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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4

Characterization of an oxide dispersion strengthened superalloy, MA-6000E, for turbine blade applications

Alloy MA 6000E was developed by the mechanical alloying process for turbine blade applications. The nominal composition of the experimental alloy is Ni-15CR-2Mo-4W-4.5Al- 2.5Ti-2Ta- .15Zr-.05C-.01B-1.1Y2O3. The 1000 hour rupture strength in the longitudinal direction is about 145 MPa at 1093 C and about 483 MPa at 760 C. The alloy displays normal three-stage creep behavior. Typically the creep elongation is 3.5% at 760 C and 2% at 1093 C. The alloy is notch ductile (K sub 1 = 3.5). The rupture properties of the alloy are not significantly degraded by thermal cycling or prior stress isothermal exposure. The alloy also has excellent longitudinal high and low cycle fatigue resistance. Limited testing indicates that MA 6000E posesses good off-axis mechanical properties. The transverse tensile elongation at 760 C is about 3%. The 100 hour transverse rupture strength is 331 MPa at 760 C and about 55 MPa at 1093 C.

Kim, Y. G.↗

Study of the Reactive-element Effect in Oxidation of Fe-cr Alloys Using Transverse Section Analytical Electron Microscopy

The role of trace additions of reactive elements like Y, Ce, Th, or Hf to Cr bearing alloys was studied by applying a new developed technique of transverse section analytical electron microscopy. This reactive-element effect improves the high temperature oxidation resistance of alloys by strongly reducing the high temperature oxidation rate and enhancing the adhesion of the oxide scale, however, the mechanisms for this important effect remain largely unknown. It is indicated that the presence of yttrium affects the oxidation of Fe-Cr-Y alloys in at least two ways. The reactive element alters the growth mechanism of the oxide scale as evidenced by the marked influence of the reactive element on the oxide scale microstructure. The present results also suggest that reactive-element intermetallic compounds, which internally oxidize in the metal during oxidation, act as sinks for excess vacancies thus inhibiting vacancy condensation at the scale-metal interface and possibly enhancing scale adhesion.

King, W. E.↗

Chaos in driven Alfven systems

The chaos in a one-dimensional system, which would be nonlinear stationary Alfven waves in the absence of an external driver, is characterized. The evolution equations are numerically integrated for the transverse wave magnetic field amplitude and phase using the derivative nonlinear Schroedinger equation (DNLS), including resistive wave damping and a long-wavelength monochromatic, circularly polarized driver. A Poincare map analysis shows that, for the nondissipative (Hamiltonian) case, the solutions near the phase space (soliton) separatrices of this system become chaotic as the driver amplitude increases, and 'strong' chaos appears when the driver amplitude is large. The dissipative system exhibits a wealth of dynamical behavior, including quasiperiodic orbits, period-doubling bifurcations leading to chaos, sudden transitions to chaos, and several types of strange attractors.

Hada, T.↗

HP9-4-.30 weld properties and microstructure

HP9-4-.30, ultra high strength steel, the case material for the Advanced Solid Rocket Motor (ASRM), must exhibit acceptable strength, ductility, toughness, and stress corrosion cracking (SCC) resistance after welding and a local post weld heat treatment (PWHT). Testing, to date, shows that the base metal (BM) properties are more than adequate for the anticipated launch loads. Tensile tests of test specimens taken transverse to the weld show that the weld metal overmatches the BM even in the PWHT condition. However, that is still some question about the toughness and SCC resistance of the weld metal in the as welded and post weld heat treated condition. To help clarify the as welded and post weld heat treated mechanical behavior of the alloy, subsize tensile specimens from the BM, the fusion zone (FZ) with and without PWHT, and the heat affected zone (HAZ) with and without PWHT were tested to failure and the fracture surfaces subsequently examined with a scanning electron microscope. Results are given and briefly discussed.

Watt, George W.↗

Parameter Comparison for Low-Noise MoAu TES Bolometers

We describe a comparative investigation of the parameters of MoAu-bilayer Transition Edge Sensor (TES) bolometers designed for infrared detectors. A set of devices with variations in geometry were fabricated at the NASA/GSFC detector development facility. These detectors have different bilayer aspect ratios (providing differing normal state resistances and current densities), and have varieties of normal metal regions to study the effects of geometry on noise. These normal metal regions are oriented either parallel to or transverse to the direction of current flow, or both. The lowest noise detectors are found to have normal metal regions oriented transversely. For about a dozen different devices, we have measured a large set of parameters by means of a suite of tests. These include complex impedance measurements to derive time constants; IV curves to determine resistance and power; thermal conductance measurements; noise measurements as a function of device resistance; and &rect resistance vs. temperature measurements .

