans to anthropogenic atmospheric iron and nitrogen (3). We also improved the representation of land disturbance on fires and fire mediated carbon cycle feedbacks in the land model (4). Finally we had planned to couple the land, atmosphere and ocean biogeochemical systems (6) and explore how this coupling changes the feedbacks in the climate system. Our work under this proposal was separated into the following 5 tasks: i) improve representation of fire dynamics in both boreal and tropical ecosystems, ii) improve estimates of industrial emissions of iron and phosphorus, iii) improve representation of atmospheric iron, phosphorus and nitrogen transport, chemistry and deposition, iv) improve representation of iron, phosphorus and nitrogen deposition impacts on ocean biogeochemistry, and v) couple emissions into atmosphere, to deposition onto land and ocean biogeochemistry. For all 5 tasks, we conducted offline experiments of the historical period to enable comparison with available aerosol and land surface observations. We had planned to conduct fully coupled simulations, however, these will be conducted as part of the coupling in version 3 and 4 of the E3SM model, and thus have not been completed.

54 ENVIRONMENTAL SCIENCES↗

NASA NTRS1992

Physical properties of Deucalionis, Eos, Xanthe-type units in the central equatorial region of Mars

Classification and mapping of surficial units in the central equatorial region of Mars (30 degrees N to 20 degrees S, 57 degrees E to 75 degrees W) using enhanced color images and Mars Consortium data, identified three distinct, high albedo, relatively red surficial units in regions with intermediate to high thermal inertias. These units have distinctive properties and morphologies, occur in different, well-defined areas, and show different seasonal and secular patterns of albedo change. Deucalionis units occupy the classical albedo area of Deucalionis Regio, south of Meridiani Sinus and Sabaeus Sinus, and adjacent areas. Eos forms a bright band that separates the dark, relatively blue Meridiani-type units that dominate the southern part of the study area from intermediate albedo, relatively red Oxia units common in the north. Xanthe forms moderately bright, relatively red, Type 1B crater-streaks and uniform sheet-deposits in and adjacent to parts of Chryse Planitia, including the Viking 1 landing site. Xanthe is always associated with Oxia deposits, and has significantly lower albedos than the Eos materials, which it can be confused with.

Strickland, Edwin L., III↗

NASA NTRS2016

Tsunami Waves Extensively Resurfaced the Shorelines of an Early Martian Ocean

Viking image-based mapping of a widespread deposit covering most of the northern low-lands of Mars led to the proposal by Parker et al. that the deposit represents the vestiges of an enormous ocean that existed approx. 3.4 Ga. Later identified as the Vastitas Borealis Formation, the latest geologic map of Mars identifies this deposit as the Late Hesperian lowland unit (lHl). This deposit is typically bounded by raised lobate margins. In addition, some margins have associated rille channels, which could have been produced sub-aerially by the back-wash of high-energy tsunami waves. Radar-sounding data indicate that the deposit is ice-rich. However, until now, the lack of wave-cut shoreline features and the presence of lobate margins have remained an im-pediment to the acceptance of the paleo-ocean hypothesis.

Vastitas Borealis Formation↗

NASA NTRS1997

There's Iron in Them Thar Hills: A Geologic Look at the Aristarchus Plateau as a Potential Landing Site for Human Lunar Return

Lunar pyroclastic deposits are unique among lunar soils. Composed of very fine grained glass beads rich in Fe, Ti and Mg they yield unique spectral signatures. From the spectra two major classes and five subclasses of lunar dark mantling deposits have been identified. Recent work by me and others has shown that the larger regional deposits are more numerous, extensive, thicker, and widely distributed than previously thought, leading us to suggest that they would make ideal resource feedstock for future lunar surface activities. Returned sample studies and the recently collected Galileo and Clementine data also corroborate these findings. Recent planning for return to the Moon indicates that large cost savings can result from using locally produced oxygen, and recent JSC laboratory results indicate that iron-rich pyroclastic dark mantling deposits may be the richest oxygen resource on the Moon. My earlier work demonstrated that instead of using regolith, bulk lunar pyroclastic deposits are better suited for beneficiation as they are thick (lO's m's), unconsolidated, fine-grained deposits. In addition, the lack of rocks and boulders and the typically flat to gently rolling terrain will facilitate their mining and processing. In preparation for the Human Lunar Return (HLR) I have characterized the Aristarchus Plateau (24 deg. N 52 deg. W) as a potential landing site for an in-situ resource utilization (ISRU) demonstration. The geologic diversity and large volume of Fe-rich pyroclastic material present at the Aristarchus site make it an ideal target for extracting O2, H2 and halogens. This paper (1) describes the current understanding of the geology of Aristarchus plateau; (2) describes the resource potential of the Aristarchus plateau; and (3) presents several candidate landing sites on the plateau for future lunar activities.

