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NASA NTRS1985

Investigation of foam flotation and phase partitioning techniques

The present status of foam flotation as a separation process is evaluated and limitations for cells and proteins are determined. Possible applications of foam flotation to separations in microgravity are discussed. Application of the fluid mechanical aspects of foam separation techniques is made to phase partitioning in order to investigate the viscous drag forces that may effect the partitioning of cells in a two phase poly(ethylene glycol) and dextran system.

Currin, B. L.↗

DOE OSTI2023

A New Approach to Monitoring Solvent Extraction Processes for the Nuclear Industry

As part of an initiative to steward research, development, and innovation into the nuclear fuel cycle, Idaho National Laboratory is building the Beartooth testbed. Beartooth will include a cascade of centrifugal contactors, glove box lines, solidification, and dissolution equipment to aid in the progression of novel separation techniques and provide hands-on opportunities to early-career separation scientists. Beartooth will incorporate novel monitoring techniques using sensors and machine learning algorithms to inform a process operator of separation conditions. This research is examining monitoring technologies not typically used in nuclear separation processes such as acoustic microphones, accelerometers, infrared cameras, red-green-blue color sensors, among others. These sensors are being examined for their functionality within a separation process and their ability to detect applicable signals. Machine learning methods are being developed to determine their utility in detecting faults and alerting operators of expected and unexpected events. These methods have the potential to impact Safeguards by Design efforts and real-time decision making. This overview will detail preliminary results from acoustic, vibration, and color sensors.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

NASA NTRS1988

The relationship between large-scale vertical motion, highly reflective cloud, and sea surface temperature in the tropical Pacific region

Vertical motion fields at 850 mbar over the tropical Pacific region are calculated from the 1963-1973 mean wind fields for 4 months of the year and for October 1972, the peak month in the 1972-1973 El Nino event. These vertical motion fields are derived using the projective separation technique, which has the unique property of separating vertical motion into components due to meridional wind convergence and zonal wind convergence. This separation permits investigation of the response of the Hadley and Walker circulations to annual and interannual variation of the sea surface temperature in the tropical Pacific. The large-scale features of the computed vertical motion fields are in agreement with those of highly reflective clouds, which indicate the locations of deep convection. Examination of the annual cycle of the vertical motion and its components shows no strong variation of the Walker circulation with the east-west gradient of sea surface temperature. On the other hand, a strong correlation is found between meridional overturning in the eastern Pacific and the local equatorial sea surface temperature: during El Nino events, the eastern and central Pacific contribution to the Hadley circulation tends to increase.

Zimmermann, Peter H.↗

NASA NTRS1983

Solar wind deceleration and MHD turbulence in the earth's foreshock region - ISEE 1 and 2 and IMP 8 observations

The interaction of the solar wind with ions backstreaming from the earth's bow shock is investigated using plasma and magnetic field measurements on ISEE 1 and 2 and IMP 8 at widely separated positions in the earth's foreshock. This technique separates temporal and spatial variations within the foreshock. It is found that the solar wind acceleration associated with backstreaming ions is correlated with the amplitude of the MHD turbulence, and that the largest decelerations are seen close to the bow shock. The density of the backstreaming ion beam is strongly correlated with distance from the shock, and decreases by about a factor of three in a distance of about 3R(e).

Bonifazi, C.↗

NASA NTRS1988

Acrolein Microspheres Are Bonded To Large-Area Substrates

Reactive cross-linked microspheres produced under influence of ionizing radiation in aqueous solutions of unsaturated aldehydes, such as acrolein, with sodium dodecyl sulfate. Diameters of spheres depend on concentrations of ingredients. If polystyrene, polymethylmethacrylate, or polypropylene object immersed in solution during irradiation, microspheres become attached to surface. Resulting modified surface has grainy coating with reactivity similar to free microspheres. Aldehyde-substituted-functional microspheres react under mild conditions with number of organic reagents and with most proteins. Microsphere-coated macrospheres or films used to immobilize high concentrations of proteins, enzymes, hormones, viruses, cells, and large number of organic compounds. Applications include separation techniques, clinical diagnostic tests, catalytic processes, and battery separators.

