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At least 721 records · Page 40

Radioactive Source Localization via Bayesian Particle Filter

In the event of a misplaced radioactive source or other emergency situation, measuring a radiation field, mapping its distribution, and determining a source location are essential tasks to ameliorating the situation. However, radiation fields may be extremely hazardous to human surveyors and minimizing received radiation doses is just as essential. Robots appear to be a potential solution to these problems. Beyond simply measuring radiation, the robot's computer processing capabilities offer a way to apply complex data analysis methods to radiation measurements in real-time. Methods which predict likely source locations can then feed this information into other processes, potentially improving path planning and enabling more efficient measurements. Given a robot mounted with a gamma-ray detector, can we: develop a methodology to account for detector performance across a wide range of source angles, distances, and photon energies? operate an autonomously navigating robot to effectively survey and characterize an area of interest? implement a data analysis method, conventionally used in measurements of motion, for source localization purposes? An open-source TurtleBot 3 robot, running Robot Operating System (ROS) on Ubuntu 16.04 LTS, was fitted with a Kromek GR1{sup R} Cadmium Zinc Telluride (CZT) solid-state gamma-ray detector. As a part of ROS, the packages OpenSlam, gmapping, and amcl were used to perform Simultaneous Localization and Mapping (SLAM), determining the robot's position and mapping the surrounding area. Data was acquired via Lidar mounted on top the TurtleBot 3. Detector Calibration Fit: The equation was fit to 365 counts of various energies, distances, and angles. A MATLAB{sup R} program was written to simulate measurements taken a robot on a random walk, with count data and positions discretized into finite element pixels. Using this program, a sample of 100 runs was performed on a map with a simulated source at the center, with a total of 200 of 2 pixels each. Similarly, multiple runs of the filter were performed on recorded robot measurement data. In both simulation and real tests, when corrected for errors (particles placed outside of bounds or on the robot, and simulation-specific errors), corresponding t-tests of predicted x and y-coordinates were within a 95% confidence interval of the actual position. For the real trial, these positions are slightly skewed right in the x-axis as the robot remained mainly to the left side of the source within the sample area. These simulations demonstrate potential validity for the usage of a particle filter as method of radioactive source localization. In the future, true real-time implementation and data fusion may further augment the performance of the robot to localize lost sources. Additionally, identification of multiple sources, determination of source types, and usage of a collimator are areas to potentially be explored.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Resolving small signal measurements in experimental plasma environments using calibrated subtraction of noise signals

The performance of many diagnostic and control systems within fusion and other fields of research are often detrimentally affected by spurious noise signals. This is particularly true for those (such as radiation or particle detectors) working with very small signals. Common sources of radiated and conducted noise in experimental fusion environments include the plasma itself and instrumentation. The noise complicates data analysis, as illustrated by noise on signals measured with the heavy ion beam probe (HIBP) installed on the Madison Symmetric Torus. The noise is time-varying and often exceeds the secondary ion beam current (in contrast with previous applications). Analysis of the noise identifies the dominant source as photoelectric emission from the detectors induced by ultraviolet light from the plasma. This has led to the development of a calibrated subtraction technique, which largely removes the undesired temporal noise signals from data. The advantages of the technique for small signal measurement applications are demonstrated through improvements realized on HIBP fluctuation measurements.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Flash Infrared Thermography Contrast Data Analysis Technique

This paper provides information on an IR Contrast technique that involves extracting normalized contrast versus time evolutions from the flash thermography inspection infrared video data. The analysis calculates thermal measurement features from the contrast evolution. In addition, simulation of the contrast evolution is achieved through calibration on measured contrast evolutions from many flat-bottom holes in the subject material. The measurement features and the contrast simulation are used to evaluate flash thermography data in order to characterize delamination-like anomalies. The thermal measurement features relate to the anomaly characteristics. The contrast evolution simulation is matched to the measured contrast evolution over an anomaly to provide an assessment of the anomaly depth and width which correspond to the depth and diameter of the equivalent flat-bottom hole (EFBH) similar to that used as input to the simulation. A similar analysis, in terms of diameter and depth of an equivalent uniform gap (EUG) providing a best match with the measured contrast evolution, is also provided. An edge detection technique called the half-max is used to measure width and length of the anomaly. Results of the half-max width and the EFBH/EUG diameter are compared to evaluate the anomaly. The information provided here is geared towards explaining the IR Contrast technique. Results from a limited amount of validation data on reinforced carbon-carbon (RCC) hardware are included in this paper.

Koshti, Ajay↗

Dual-angle, self-calibrating Thomson scattering measurements in RFX-MOD

In the multipoint Thomson scattering (TS) system of the RFX-MOD experiment the signals from a few spatial positions can be observed simultaneously under two different scattering angles. In addition the detection system uses optical multiplexing by signal delays in fiber optic cables of different length so that the two sets of TS signals can be observed by the same polychromator. Owing to the dependence of the TS spectrum on the scattering angle, it was then possible to implement self-calibrating TS measurements in which the electron temperature T{sub e}, the electron density n{sub e} and the relative calibration coefficients of spectral channels sensitivity C{sub i} were simultaneously determined by a suitable analysis of the two sets of TS data collected at the two angles. The analysis has shown that, in spite of the small difference in the spectra obtained at the two angles, reliable values of the relative calibration coefficients can be determined by the analysis of good S/N dual‑angle spectra recorded in a few tens of plasma shots. This analysis suggests that in RFX-MOD the calibration of the entire set of TS polychromators by means of the similar, dual-laser (Nd:YAG/Nd:YLF) TS technique, should be feasible.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Performance optimization of CO 2 heat pump water heater