Coombs, Cassandra R.↗

NASA NTRS1990

Measurements of tropospheric nitric acid over the western United States and northeastern Pacific Ocean

HNO3 measurements obtained in the free troposphere (FT) and boundary layer (BL) over the western U.S. and the NE Pacific during the NASA Global Tropospheric Experiment Chemical Instrumentation Test and Evaluation 2 (CITE 2) program in summer 1986 are reported. The CITE 2 HNO3 instruments and flight protocols are described, and the results are presented in tables and graphs. Over the ocean, the average HNO3 mixing ratios were found to be 108 parts per trillion by volume (pptv) in the FT and 62 pptv in the BL, suggesting removal of HNO3 from the BL by dry deposition. The corresponding values over land were 61 pptv for the FT and 767 pptv for the BL, and the horizontal distribution of BL HNO3 indicated an anthropogenic origin.

Lebel, P. J.↗

NASA NTRS2001

Orbital Imaging Radar and the Search for Water on Mars

The surface of Mars has been modified by a range of geologic processes, and many regions are mantled by varying depths of wind-blown dust, volcanic ash, and fluvially deposited or other water-lain sediments. We are proposing an orbital mission carrying a synthetic aperture radar (SAR) that can penetrate a significant depth of overlying material to reveal the detailed geomorphology as it relates to the changing fluvial, eolian, volcanic, and cratering history of Mars. Moreover, the data to be returned are of direct relevance to the search for past and present occurrences of liquid water, life, changing martian climate, and geologic history (e.g., origin of the northern plains, mechanisms for past and possible present valley formation, and genesis of widespread mantling deposits), the validation of potential landing sites for rover safety, and evaluation of sub-surface accessibility for drilling.

Campbell, B. A.↗

NASA NTRS1994

Mars Pathfinder and the exploration of southern Amazonis Planitia

The southern region of Amazonis Planitia provides a variety of target terrains for a roving vehicle such as the Mars Pathfinder Mission. A landing site is proposed at 4 deg N latitude 162 deg W longitude. This area has a reference altitude of between 0 and -1 km and consists of relatively smooth Amazonian-aged deposits within the entire 100 x 200 km landing ellipse. The proposed landing site is within the Upper Member Medusae Fossae Formation deposits (Amu) and near the boundary with Middle Member Medusae Fossae Formation deposits (Amm) and Member 1 Arcadia Formation plains (Aa(sub 1)). Slightly further afield are 107-km-diameter Nicholson crater, its ejecta deposits, and knobby terrain of proposed Hesperian age (HNu). Depending on the exact landing site of the spacecraft and the traverse distance of the rover, these materials also may be sampled.

Barlow, Nadine G.↗

DOE OSTI2022

Sputter deposition of high electrical resistivity Au-Ta alloy coatings on rotating substrates

Sputter deposition of gold-tantalum alloy coatings is a key process for manufacturing hohlraums for magnetically-assisted inertial confinement fusion implosions. In this report we describe direct current magnetron sputter deposition of ~ 10 - μ~ 10 - μm-thick films of Au-80 at.% Ta onto rotating sphero-cylindrical hohlraum and planar Si witness substrates. Emphasis is given to how film microstructure and properties are affected by main deposition parameters, including argon working gas pressure, substrate bias, and the source composition (a single alloyed target compared to co-sputtering from two elemental targets). Experimental findings are correlated with distributions of landing energies and incident angles of depositing species calculated by Monte Carlo simulations of ballistic collisions and gas phase atomic transport. Deposition conditions characterized by low energetics of depositing species favor the formation of a β-Ta-like phase. Implications of these results to hohlraum fabrication are discussed.

