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At least 73 records · Page 4

Microstructural evolution in shear-punch tests: A comparative study of pure Cu and Cu-Cr alloy

Understanding the mechanisms behind microstructural evolution during shear deformation has been a long-standing area of interest. However, establishing a connection between microstructure, mechanical properties, and extent of shear deformation is challenging and requires refined experimental approaches. Shear-punch testing (SPT) provides a controlled method to introduce shear into small volumes of material that later can be subjected to detailed microstructural characterization. In this study, we utilize an SPT device to induce shear deformation to pure copper and a binary copper-chromium alloy. Electron backscatter diffraction and transmission electron microscopy were used to study the mechanisms of plastic deformation after SPT. Our results indicate that shear deformation of pure Cu produces a dense network of intercepting microshear bands upon sustained deformation. Twin boundaries undergo degradation into high angle grain boundaries due to simultaneous deviation from the axis-angle pair condition of 60° misorientation on [111] direction. The presence of 50% volume Cr particles in the soft Cu matrix fundamentally altered the shear deformation mechanism. Preferential deformation of the Cu matrix led to accelerated shear-induced formation of low and high angle grain boundaries, and subsequent grain refinement. Comparatively, no grain refinement occurred in pure Cu at a strain ~10 times larger (ϵ = 4.73) than that of the copper-chromium case (ϵ = 0.42). Overall, our study sheds light on the microstructural evolution during shear deformation and highlights the significant influence of particle reinforcements on the shear deformation mechanisms of metals.

36 MATERIALS SCIENCE↗

Development and Evaluation of Stitched Sandwich Panels

This study explored the feasibility and potential benefits provided by the addition of through-the-thickness reinforcement to sandwich structures. Through-the-thickness stitching is proposed to increase the interlaminar strength and damage tolerance of composite sandwich structures. A low-cost, out-of-autoclave processing method was developed to produce composite sandwich panels with carbon fiber face sheets, a closed-cell foam core, and through-the-thickness Kevlar stitching. The sandwich panels were stitched in a dry preform state, vacuum bagged, and infiltrated using Vacuum Assisted Resin Transfer Molding (VARTM) processing. For comparison purposes, unstitched sandwich panels were produced using the same materials and manufacturing methodology. Test panels were produced initially at the University of Utah and later at NASA Langley Research Center. Four types of mechanical tests were performed: flexural testing, flatwise tensile testing, core shear testing, and edgewise compression testing. Drop-weight impact testing followed by specimen sectioning was performed to characterize the damage resistance of stitched sandwich panels. Compression after impact (CAI) testing was performed to evaluate the damage tolerance of the sandwich panels. Results show significant increases in the flexural stiffness and strength, out-of-plane tensile strength, core shear strength, edgewise compression strength, and compression-after-impact strength of stitched sandwich structures.

Stanley, Larry E.↗

Material Testing of PH13-8MO H950 Steel for Xue-Wierzbicki Fracture Criterion Determination

Four tensile coupon designs of PH13-8Mo H950 steel were tested to failure using quasi-static rates to obtain data to calibrate the Xue-Wierzbicki failure model for ductile fracture. The tests recorded the force-displacement, location of the first crack, displacement to fracture, area reduction, and crack propagation path. The test method and coupon designs were adopted from Tomasz Wierzbicki’s “Calibration and evaluation of seven fracture models” report. The XueWierzbicki model predicts fracture based on accumulated equivalent plastic strain, stress triaxiality, and deviatoric state parameter. Calibrating the Xue-Wierzbicki failure model required testing four coupon designs to calculate the four free parameters in the model. The coupon designs tested a range of stress triaxialities with two axisymmetric tests, one shear test, and one plane stress test. The data obtained and presented in this report can be used to develop a Xue-Wierzbicki fracture model for PH13-8Mo H950 steel.

