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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4

Nickel-based superalloy single crystals fabricated via electron beam melting

Additive manufacturing technologies have emerged as potential disruptive processes whose possible impacts range from supply chain logistics, prototyping, and novel materials synthesis. Numerous works illustrate the ability to control mi- crostructure in fusion based processes and a few recent authors have even produced single crystals. However, a number of open questions remain regarding the process window which enables printing of single crystals. Furthermore, it has been observed that these additively manufactured single crystals exhibit a preferred $\langle$011$\rangle$ secondary orientation. In this work we investigate fabrication conditions which enable printing of single crystals via electron beam melting. A space filling design of experiments is utilized to efficiently explore the fabrication space. Single crystals were success- fully obtained using both commercially available powders and custom melt alloys. Microstructures obtained via these exploratory experiments exhibited a continuum of columnar structures ranging from weakly textured polycrystals, near single crystal, and fully single crystalline material. Complex geometry experiments are performed to study the grain selection mechanism. We find that the grain selection mechanism is independent of the bulk scale geometry and must therefore by driven by local heat transfer and solidification dynamics. Furthermore, grain selection is shown to be driven by competing driving forces; one which prefers epitaxial growth and another which is driven by the imposed scan pattern geometry. Finally, a mechanism is proposed for the anomalous secondary orientation preference.

36 MATERIALS SCIENCE↗

A comparative study of solute trapping in Fe-(33–45 at%) Cu alloys manufactured by laser directed energy deposition

The high cooling rates in laser directed energy deposition (DED-LB) of alloys lead to substantial amounts of solute trapping as solute atoms cannot diffuse away from the solid/liquid interface before it advances. In some concentrated alloys, this results in supersaturated solid phases that form nanoscale hierarchical microstructures when the solute atoms precipitate out during reheating from subsequent laser passes. We choose the Iron-Copper (Fe-Cu) binary alloy as model system as it is chemically homogeneous in the liquid phase and has negligible solid solubility at room temperature. Two alloys with nominal compositions in atomic (at.) %, Fe67Cu33 and Fe55Cu45, were manufactured using DED-LB. Scanning transmission electron microscopy (STEM), energy dispersive spectroscopy (EDS) and wavelength dispersive spectroscopy (WDS) were used to characterize the nanostructures and heterogeneous chemical compositions. A non-equilibrium solute partitioning model was used to compute the supersaturated chemistries of the constituent phases and validated with experimentally measured compositions. The measured phase compositions of the two alloys were very similar, at roughly 12 at.% Cu and 4 at.% Fe in the α(bcc)-Fe and ε(fcc)-Cu phases respectively, despite having different processing parameters and mechanical behavior. This indicates that the total thermal history, that depends on both the processing parameters and laser scan pattern, plays a stronger role on the final microstructure evolution than just the initial quantity of trapped solute. In addition, we find that current non-equilibrium solute partitioning models applied on the continuum scale fall short of predicting accurate quantitative phase compositions in concentrated alloys, although the qualitative trends are captured correctly.

36 MATERIALS SCIENCE↗

Microstructure and properties of additively manufactured Al–Ce–Mg alloys

Additive manufacturing of aluminum alloys is largely dominated by a near-eutectic Al-Si compositions, which are highly weldable, but have mechanical properties that are not competitive with conventional wrought Al alloys. In addition, there is a need for new Al alloys with improved high temperature properties and thermal stability for applications in the automotive and aerospace fields. In this work, we considered laser powder bed fusion additive manufacturing of two alloys in the Al–Ce–Mg system, designed as near-eutectic (Al–11Ce–7Mg) and hyper-eutectic (Al–15Ce–9Mg) compositions with respect to the binary L → Al + Al 11 Ce eutectic reaction. The addition of magnesium is used to promote solid solution strengthening. A custom laser scan pattern was used to reduce the formation of keyhole porosity, which was caused by excessive vaporization due to the high vapor pressure of magnesium. The microstructure and tensile mechanical properties of the alloys were characterized in the as-fabricated condition and following hot isostatic pressing. The two alloys exhibit significant variations in solidification structure morphology. These variations in non-equilibrium solidification structure were rationalized using a combination of thermodynamic and thermal modeling. Both alloys showed higher yield strength than AM Al-10Si-Mg for temperatures up to 350 °C and better strength retention at elevated temperatures than additively manufactured Scalmaloy.