36 MATERIALS SCIENCE↗

NASA NTRSDate not supplied

Artemis Internal Science Team Update: Deployed Payloads

Artemis will reestablish human presence on the Moon and lead to a new era of scientific discovery and exploration. Led by the National Aeronautics and Space Administration (NASA), the Artemis effort includes a collaboration of space agencies and companies from around the world [1]. In support of Artemis, a cross-disciplinary effort of science, engineering, operations, and human factors personnel is currently developing the best methods, facilities, and field locations to test hardware, train astronauts, and evaluate concepts of operations. This abstract, as part of the Artemis Internal Science Team (AIST) [2], provides an update to NASA’s plans for the solicitation, development, and operations of deployed surface payloads. In calendar year 2023, NASA’s Science Mission Directorate will solicit proposals for instruments to be deployed by crew on the surface of the Moon (Fig. 1), beginning with Artemis III [3]. The Artemis III mission will land in the south polar region of the Moon, within 6º of latitude from the south pole, in the vicinity of both persistently illuminated and permanently shadowed areas of the Moon, with potential access to surface-accessible volatile deposits [4]. Several of the proposed landing regions are located among some of the oldest parts of the Moon, and together with the permanently shadowed regions, provide the opportunity to learn about the history of the Moon through previously unexplored lunar regions [5]. Deployed payloads will be a critical part of a notional program that captures the highest-priority science for Artemis III and provides the greatest feedforward to follow-on missions and the build-up to the Artemis Base Camp

R. C. Weber↗

NASA NTRS2000

After the Mars Polar Lander: Where to Next?

The recent loss of the Mars Polar Lander (MPL) mission represents a serious setback to Mars science and exploration. Targeted to land on the Martian south polar layered deposits at 76 degrees south latitude and 195 degrees west longitude, it would have been the first mission to study the geology, atmospheric environment, and volatiles at a high-latitude landing site. Since the conception of the MPL mission, a Mars exploration strategy has emerged which focuses on Climate, Resources and Life, with the behavior and history of water as the unifying theme. A successful MPL mission would have made significant contributions towards these goals, particularly in understanding the distribution and behavior of near-surface water, and the nature and climate history of the south polar layered deposits. Unfortunately, due to concerns regarding the design of the MPL spacecraft, the rarity of direct trajectories that enable high-latitude landings, and funding, an exact reflight of MPL is not feasible within the present planning horizon. However, there remains significant interest in recapturing the scientific goals of the MPL mission. The following is a discussion of scientific and strategic issues relevant to planning the next polar lander mission, and beyond.

Paige, D. A.↗

NASA NTRS1973

Release of Bacterial Spores from the Inner Walls of a Stainless Steel Cup Subjected to Thermal Stresses and Mechanical Shock

The release and fallout of particulates from surfaces afforded thermal or impact stress is of concern for control of contamination of Mars from planetary landing vehicles. A metal vessel contaminated by aerosols of spores was used as a model system and the fallout of spores as affected by various mechanisms was examined. Thermal stresses simulating those expected on the Mars lander dislodged approximately .01% of the aerosol deposited surface burden as did a landing shock of 8 to 10G deceleration. Spores imprinted by finger or swab contact yielded similar results. In all cases where repeated cycling of temperature, motion, or shock were employed the majority of fallout occurred in the first cycle. Particles released from the surface were predominantly in the size range 1 to 5 microns.

Wolochow, H.↗

DOE OSTI2024

Mobility Selective Ion Soft-Landing and Characterization Enabled Using Structures for Lossless Ion Manipulation

In this study, while conventional ion-soft landing uses the mass-to-charge (m/z) ratio to achieve molecular selection for deposition, here we demonstrate the use of Structures for Lossless Ion Manipulation (SLIM) for mobility-based ion selection and deposition. The dynamic rerouting capabilities of SLIM were leveraged to enable the rerouting of a selected range of mobilities to a different SLIM path (rather than MS) that terminated at a deposition surface. A selected mobility range from a phosphazene ion mixture was rerouted and deposited with a current pulse (~150 pA) resembling its mobility peak. In addition, from a mixture of tetra-alkyl ammonium (TAA) ions containing chain lengths of C5–C8, selected chains (C6, C7) were collected on a surface, reconstituted into solution-phase, and subsequently analyzed with a SLIM-qToF to obtain an IMS/MS spectrum, confirming the identity of the selected species. Further, this method was used to characterize triply charged tungsten-polyoxometalate anions, PW 12 O 40 3– (WPOM). The arrival time distribution of the IMS/MS showed multiple peaks associated with the triply charged anion (PW 12 O 40 3– ), of which a selected ATD was deposited and imaged using TEM. Additionally, the identity of the deposited WPOM was ascertained using energy-dispersive (EDS) spectroscopy. Further, we present theory and computations that reveal ion landing energies, the ability to modulate the energies, and deposition spot sizes.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1993