36 MATERIALS SCIENCE↗

Strain Monitoring of Flexible Structures

One of the biggest challenges facing NASA's deep space exploration goals is structural mass. A long duration transit vehicle on a journey to Mars, for example, requires a large internal volume for cargo, supplies and crew support. As with all space structures, a large pressure vessel is not enough. The vehicle also requires thermal, micro-meteoroid, and radiation protection, a navigation and control system, a propulsion system, and a power system, etc. As vehicles get larger, their associated systems also get larger and more complex. These vehicles require larger lift capacities and force the mission to become extremely costly. In order to build large volume habitable vehicles, with only minimal increases in launch volume and mass, NASA is developing lightweight structures. Lightweight structures are made from non-metallic materials including graphite composites and high strength fabrics and could provide similar or better structural capability than metals, but with significant launch volume and mass savings. Fabric structures specifically, have been worked by NASA off and on since its inception, but most notably in the 1990's with the TransHAB program. These TransHAB developed structures use a layered material approach to form a pressure vessel with integrated thermal and micro-meteoroid and orbital debris (MMOD) protection. The flexible fabrics allow the vessel to be packed in a small volume during launch and expand into a much larger volume once in orbit. NASA and Bigelow Aerospace recently installed the first human-rated inflatable module on the International Space Station (ISS), known as the Bigelow Expandable Activity Module (BEAM) in May of 2016. The module provides a similar internal volume to that of an Orbital ATK Cygnus cargo vehicle, but with a 77% launch volume savings. As lightweight structures are developed, testing methods are vital to understanding their behavior and validating analytical models. Common techniques can be applied to fabric materials, such as tensile testing, fatigue testing, and shear testing, but common measurement techniques cannot be used on fabric. Measuring strain in a material and during a test is a critical parameter for an engineer to monitor the structure during the test and correlate to an analytical model. The ability to measure strain in fabric structures is a challenge for NASA. Foil strain gauges, for example, are commonplace on metallic structures testing, but are extremely difficult to interface with a fabric substrate. New strain measuring techniques need to be developed for use with fabric structures. This paper investigates options for measuring strain in fabric structures for both ground testing and in-space structural health monitoring. It evaluates current commercially available options and outlines development work underway to build custom measurement solutions for NASA's fabric structures.

Litteken, Douglas A.↗

Shear Punch Testing of Neutron-Irradiated HT-9 and 14YWT

Shear punch mechanical testing was performed on neutron-irradiated HT-9 and 14YWT alloys, comparing the traditional ferritic/martensitic steel with the advanced oxide dispersion strengthened nanostructured ferritic alloy. The samples were irradiated at various temperatures between 380°C and 520°C. In HT-9, on increasing the irradiation temperature, the 1% offset shear stress and maximum shear stress decreased. The advanced 14YWT alloy was less sensitive to irradiation temperature with respect to irradiation hardening. However, it still exhibited irradiation hardening at each temperature.

36 MATERIALS SCIENCE↗

Degradation in PV Encapsulant Strength of Attachment: An Interlaboratory Study Towards a Climate-Specific Test

Reduced strength of attachment of the encapsulant resulting from the outdoor environment, including ultraviolet (UV) radiation, may decrease photovoltaic (PV) module lifetime by enabling widespread corrosion of internal components. To date, few studies exist showing how the adhesion of PV components varies with environmental stress. We have conducted an interlaboratory experiment to provide an understanding that will be used to develop climatic specific module tests. Factors examined in the study included the UV light source (lamp type), temperature, and humidity to be proposed for use in accelerated aging tests. A poly (ethylene-co-vinyl acetate) (EVA) formulation often used in veteran PV installations was studied using a compressive shear test - to quantify the strength of attachment at the EVA/glass interface. Replicate laminated glass/polymer/glass coupon specimens were weathered at 12 institutions using a variety of indoor chambers or field aging. Shear strength, shear strain, and toughness were measured using a mechanical load-frame for the compressive shear test, with subsequent optical imaging and electron microscopy of the separated surfaces.

14 SOLAR ENERGY↗

Shear-Panel Test Fixture Eliminates Corner Stresses

New design eliminates corner stresses while maintaining uniform stress across panel. Shear panel test fixture includes eight frames and eight corner pins. Fixture assembled in two halves with shear panel sandwiched in between. Results generated from this fixture will result in good data base for design of efficient aircraft structures and other applications.

Kiss, J. J.↗

CFD Analysis of Flexible Thermal Protection System Shear Configuration Testing in the LCAT Facility

This paper documents results of computational analysis performed after flexible thermal protection system shear configuration testing in the LCAT facility. The primary objectives were to predict the shear force on the sample and the sensitivity of all surface properties to the shape of the sample. Bumps of 0.05, 0.10,and 0.15 inches were created to approximate the shape of some fabric samples during testing. A large amount of information was extracted from the CFD solutions for comparison between runs and also current or future flight simulations.

Ferlemann, Paul G.↗

Probing elastically or plastically induced structural heterogeneities in bulk metallic glasses by nanoindentation pop-in tests

Shear banding dynamics in bulk metallic glasses (BMGs) is manifested by the spatiotemporal evolution of strain fields which in turn depend on structural heterogeneities. The spacing of these heterogeneities, as a characteristic length scale, was determined from the analysis of nanoindentation pop-in tests using a stochastic model. Furthermore, the pre-stress by elastic bending and residual stress by plastic bending of BMG plates were found to dramatically decrease such spacings, thus increasing heterogeneity density and mechanically rejuvenating the glass structure.