Rembaum, Alan↗

NASA NTRS1990

Acoustophoresis - A New Separation Concept

Ultrasound separates chemical species. Concept under development expands technology of chemical separation to include ultrasonic-radiation pressure. New technique separates species of particles according to ultrasonic properties. Acoustophoresis concept utilizes not only bulk compressional waves but also surface waves or boundary waves between solid (or liquid) container wall and subject liquid.

Heyman, Joseph S.↗

NASA NTRS1996

Binary Oscillatory Crossflow Electrophoresis

We present preliminary results of our implementation of a novel electrophoresis separation technique: Binary Oscillatory Cross flow Electrophoresis (BOCE). The technique utilizes the interaction of two driving forces, an oscillatory electric field and an oscillatory shear flow, to create an active binary filter for the separation of charged species. Analytical and numerical studies have indicated that this technique is capable of separating proteins with electrophoretic mobilities differing by less than 10%. With an experimental device containing a separation chamber 20 cm long, 5 cm wide, and 1 mm thick, an order of magnitude increase in throughput over commercially available electrophoresis devices is theoretically possible.

Molloy, Richard F.↗

NASA NTRS1992

Design of multisample, multistep phase partitioning apparatus for use on Space Shuttle Spacelab, and Spacelab missions

Traditional separation techniques are inadequate for many new bioprocessing challenges. Innovative separation methods such as aqueous two phase partitioning are needed to perpetuate bioprocess commercialization. Aqueous two phase polymer partitioning systems provide a process for separating biological materials when combined with microgravity. An innovative space qualified apparatus developed for carrying out separations by partitioning in immiscible polymer systems under mirogravity conditions is described. The apparatus offers an innovative approach to low gravity bioseparations in general and phase partitioning in particular. These capabilities support NASA's interest in serving the biotechnology research community and providing quantitative data in the gravity dependent components of separation processes.

Deuser, Mark S.↗

NASA NTRS1966

Tool separates sleeve-type unions without heat

Tool that uses conventional milling and cutting techniques separates sleeve type tubing unions and tubes without using heat. A selection of holders, associated bits, and cutting wheels permits preparation of varied diameter unions.

Millett, A. U.↗

NASA NTRS1995

Scheduling logic for Miles-In-Trail traffic management

This paper presents an algorithm which can be used for scheduling arrival air traffic in an Air Route Traffic Control Center (ARTCC or Center) entering a Terminal Radar Approach Control (TRACON) Facility . The algorithm aids a Traffic Management Coordinator (TMC) in deciding how to restrict traffic while the traffic expected to arrive in the TRACON exceeds the TRACON capacity. The restrictions employed fall under the category of Miles-in-Trail, one of two principal traffic separation techniques used in scheduling arrival traffic . The algorithm calculates aircraft separations for each stream of aircraft destined to the TRACON. The calculations depend upon TRACON characteristics, TMC preferences, and other parameters adapted to the specific needs of scheduling traffic in a Center. Some preliminary results of traffic simulations scheduled by this algorithm are presented, and conclusions are drawn as to the effectiveness of using this algorithm in different traffic scenarios.

Synnestvedt, Robert G.↗

NASA NTRS1990

Study of a co-designed decision feedback equalizer, deinterleaver, and decoder

A technique that promises better quality data from band limited channels at lower received power in digital transmission systems is presented. Data transmission, in such systems often suffers from intersymbol interference (ISI) and noise. Two separate techniques, channel coding and equalization, have caused considerable advances in the state of communication systems and both concern themselves with removing the undesired effects of a communication channel. Equalizers mitigate the ISI whereas coding schemes are used to incorporate error-correction. In the past, most of the research in these two areas has been carried out separately. However, the individual techniques have strengths and weaknesses that are complementary in many applications: an integrated approach realizes gains in excess to that of a simple juxtaposition. Coding schemes have been successfully used in cascade with linear equalizers which in the absence of ISI provide excellent performance. However, when both ISI and the noise level are relatively high, nonlinear receivers like the decision feedback equalizer (DFE) perform better. The DFE has its drawbacks: it suffers from error propagation. The technique presented here takes advantage of interleaving to integrate the two approaches so that the error propagation in DFE can be reduced with the help of error correction provided by the decoder. The results of simulations carried out for both, binary, and non-binary, channels confirm that significant gain can be obtained by codesigning equalizer and decoder. Although, systems with time-invariant channels and simple DFE having linear filters were looked into, the technique is fairly general and can easily be modified for more sophisticated equalizers to obtain even larger gains.