Remote identification of a gravel laden Pleistocene river bed

The abundance of gravel deposits is well known in certain areas across the Gulf of Mexico coastal plain, including lands within several National Forests. These Pleistocene gravels were deposited following periods of glacial buildup when ocean levels were down and the main river channels had cut deep gorges, leaving the subsidiary streams with increased gradients to reach the main channels. During the warm interglacial periods that followed each glaciation, melting ice brought heavy rainfall and torrents of runoff carrying huge sediment loads that separated into gravel banks below these steeper reaches where abraiding streams, developed. As the oceans rose again, filling in the main channels, these abraiding areas were gradually flattened and covered over by progressively finer material. Older terraces were uplifted by tectonic movements associated with the Gulf Coastal Plain, and the subsequent erosional processes gradually brought the gravels closer to the surface. The study area is located on the Kisatchie National Forest, in central Louisiana, near Alexandria. Details of the full study have been discussed elsewhere. The nearest source of chert is in the Ouachita Mountains located to the northeast. The Ouachita River flows south, out of these mountains, and in Pleistocene times probably carried these chert gravels into the vicinity of the present day Little River Basin which lies along the eastern boundary of the National Forest. Current day drainages cross the National Forest from west to east, emptying into the Little River on the east side. However, a north-south oriented ridge of hills along the west side of the Forest appears to be a recent uplift associated with the hinge line of the Mississippi River depositional basin further to the east, and 800,000 years ago, when these gravels were first deposited during the Williana interglacial period, the streams probably flowed east to west, from the Little River basin to the Red River basin on the west side of the Forest. Within the National Forest and north of Alexandria, along Fish Creek, and east and west of an area known as Breezy Hill, exist several small, worked out gravel pits on privately owned blocks of land, formerly used by the state and county road departments. The pattern presented by these pits gives the impression of a series of north-south drainages lacing through the Forest, probable tributaries to Fish Creek which flows south of east from the west side of the Forest to empty into the Little River. Because of this predominant north-south pattern, no consideration was given to areas between these drainages during early gravel exploration efforts.

Scholen, Douglas E.↗

NASA NTRS1992

Estimating Lunar Pyroclastic Deposit Depth from Imaging Radar Data: Applications to Lunar Resource Assessment

Lunar pyroclastic deposits represent one of the primary anticipated sources of raw materials for future human settlements. These deposits are fine-grained volcanic debris layers produced by explosive volcanism contemporaneous with the early stage of mare infilling. There are several large regional pyroclastic units on the Moon (for example, the Aristarchus Plateau, Rima Bode, and Sulpicius Gallus formations), and numerous localized examples, which often occur as dark-halo deposits around endogenic craters (such as in the floor of Alphonsus Crater). Several regional pyroclastic deposits were studied with spectral reflectance techniques: the Aristarchus Plateau materials were found to be a relatively homogeneous blanket of iron-rich glasses. One such deposit was sampled at the Apollo 17 landing site, and was found to have ferrous oxide and titanium dioxide contents of 12 percent and 5 percent, respectively. While the areal extent of these deposits is relatively well defined from orbital photographs, their depths have been constrained only by a few studies of partially filled impact craters and by imaging radar data. A model for radar backscatter from mantled units applicable to both 70-cm and 12.6-cm wavelength radar data is presented. Depth estimates from such radar observations may be useful in planning future utilization of lunar pyroclastic deposits.