36 MATERIALS SCIENCE↗

Simple torsion test for shear moduli determination of orthotropic composites

By means of torsion tests performed on test specimens of the same material having a minimum of two different cross sections (flat sheet of different widths), the effective in-plane (G13) and out-of-plane (G23) shear moduli were determined for two composite materials of uniaxial and angleply fiber orientations. Test specimens were 16 plies (nominal 2 mm) thick, 100 mm in length, and in widths of 6.3, 9.5, 12.5, and 15.8 mm. Torsion tests were run under controlled deflection (constant angle of twist) using an electrohydraulic servocontrolled test system. In-plane and out-of-plane shear moduli were calculated from an equation derived in the theory of elasticity which relates applied torque, the torsional angle of twist, the specimen width/thickness ratio, and the ratio of the two shear moduli G13/G23. Results demonstrate that torsional shear moduli, G23 as well as G13, can be determined by simple torsion tests of flat specimens of rectangular cross section. Neither the uniaxial nor angleply composite material were transversely isotropic.

Sumsion, H. T.↗

Shear Punch Testing of BOR60 Irradiated HT-9 and 14YWT

Ferritic/martensitic (FM) steels and nanostructured ferritic alloys (NFA) are being developed for next generation reactor applications. Applications such as transmutation of long lived isotopes in used fuels require cladding materials that can withstand high irradiation doses, potentially in the hundreds of displacements per atom (dpa). The FM steels in this report include HT-9 steel, which is a Fe-12Cr steel with additions of Mo, Mn, Ni, V and W. An oxide dispersion strengthened (ODS) 14YWT is also presented, which has a distribution of nano-scale oxide particles throughout the microstructure. Shear punch testing was performed on both steels. The material was neutron irradiated at the BOR60 reactor in Russia and transferred to LANL for shear punch mechanical testing. These results are complementary to a previous report, also from a BOR60 irradiation.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Reporting Verification of BOP Shear Ram Capability: Requirements and Good Practices on Reporting Blowout Preventer (BOP) Shear Ram Capability for Outer Continental Shelf (OCS) Oil and Gas Operations

The Bureau of Safety and Environmental Enforcement (BSEE) Well Control Rule (Subpart G)1 became effective on July 28, 2016. This rule is part of the BSEE regulations pertaining to well control equipment used for oil and gas operations on the U.S. Outer Continental Shelf (OCS). More recently BSEE issue a proposed rule to amend portions of the 2016 well control rule. This proposed rule (now implemented) appeared in the Federal Register on May 18, 2018. This report was prepared late in the public comment period for the current rule and intended is a sample of desirable documentation of blind shear ram shear testing and associated regulatory requirements either in place or anticipated at the time of preparation. In accordance with this original rule and the proposed revisions, BSEE requests specific information regarding the capabilities of blind shear rams (BSR) in the Blowout Preventer (BOP). This information is required prior to beginning any operation involving the use of any BOP. More specifically, Title 30 CFR 250.732(b) of these regulations requires documentation of shear testing demonstrating the shearing and sealing capabilities of the BOP BSR. Such documentation is consistent with and complementary to other documentation verifying the designs of individual well control components and the overall BOP system. Verification demonstrates performance and reliability of the equipment based on a testing process that is repeatable and reproducible.2 This document, an annotated outline of verification documentation, arises from the combination of regulations and good practices concerning how to report BOP shear ram tests and third-party verification of BSR capability to support BSEE’s regulatory role.

03 NATURAL GAS↗

A LASER INTERFERENCE-BASED SURFACE TREATMENT OF AL AND CARBON FIBER POLYMER COMPOSITES FOR ENHANCED BONDING

Due to its increased use in the automotive and aerospace industries, joining of Carbon Fiber-reinforced Polymer matrix Composites (CFPC) to metals demands enhanced surface preparation and control of surface morphology prior to joining. In this study, surfaces of both composite and aluminum were prepared for joining using a new laser based technique, in which the laser interference power profile was created by splitting the beam and guiding those beams to the sample surface by overlapping each other with defined angles to each other. Results were presented for the overlap shear testing of single-lap joints made with Al 5182 and CFPC specimens whose surfaces prepared by (a) surface abrasion and solvent cleaning; and (b) laser-interference structured surfaces by rastering with a 4 mm laser beam at approximately 3.5 W power. CFPC specimens of T700S carbon fiber, Prepreg T70 epoxy, 4 or 5 ply thick, 0/90o plaques were used. Adhesive DP810 was used to bond Al and CFPC. The bondline was 0.25mm and the bond length was consistent among all joints produced. First, the effect of the laser speed on the joint performance was evaluated by laser-interference structure Al and CFPC surfaces with a beam angle of 3o and laser beam speeds of 3, 5, and 10 mm/s. For this sensitivity study, 3 joint specimens were used per each joint type. Based on the results for minimum, maximum, and mean values for the shear lap strength and maximum load for all the 9 joint types, two joint types were selected for further evaluations. Six additional joint specimens were prepared for these two joint types in order to obtain better statistics and the shear test data was presented for the range, mean, and standard deviation. The results for the single-lap shear tests obtained for six joint specimens, indicate that the shear lap strength, maximum load, and displacement at maximum load for those joints made with laser-interference structured surfaces were increased by approximately 14.8%, 16%, and 100%, respectively over those measured for the baseline joints.