36 MATERIALS SCIENCE↗

Imaging Enhanced Simulation Validation for Directed Energy Deposition Additive Manufacturing (Final CRADA Report – NFE-22-09107)

Directed Energy Deposition (DED) is a welding-based metal Additive Manufacturing (AM) process that relies on the programmed rastering of an electric arc or laser induced weld pool to construct a component in a layerwise fashion. The induced complex thermal field and uneven thermal contraction depends on the printed geometry and scan pattern, and as such, accumulated residual stresses and distortions are complex and difficult to predict. Several prior works have resulted in tools to combat this issue; ANSYS has developed a thermoplastic simulation package targeting DED AM, and ORNL has developed an in-situ imaging sensor package ‘Stereo Correlated Optical and Pyrometric System’ (SCOPS) that can spatially monitor temperature and full field strain. In this CRADA, these tools are compared in order to validate the results and complimentarily address the weaknesses in each other.

36 MATERIALS SCIENCE↗

Femtosecond Laser Additive Manufacturing of Multi-Material Layered Structures

Laser additive manufacturing (LAM) of a multi-material multi-layer structure was investigated using femtosecond fiber lasers. A thin layer of yttria-stabilized zirconia (YSZ) and a Ni–YSZ layer were additively manufactured to form the electrolyte and anode support of a solid oxide fuel cell (SOFC). A lanthanum strontium manganite (LSM) layer was then added to form a basic three layer cell. This single step process eliminates the need for binders and post treatment. Parameters including laser power, scan speed, scan pattern, and hatching space were systematically evaluated to obtain optimal density and porosity. This is the first report to build a complete and functional fuel cell by using the LAM approach.

36 MATERIALS SCIENCE↗

3D Printing with Mixed Powders of Boron Carbide and Al Alloy

Laser additive manufacturing with mixed powders of boron carbide and aluminum alloy is investigated. Parameters such as laser power, scan speed, scan pattern, and hatching space are systematically evaluated and optimized to obtain the desired density and porosity. These results show that the AM part contains 20 wt% boron carbide and 80 wt% aluminum alloy, which are well mixed and synthesized during the melting process. Its mechanical properties are close to those of aluminum. A thin-wall structure based two dimensional and three dimensional radial collimators were fabricated with well-controlled geometry for neutron scattering measurement.

36 MATERIALS SCIENCE↗

Empirical Investigation of Properties for Additive Manufactured Aluminum Metal Matrix Composites

Laser additive manufacturing with mixed powders of aluminum alloy and silicon carbide (SiC) or boron carbide (B4C) is investigated in this experiment. With various mixing ratios of SiC/Al to form metal matrix composites (MMC), their mechanical and physical properties are empirically investigated. Parameters such as laser power, scan speed, scan pattern, and hatching space are optimized to obtain the highest density for each mixing ratio of SiC/Al. The mechanical and thermal properties are systematically investigated and compared with and without heat treatment. It shows that 2 wt% of SiC obtained the highest strength and Young’s modulus. Graded composite additive manufacturing (AM) of MMC is also fabricated and characterized. Various types of MMC devices, such as heat sink using graded SiC MMC and grid type three-dimensional (3D) neutron collimators using boron carbide (B4C), were also fabricated to demonstrate their feasibility for applications.

36 MATERIALS SCIENCE↗

Understanding Uncertainty in Microstructure Evolution and Constitutive Properties in Additive Process Modeling

Coupled process–microstructure–property modeling, and understanding the sources of uncertainty and their propagation toward error in part property prediction, are key steps toward full utilization of additive manufacturing (AM) for predictable quality part development. The OpenFOAM model for process conditions, the ExaCA model for as-solidified grain structure, and the ExaConstit model for constitutive mechanical properties are used as part of the ExaAM modeling framework to examine a few of the various sources of uncertainty in the modeling workflow. In addition to “random” uncertainty (due to random number generation in the orientations and locations of grains present), the heterogeneous nucleation density N 0 and the mean substrate grain spacing S 0 are varied to examine their impact of grain area development as a function of build height in the simulated microstructure. While mean grain area after 1 mm of build is found to be sensitive to N 0 and S 0 , particularly at small N 0 and large S 0 (despite some convergence toward similar values), the resulting grain shapes and overall textures develop in a reasonably similar manner. As a result of these similar textures, ExaConstit simulation using ExaCA representative volume elements (RVEs) from various permutations of N 0 , S 0 , and location within the build resulted in similar yield stress, stress–strain curve shape, and stress triaxiality distributions. It is concluded that for this particular material and scan pattern, 15 layers is sufficient for ExaCA texture and ExaConstit predicted properties to become relatively independent of additional layer simulation, provided that reasonable estimates for N 0 and S 0 are used. However, additional layers of ExaCA will need to be run to obtain mean grain areas independent of build height and baseplate structure.