Benford, D. J.↗

Convective heat transfer from circular cylinders located within perforated cylindrical shrouds

The influence of perforated cylindrical shrouds on the convective heat transfer to circular cylinders in transverse flow has been studied experimentally. Geometries studied were similar to those used in industrial platinum resistance thermometers. The influence of Reynolds number, ventilation factor (ratio of the open area to the total surface area of shroud), radius ratio (ratio of shroud's inside radius to bare cylinder's radius), and shroud orientation with respect to flow were studied. The experiments showed that perforated shrouds with ventilation factors in the range 0.1 to 0.4 and radius ratios in the range 1.1 to 2.1 could enhance the convective heat transfer to bare cylinders up to 50%. The maximum enhancement occurred for a radius ratio of 1.4 and ventilation factors between 0.2 and 0.3. It was found that shroud orientation influenced the heat transfer, with maximum heat transfer generally occurring when the shroud's holes were centered on either side of the stagnation line. However, the hole orientation effect is of second order compared to the influence of ventilation factor and radius ratio.

Daryabeigi, K.↗

Characterization of damage modes in impacted thermoset and thermoplastic composites

Composite materials remain extremely vulnerable to out-of-plane impact loads, which may lead to severe losses in strength and stiffness. Impact induced damage is often a complex mixture of transverse cracks, delaminations and fiber failures. An experimental investigation was undertaken to quantify damage tolerance and resistance in composite materials impacted using the drop-weight method. Tests were conducted on laminates of several different carbon-fiber composite systems such as epoxies, modified epoxies, and amorphous and semicrystalline thermoplastics. In this paper, impacted composite specimens have been examined using destructive and nondestructive techniques to establish the characteristic damage states. Specifically, optical microscopy, ultrasonic and scanning electron microscopy techniques have been used to identify impact induced damage mechanisms. Damage propagation during post impact compression was also studied.

Srinivasan, K.↗

Environmental effects on aluminum fracture

The sustained load stress corrosion cracking (SCC) threshold for aluminum alloy 214 was determined using smooth (sigma sub TH) and precracked (K sub ISCC) specimens, and cyclic load growth behavior in 3.5% NaCl salt solution was studied. The relationship between K sub ISCC and sigma sub TH was also studied. The work showed that 2124-T851 aluminum alloy in plate gage has a moderately high resistance to stress corrosion attack. Experimental results showed that no SCC occurred in the longitudinal and long transverse directions in any of the tests. Some SCC was found by smooth tests in the short transverse direction, and the data were confirmed by two test methods-sigma sub TH = 275 MN/sq m (40 ksi). No SCC was found from compact specimen tests in any direction: surface flaw and center notch specimens evaluated in the short transverse direction exhibited SCC. The data indicate that stress corrosion behavior is defect, size, and stress dependent, but not entirely in accordance with a stress intensity controlled mechanism.

Schwartzberg, F. R.↗

Resistance fail strain gage technology as applied to composite materials

Existing strain gage technologies as applied to orthotropic composite materials are reviewed. The bonding procedures, transverse sensitivity effects, errors due to gage misalignment, and temperature compensation methods are addressed. Numerical examples are included where appropriate. It is shown that the orthotropic behavior of composites can result in experimental error which would not be expected based on practical experience with isotropic materials. In certain cases, the transverse sensitivity of strain gages and/or slight gage misalignment can result in strain measurement errors.

Tuttle, M. E.↗

Magnetically Diffused Radial Electric-Arc Air Heater Employing Water-Cooled Copper Electrodes

A magnetically rotated electric-arc air heater has been developed that is novel in that an intense magnetic field of the order of 10,000 to 25,000 gauss is employed. This field is supplied by a coil that is connected in series with the arc. Experimentation with this heater has shown that the presence of an intense magnetic field transverse to the arc results in diffusion of the arc and that the arc has a positive effective resistance. With the field coil in series with the arc, highly stable arc operation is obtained from a battery power supply. External ballast is not required to stabilize the arc when it is operating at maximum power level. The electrode erosion rate is so low that the airstream contamination is no more than 0.07 percent and may be substantially less.

COPPER↗

Hybrid composites - State-of-the-art review: Analysis, design, application and fabrication

The review covers hybrid composites that consist of two or more different types of fibers (or fiber composites) in a frequently repeated pattern in a laminate. The fibers considered are boron, graphite, glass, and Kevlar; the resins considered include mostly structural epoxies, with some utilization of polyimides and thermoplastics. The review shows that considerable data have been generated for the tensile strength properties, as well as tensile and thermal fatigue, of interply hybrids, and for the impact resistance of interply and intraply hybrids. The rule of mixtures appears to be adequate for predicting longitudinal and transverse mechanical properties of unidirectional interply hybrids, and linear laminate theory appears to be adequate for predicting the elastic response of hybrids.

Chamis, C. C.↗

Longitudinal shear behavior of several oxide dispersion strengthened alloys

Two commercial oxide dispersion strengthened (ODS) alloys, MA-753 and MA-754, and three experimental ODS alloys, MA-757E, MA-755E, and MA-6000E, were tested in shear at 760 C. Comparisons were made with other turbine blade and vane alloys. All of the ODS alloys exhibited less shear strength than directionally solidified Mar-M 200 = Hf or then conventionally cast B-1900. The strongest ODS alloy tested, MA-755E, was comparable in both shear and tensile strength to the lamellar directionally solidified eutectic alloy gamma/gamma prime - delta. Substantial improvements in shear resistance were found for all alloys tested when the geometry of the specimen was changed from one generating a transverse tensile stress in the shear area to one generating a transverse compressive stress. Finally, 760 C shear strength as a fraction of tensile strength was found to increase linearly with the log of the transverse tensile ductility.