Sabau, Adrian S↗

Shear Punch Testing of BOR-60 Irradiated TEM Specimens

As a part of the project “High Fidelity Ion Beam Simulation of High Dose Neutron Irradiation” an Integrated Research Program (IRP) project from the U.S. Department of Energy, Nuclear Energy University Programs (NEUP), TEM geometry samples of ferritic cladding alloys, Ni based super alloys and model alloys were irradiated in the BOR-60 reactor to ~16 dpa at ~370°C and ~400°C. Samples were sent to Los Alamos National Laboratory and subjected to shear punch testing. This report presents the results from this testing.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Assessment of four strain energy decomposition methods for phase field fracture models using quasi-static and dynamic benchmark cases

Abstract Strain energy decomposition methods in phase field fracture models separate strain energy that contributes to fracture from that which does not. However, various decomposition methods have been proposed in the literature, and it can be difficult to determine an appropriate method for a given problem. The goal of this work is to facilitate the choice of strain decomposition method by assessing the performance of three existing methods (spectral decomposition of the stress or the strain and deviatoric decomposition of the strain) and one new method (deviatoric decomposition of the stress) with several benchmark problems. In each benchmark problem, we compare the performance of the four methods using both qualitative and quantitative metrics. In the first benchmark, we compare the predicted mechanical behavior of cracked material. We then use four quasi-static benchmark cases: a single edge notched tension test, a single edge notched shear test, a three-point bending test, and a L-shaped panel test. Finally, we use two dynamic benchmark cases: a dynamic tensile fracture test and a dynamic shear fracture test. All four methods perform well in tension, the two spectral methods perform better in compression and with mixed mode (though the stress spectral method performs the best), and all the methods show minor issues in at least one of the shear cases. In general, whether the strain or the stress is decomposed does not have a significant impact on the predicted behavior.

Zhang, Shuaifang↗

Ten Deg Off-Axis Test for Shear Properties in Fiber Composites

A combined theoretical and experimental investigation was conducted to assess the suitability of the 10 deg off-axis tensile test specimen for the intralaminar shear characterization of unidirectional composites. Composite mechanics, a combined-stress failure criterion, and a finite variation across the specimen width and the relative stress and strain magnitudes at the 10 deg plane. Strain gages were used to measure the strain variation across the specimen width at specimen midlength and near the end tabs. Specimens from Mod-I/epoxy, T-300/epoxy, and S-glass/epoxy were used in the experimental program. It was found that the 10 deg off-axis tensile test specimen is suitable for intralaminar shear characterization, and it is recommended that it should be considered as a possible standard test specimen for such a characterization.

Chamis, C. C.↗

10-deg off-axis test for shear properties in fiber composites

A combined theoretical and experimental investigation was conducted to assess the suitability of the 10-deg off-axis tensile test specimen for the intralaminar shear characterization of unidirectional composites. Composite mechanics, a combined-stress failure criterion, and a finite-element analysis were used to determine theoretically the stress-strain variation across the specimen width and the relative stress and strain magnitudes at the 10-deg plane. Strain gages were employed to measure the strain variation across the specimen width at specimen midlength and near the end tabs. Specimens from Mod-I/epoxy, T-300/epoxy, and S-glass/epoxy were used in the experimental program. It was found that the 10-deg off-axis tensile test specimen is suitable for intralaminar shear characterization, and it is recommended that it should be considered as a possible standard test specimen for such a characterization.

Chamis, C. C.↗

Ultrasonic additive manufacturing of 4130 steel using Ni interlayers

Ultrasonic additive manufacturing (UAM) is a solid-state manufacturing process for making complex components. However, fabrication of ferritic (body centered cubic) steels has been challenging for UAM due to its high hardness. This research successfully joined AISI 4130 steel sheets by using soft Ni (face centered cubic) interlayers. The localisation of plastic deformation in the Ni-interlayer leads to a significant reduction in voids. A post-process heat-treatment was designed using thermodynamic calculations to dissolve nickel into steel matrix. Energy dispersive X-ray spectroscopy measurements showed ~10 µm Ni from the interlayer diffused into the steel side, confirming the feasibility of the approach. The shear tests show a higher shear strength in comparison to as-processed 4130 without interlayers and post processed using hot isostatic pressing (HIP).

36 MATERIALS SCIENCE↗