36 MATERIALS SCIENCE↗

On turbulence models and lidar measurements for wind turbine control

Abstract. To provide comprehensive information that will assist in making decisions regarding the adoption of lidar-assisted control (LAC) in wind turbine design, this paper investigates the impact of different turbulence models on the coherence between the rotor-effective wind speed and lidar measurement. First, the differences between the Kaimal and Mann models are discussed, including the power spectrum and spatial coherence. Next, two types of lidar systems are examined to analyze the lidar measurement coherence based on commercially available lidar scan patterns. Finally, numerical simulations have been performed to compare the lidar measurement coherence for different rotor sizes. This work confirms the association between the measurement coherence and the turbulence model. The results indicate that the lidar measurement coherence with the Mann turbulence model is lower than that with the Kaimal turbulence model. In other words, the potential value creation of LAC based on simulations during the wind turbine design phase, evaluated using the Kaimal turbulence model, will be diminished if the Mann turbulence model is used instead. In particular, the difference in coherence is more significant for larger rotors. As a result, this paper suggests that the impacts of different turbulence models should be considered uncertainties while evaluating the benefits of LAC.

17 WIND ENERGY↗

Comparison of ERTS-1 and Skylab-EREP for interdisciplinary coastal investigations

The author has identified the following significant results. NASA's ERTS-1 satellite and Skylab EREP have both provided imagery suitable for investigating coastal vegetation, land use, current circulation, water turbidity, waste disposal, and sea state. Based on high contrast targets, such as piers and breakwaters, the ERTS-1 MSS seems to have a resolution of 70-100 meters, Skylab's S190A about 30-70 meters, and its S190B about 10-30 meters. Important coastal land use details can be more readily mapped using Skylab's imagery. On the other hand, the regular eighteen day cycle of ERTS-1 allows observation of important manmade and natural changes, and facilitates collection of ground truth. The Skylab/EREP multispectral scanner offers 13 spectral bands as compared to 4 bands on ERTS-1. However, EREP scanner tapes require special filtering to remove several types of noise and their conical line scan pattern must be linearized before one can identify small targets based on spatial features.

Klemas, V.↗

Skylab/EREP application to ecological, geological and oceanographic investigations of Delaware Bay

The author has identified the following significant results. NASA's ERTS-1 satellite and Skylab-EREP have both provided imagery suitable for investigating coastal vegetation, land use, current circulation, water turbidity, waste disposal, and sea state. Based on high contrast targets, such as piers and breakwaters, the ERTS-1 MSS seems to have a resolution of 70-100 meters, Skylab's S190A about 30-70 meters, and its S190B about 10-30 meters. Important coastal land use details can be more readily mapped using Skylab's imagery. On the other hand, the regular eighteen day cycle of ERTS-1 allows observation of important man-made and natural changes, and facilitates collection of ground truth. The Skylab/EREP multispectral scanner offers 13 spectral bands as compared to 4 bands on ERTS-1. However, EREP scanner tapes require special filtering to remove several types of noise and their conical line scan pattern must be linearized before small targets can be identified based on spatial features.

Klemas, V.↗

Data analysis study and performance evaluation of the scanning laser Doppler system

A simulation program which provided information on theoretically expected vortex spectra, evaluations of potential algorithms, and expected location accuracies for given scan patterns is presented. Field tests using an aircraft engine flow field and aircraft vortices during flyby tests were compared to the results of the simulation. From these studies, a vortex location algorithm was developed which provided vortex location for one or two vortices as a function of time. Results of this algorithm used on data from flyby tests were used to study vortex transport, to evaluate system performance, and to provide suggestions for real-time vortex location algorithms. The results of real-time analysis were compared to those which were expected based on theoretical considerations.

Sonnenschein, C. M.↗

Holographic analyzer and image scanner

The characteristics, components, and operating procedures are described for a holographic camera real images projection displayer and scanner unit having the capability to upgrade to multiple types of automated raster scan patterns. Schematics of the optical components are included with a diagram of the electric circuit connections.

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Single pilot scanning behavior in simulated instrument flight

A simulation of tasks associated with single pilot general aviation flight under instrument flight rules was conducted as a baseline for future research studies on advanced flight controls and avionics. The tasks, ranging from simple climbs and turns to an instrument landing systems approach, were flown on a fixed base simulator. During the simulation the control inputs, state variables, and the pilots visual scan pattern including point of regard were measured and recorded.

Pennington, J. E.↗

Finding the times that SMMR observed a ship

In order to facilitate the coincidence calculations, the coordinates of the ship and the satellite were transformed to the ECO system in which the equatorial plane is the plane of the satellite's orbit. The transformation matrices for each step are presented. The ship could be observed when it was in a band about the equator in the ECO system. The width of the band was determined by the scan pattern of the instrument.

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