Glasgow, T. K.↗

Longitudinal shear behavior of several oxide dispersion strengthened alloys

Two commercial oxide dispersion strengthened (ODS) alloys, MA-753 and MA-754, and three experimental ODS alloys, MA-757E, MA-755E, and MA-6000E, were tested in shear at 760 C. Comparisons were made with other turbine-blade and vane alloys. All of the ODS alloys exhibited less shear strength than directionally solidified Mar-M 200 + Hf or than conventionally cast B-1900. The strongest ODS alloy tested, MA-755E, was comparable in both shear and tensile strength to the lamellar directionally solidified eutectic alloy gamma/gamma-prime - delta. Substantial improvements in shear resistance were found for all alloys tested when the geometry of the specimen was changed from one generating a transverse tensile stress in the shear area to one generating a transverse compressive stress. Finally, 760-C shear strength as a fraction of tensile strength was found to increase linearly with the log of the transverse tensile ductility.

Glasgow, T. K.↗

Laminates Reinforced By Short Transverse Rods

Short transverse rods incorporated into laminated composite panels to increase interlaminar strengths of panels, according to proposal. Rods help panels resist delamination caused by impacts from dropped tools or, in vehicles, by debris. Inserted into selected individual internal layers during preimpregnation.

Farley, Gary L.↗

Point drag and total drag of navy struts no. 1 modified

This report deals with the results of tests on struts conducted at Washington Navy Yard. Two models of the modified Navy strut, no. 1, were tested in the 8 by 8 foot wind tunnel. The tests were made to determine the total resistance end effect and the pressure distribution at various wind-tunnel speeds with the length of the strut transverse to the current. Only the measurements made at zero pitch and yaw are given in this report.

Zahm, A F↗

Transverse flexural tests as a tool for assessing damage to PMR-15 composites from isothermal aging in air at elevated temperatures

To date, the effect of thermo-oxidative aging on unidirectional composite mechanical properties has been monitored by the measurement of interlaminar shear strength (ILSS) and either three or four point longitudinal flexural strength (LFS) of the composites being tested. Both results are affected by the fiber-to-matrix bonding, the former being dependent on the shear resistance of the interface and the latter on the degree of load sharing by the fibers through the fiber/matrix interface. Recently, fiber/matrix interfacial bond strengths have been monitored using a transverse flexural strength (TFS) test method. This test method was used to evaluate the effect of fiber surface treatment on the fiber/matrix bond. The interface bonding was varied in these tests using Hercules A-fibers with three-types of surfaces that produce bonds of poor, better, and good quality. The TFS was found not only to be sensitive to the bonding, but also to the aging time of unidirectional A-fiber/PMR-15 composites. This relationship reflects the mechanism by which the PMR-15 degrades during thermal aging.

Bowles, Kenneth J.↗

Transverse flexural tests as a tool for assessing damage to PMR-15 composites from isothermal aging in air at elevated temperatures

To date, the effect of thermo-oxidative aging on unidirectional composite mechanical properties has been monitored by the measurement of interlaminar shear strength (ILSS) and either three or four point longitudinal flexural strength (LFS) of the composites being tested. Both results are affected by the fiber-to-matrix bonding, the former being dependent on the shear resistance of the interface and the latter on the degree of load sharing by the fibers through the fiber/matrix interface. Recently, fiber/matrix interfacial bond strengths have been monitored using a transverse flexural strength (TFS) test method. This test method was used to evaluate the effect of fiber surface treatment on the fiber/matrix.

Bowles, Kenneth J.↗

Creep properties of PWC-11 base metal and weldments as affected by heat treatment

In a preliminary study using single specimens for each condition, PWC-11 (a niobium-base alloy with a nominal composition of Nb-1%Zr-0.1%C) was creep tested at 1350 K and 40 MPa. Base metal specimens and specimens with transverse electron beam welds were tested with and without a 1000 hr, 1350 K aging treatment prior to testing. In the annealed condition (1 hr at 1755 K + 2 hr at 1475 K), the base metal exhibited superior creep strength compared to the nonaged condition, reaching 1 percent strain in 3480 hr. A 1000 hr, 1350 K aging treatment prior to creep testing had a severe detrimental effect on creep strength of the base metal and transverse electron beam weldments, reducing the time to attain 1 percent strain by an order of magnitude. Extrapolated temperature compensated creep rates indicate that the present heat of PWC-11 may be four times as creep resistant as similarly tested Nb-1%Zr. The extrapolated stress to achieve 1 percent creep strain in 7 yr at 1350 K is 2.7 MPa for annealed Nb-1%Zr and 12 MPa for annealed and aged PWC-11 base metal with and without a transverse electron beam weld.

Titran, R. H.↗