Peile, Robert E.↗

DOE OSTI2023

Proof-of-concept studies of novel protocols for producing highly pure 48 V from a 48 Cr/ 48 V generator

Here, the quest to improve the quality of nuclear data, such as half-lives, transition yields, and reaction cross-sections, is a shared endeavor among various areas of nuclear science. 48 V is a vanadium isotope for which experimental data on neutron reaction cross-sections is needed. However, traditional isotope production techniques cannot produce 48 V with high enough isotopic purity for some of these measurements. “Isotope harvesting” at the Facility for Rare Isotope Beams (FRIB) is a new isotope production technique that could potentially yield 48 V with the necessary purity for such studies. In this case, 48Cr would be collected and allowed to generate 48 V that can be separated from undecayed 48 Cr to yield highly pure 48 V. Thus, any protocol for producing pure 48 V via isotope harvesting would involve utilizing a separation technique that can effectively separate 48 Cr and 48 V. In this study, the radiotracers 51 Cr and 48 V were used to develop possible radiochemical separation methodologies, which can be translated to obtain high purity 48 V via this novel isotope production method. The developed protocols utilize either ion exchange or extraction chromatographic resins. Separations of 51 Cr and 48 V with AG 1-X8 anion exchange resin respectively resulted in recoveries of 95.6(26)% and 96.2(12)% with radionuclidic purities of 92(2)% and 99(1)%. An even more effective Cr and V separation was obtained with an extraction chromatographic resin (TRU resin) and 10 M HNO 3 loading solution. Here, 51 Cr and 48 V respectively had recoveries of 94.1(28)% and 96.2(13)% with high radionuclidic purities (100(2)% and 100(1)%) in small volumes (8.81(8) mL and 5.39(16) mL). This study suggests that, to maximize the yield and isotopic purity of 48 V, the best production protocol would involve utilizing two separations with TRU resin and 10 M HNO 3 to isolate 48 Cr and purify the generated 48 V.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

NASA NTRS1982

Polymer research at NASA Langley Research Center

Polymer synthesis programs involve the development of Novel thermoplastics, pseudothermoplastics, and thermosets. These systems are prepared to elucidate structure-property relationships involving thermal capabilities, toughness, processability and environmental stability. Easily processable polyimides, solvent-resistant polysulfones and polyphenylquinoxalines, and tougher high and intermediate temperature polymers were developed. Characterization efforts included high pressure liquid chromatography methodology, the development of toughness tests for fiber reinforced composites, a study of electrical properties of metal ion filled polyimides, and a study of the mutagenicity of aromatic diamines. Also the mechanism of cure/degradation of experimental polymers was studied by rheology, mechanical behavior, separation techniques and spectroscopy. The degradative crosslinking of alkyl-containing polyimides, the separation and identification of crosslinked phenylquinoxalines, the rheological behavior of hot-melt polyimides, and the elucidation of the cure of norbornene endcapped imides were also studied.

Terry L. St. Clair↗

NASA NTRS1990

Fluid Phase Separation (FPS) experiment for flight on a space shuttle Get Away Special (GAS) canister

The separation of fluid phases in microgravity environments is of importance to environmental control and life support systems (ECLSS) and materials processing in space. A successful fluid phase separation experiment will demonstrate a proof of concept for the separation technique and add to the knowledge base of material behavior. The phase separation experiment will contain a premixed fluid which will be exposed to a microgravity environment. After the phase separation of the compound has occurred, small samples of each of the species will be taken for analysis on the Earth. By correlating the time of separation and the temperature history of the fluid, it will be possible to characterize the process. The experiment has been integrated into space available on a manifested Get Away Special (GAS) experiment, CONCAP 2, part of the Consortium for Materials Complex Autonomous Payload (CAP) Program, scheduled for STS-42. The design and the production of a fluid phase separation experiment for rapid implementation at low cost is presented.