Campbell, B. A.↗

NASA NTRS2003

Meridiani Planum Hematite Deposit: Potential for Preservation of Microfossils

Christensen et al., using data from the Mars Global Surveyor Thermal Emission Spectrometer (TES), have identified gray crystalline hematite in a 350 km by 750 km region near Meridiani Planum. The deposit corresponds closely to the low-albedo highlands unit sm, mapped as a wind-eroded, ancient, subaqueous sedimentary deposit. Christensen et al. interpreted the Meridiani Planum deposit to be an in-place, rock-stratigraphic sedimentary unit characterized by smooth, friable layers composed primarily of basaltic sediments with approximately 10 to 15% crystalline gray hematite. The Meridiani Planum hematite deposit has recently been designated as the prime landing site for one of the two Mars Exploration Rover (MER) spacecraft. The MER landings are scheduled for January, 2004. Christensen et al. discussed five possible mechanisms for the formation of this deposit: direct precipitation from standing, oxygenated, Fe-rich water; precipitation from Fe-rich hydrothermal fluids; low-temperature dissolution and precipitation through mobile groundwater leaching; surface weathering and coatings; thermal oxidation of magnetite-rich lavas. Four of these mechanisms involve the interactions of rock with water, and thus have implications in the search for evidence of microbial life.

C C Allen↗

DOE OSTI2021

Gold-tantalum alloy films deposited by high-density-plasma magnetron sputtering

Gold-tantalum alloy films are of interest for biomedical and magnetically-assisted inertial confinement fusion applications. Here, we systematically study the effects of substrate tilt (0°–80°) and negative substrate bias (0–100 V) on properties of ≲3-μm-thick films deposited by high-power impulse magnetron sputtering (HiPIMS) from a Au–Ta alloy target (with 80 at. % of Ta). Results reveal that, for all the substrate bias values studied, an increase in substrate tilt leads to a monotonic decrease in film thickness, density, residual compressive stress, and electrical conductivity. Larger substrate bias favors the formation of a body-centered cubic phase, with films exhibiting lower column tilt and higher density, electrical conductivity, and residual compressive stress. Furthermore, these changes are attributed to metal atom ionization effects, based on the lack of correlation with distributions of landing energies and incident angles of depositing species as calculated by Monte Carlo simulations of ballistic collisions and gas phase atomic transport. By varying substrate tilt and bias in HiPIMS deposition, properties of Au–Ta alloy films can be controlled in a very wide range, including residual stress from –2 to +0.5 GPa, density from 12 to 17 g/cm 3 , and the electrical resistivity from 50 to 4500 μΩ cm, enabling optimum deposition conditions to be selected for specific applications.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Direct functionalization of C-H bonds by electrophilic anions

Bond formation between two of the most inert molecules, alkanes and [B12X12]2- (X = Cl, Br), is performed in a two step process. Fragmentation of [B12X12]2- in the gas phase generates highly reactive [B12X11]- ions which spontaneously react with alkanes. The reaction mechanism was investigated using tandem mass spectrometry and gas-phase vibrational spectroscopy combined with electronic structure calculations. This effort revealed the unprecedented and counterintuitive electrophilic substitution of a proton in an alkane by a negatively charged ion resulting in a B-C bond formation. The product is a dianionic [B12X11CnH2n+1]2- species, in which H+ is electrostatically bound to the dianion. High flux ion soft-landing was performed to co-deposit [B12X11]- and complex organic molecules (phthalates) in thin layers on surfaces. Molecular structure analysis of the product films revealed that C-H functionalization by [B12X11]- occured in the presence of other more reactive functional groups. This observation demonstrates the utility of highly reactive fragment ions for defined bond formation processes and may pave the way to the use of gas phase ion chemistry for chemical synthesis in the condensed phase.

Warneke, Jonas↗

NASA NTRS1983

Mapping project on land use changes in the carboniferous region of Santa Catarina

The utilization of remote sensing data for monitoring land use changes by means of digital image analysis is described. The following data were utilized: LANDSAT data from September 4, 1975, April 24, 1978, and September 8, 1981; LANDSAT paper photography data; area IV color photographs; IBGE topography maps, and auxiliary data about the Brazilian state of Santa Catarina. Three kinds of analyses of digital images were carried out. The project identified and mapped major classes of land use areas including urban areas, coal deposits, agricultural areas, forests, lakes, and flood plains. Five areas directly affected by coal exploration southeast of Santa Catarina are identified and described. In addition, the classification system used for organizing data about land cover in a hierarchical arrangement is presented. The project made use of two remote sensing data sources: data of MSS spectral (Mulitspectral Scanner System)/LANDSAT on a scale of 1:100,000 with approximately 80 m resolution, and infrared color aerial photographs on a scale of 1:45,000 with approximately 5 m resolution. Therefore, the classification system included three levels, two selected to be compatible with aerial photography data and the third to conform to the resolution of MSS/LANDSAT.

Valeriano, D. D.↗