Peters, Bruce↗

NASA NTRS1990

Fluid Phase Separation (FPS) experiment for flight on the shuttle in a Get Away Special (GAS) canister: Design and fabrication

The separation of fluid phases in microgravity environments is of importance to environmental control and life support systems (ECLSS) and materials processing in space. A successful fluid phase separation experiment will demonstrate a proof of concept for the separation technique and add to the knowledge base of material behavior. The phase separation experiment will contain a premixed fluid that will be exposed to a microgravity environment. After the phase separation of the compound has occurred, small samples of each of the species will be taken for analysis on Earth. By correlating the time of separation and the temperature history of the fluid, it will be possible to characterize the process. The phase separation experiment is totally self-contained, with three levels of containment on all fluids, and provides all necessary electrical power and control. The controller regulates the temperature of the fluid and controls data logging and sampling. An astronaut-activated switch will initiate the experiment and an unmaskable interrupt is provided for shutdown. The experiment has been integrated into space available on a manifested Get Away Special (GAS) experiment, CONCAP 2, part of the Consortium for Materials Complex Autonomous Payload (CAP) Program, scheduled for STS 42 in April 1991. Presented here are the design and the production of a fluid phase separation experiment for rapid implementation at low cost.

Source record↗

DOE OSTI2025

Dynamic separation of gases using microsieves

Separation of light weight molecules, such as nitrogen, argon, and oxygen, from heavier compounds can have significant impacts on energy capture, environmental monitoring, or isotopic applications. Large-scale gas separation techniques, like gas centrifugation and membrane mitigation, can be problematic as they impart tremendous energy and induce high mechanical stress onto the instrumentation. Microsieves, also known as micronozzles or microfunnels, are developed to create physical barriers to separate specific isotopes and gases. Separation is achieved using a converging and diverging micronozzle to impose supersonic gas flow around a curved wall, and it has been used for the separation of heavy actinide isotopes in low weight gas as well as separation of low weight gas compositions of nitrogen and argon back in 1900s. However, systematic reviews of this unique technology are lacking. The application of the Laval style nozzle, which has a converging/diverging entrance fundamental to the micronozzle, is included in this review due to its importance in industrial applications in uranium (U) isotope refinement. Using advanced computational fluid dynamic (CFD) simulations, the extent of gas separation can be modelled. Herein, we first examine the literature and survey recent advances on fabrication techniques for creating curved micronozzles, methods and separation principles used to design devices. Furthermore, we then follow with highlights of CFD simulations applied to evaluate the separation effects using microsieves. Finally, identification of the gap and recommendation for future development and applications are suggested for using intrinsic molecular features and fluidic dynamics in formulating separation strategies.

30 Microfluidics↗

DOE OSTI2024

Membrane Separations in Biomass Processing

The development of integrated biorefineries and the greater utilization of biomass resources to reduce dependence on fossil fuel-derived products require research emphasis not just on conversion strategies but also on improving separations associated with biorefining. A significant roadblock towards developing biorefineries is the lack of effective separation techniques evidenced by the relative deficiency of literature in this area. Additionally, high conversion yields may only be realized if effective separations generate feedstock of sufficient purity – this makes research into biomass conversion strategies all the more critical. In this review, the challenges associated with biomass separations are discussed, followed by an overview of the most appropriate separation strategies for processing biomass. One of the unit operations most appealing for biorefining, membrane separations (MS), is then considered along with a review of the recent literature utilizing this technique in biomass processing.

09 BIOMASS FUELS↗

DOE OSTI2021

Single-hole couplings in GaAs/AlGaAs double dots probed with transport and EDSR spectroscopy

Here, we report a detailed study of the tunnel barriers within a single-hole GaAs/AlGaAs double quantum dot device (DQD). For quantum information applications as well as fundamental studies, careful tuning and reliable measurements of the barriers are important requirements. In order to tune a DQD device adequately into the single-hole electric dipole spin resonance regime, one has to employ a variety of techniques to cover the extended range of tunnel couplings. In this work, we demonstrate four separate techniques, based upon charge sensing, quantum transport, time-resolved pulsing, and electron dipole spin resonance spectroscopy to determine the couplings as a function of relevant gate voltages and magnetic field. Measurements were performed under conditions of both symmetric and asymmetric tunnel couplings to the leads. Good agreement was observed between different techniques when measured under the same conditions. The results indicate that even in this relatively simple circuit, the requirement to tune multiple gates and the consequences of real potential profiles result in non-intuitive dependencies of the couplings as a function of the plunger gate voltage and the magnetic field.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