A preliminary analysis was conducted to analyze the performance of a heat pump water heater (HPWH) that uses CO 2 as the refrigerant. A model to predict the performance was developed and calibrated based on the experimental data for an existing HPWH using a CO 2 refrigerant. The calibrated model was then used to run a parametric analysis in which factors such as water supply temperature, water circulation rate, tank stratification, and condenser configuration were considered. The performance of a commercial CO 2 system was compared with that of a similar system using R-134a as the refrigerant. It was found that CO 2 HPWH performance was comparable to that of an R-134a HPWH, more so for a separated gas cooler configuration. For comparable performance, the compressor size and the tube-in-tube heat exchanger (condenser/gas cooler) size were compared for CO 2 - and R-134a-based systems. Finally, the impact of the water circulation rate on the water temperature stratification in the tank, an essential requirement for higher performance for CO 2 HPWH systems was also investigated.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

Using IR spectroscopy to determine biodiesel conversion

This project’s aim was to develop a way to use Infrared (IR) Spectroscopy to determine the extent of the conversion of oil to biodiesel produced during a typical transesterification process. The most reliable method of biodiesel analysis is gas chromatography with flame ionization detector (GC-FID) analysis. This analysis is not ideal for the educational or field applications since it is time intensive and requires expensive, specialized equipment. The use of the FT-IR is faster and more affordable. A calibration curve was created by comparing data on the purity of biodiesel samples obtained from the GC-FID analysis to the ratio of the absorbances at 1197 cm -1 to 1166 cm -1 from the FT-IR spectrum. For field application, a similar method was developed using a portable IR spectrometer, the InfraSpecTM VFA-IR spectrometer. As a result, the data collected gave a good linear fit for % purity of the samples and can be used as a method for monitoring the conversion of different types of oils to biodiesel and determining the purity of biodiesel produced from oil.

09 BIOMASS FUELS↗

Assessing the Validity of the Simplified Potential Energy Clock Model for Modeling Glass-Ceramics

Glass-ceramic seals may be the future of hermetic connectors at Sandia National Laboratories. They have been shown capable of surviving higher temperatures and pressures than amorphous glass seals. More advanced finite-element material models are required to enable model-based design and provide evidence that the hermetic connectors can meet design requirements. Glass-ceramics are composite materials with both crystalline and amorphous phases. The latter gives rise to (non-linearly) viscoelastic behavior. Given their complex microstructures, glass-ceramics may be thermorheologically complex, a behavior outside the scope of currently implemented constitutive models at Sandia. However, it was desired to assess if the Simplified Potential Energy Clock (SPEC) model is capable of capturing the material response. Available data for SL 16.8 glass-ceramic was used to calibrate the SPEC model. Model accuracy was assessed by comparing model predictions with shear moduli temperature dependence and high temperature 3-point bend creep data. It is shown that the model can predict the temperature dependence of the shear moduli and 3- point bend creep data. Analysis of the results is presented. Suggestions for future experiments and model development are presented. Though further calibration is likely necessary, SPEC has been shown capable of modeling glass-ceramic behavior in the glass transition region but requires further analysis below the transition region.

36 MATERIALS SCIENCE↗

Data Analysis for the Scintillating Optical Fiber Calorimeter (SOFCAL)

The scintillating optical fiber calorimeter is a hybrid instrument with both active and passive components for measuring the proton and helium cosmic ray spectra from 0.2 to IO TeV kinetic energy. A thin emulsion/x-ray film chamber is situated between a cerenkov counter and an imaging calorimeter. Scintillating optical fibers sample the electromagnetic showers that develop in the calorimeter and identify the trajectory of cosmic rays that interact in SOFCAL. The emulsion/x-ray film data provide an in flight calibration for SOFCAL. The data reduction techniques used will be discussed and interim results of the analysis from a 20 hour balloon flight will be presented.

Christl, Mark J.↗

Multiphysics Lattice Discrete Particle Modeling (M-LDPM) for the Simulation of Shale Fracture Permeability

A three-dimensional multiphysics lattice discrete particle model (M-LDPM) framework is formulated to investigate the fracture permeability behavior of shale. The framework features a dual lattice system mimicking the mesostructure of the material and simulates coupled mechanical and flow behavior. The mechanical lattice model simulates the granular internal structure of shale, and describes heterogeneous deformation by means of discrete compatibility and equilibrium equations. The network of flow lattice elements constitutes a dual graph of the mechanical lattice system. A discrete formulation of mass balance for the flow elements is presented to model fluid flow along cracks and intact materials. The overall computational framework is implemented with a mixed explicit–implicit integration scheme and a staggered coupling method that makes use of the dual lattice topology enabling the seamless two-way coupling of the mechanical and flow behaviors. The proposed model is used for the computational analysis of shale fracture permeability behavior by simulating triaxial direct shear tests on Marcellus shale specimens under various confining pressures. The simulated mechanical response is calibrated against the experimental data, and the predicted permeability values are also compared with the experimental measurements. Moreover, the paper presents the scaling analysis of both the mechanical response and permeability measurements based on simulations performed on geometrically similar specimens with increasing size. The simulated stress strain curves reflect a significant size effect in the post-peak due to the presence of localized fractures. The scaling analysis of permeability measurements enables prediction of permeability for large specimens by extrapolating the numerical results of small ones.

58 GEOSCIENCES↗

Energy dependent calibration of XR-QA2 radiochromic film with monochromatic and polychromatic x-ray beams

Purpose: This work investigates the energy response and dose-response curve determinations for XR-QA2 radiochromic film dosimetry system used for synchrotron radiation work and for quality assurance in diagnostic radiology, in the range of effective energies 18–46.5 keV. Methods: Pieces of XR-QA2 films were irradiated, in a plane transverse to the beam axis, with a monochromatic beam of energy in the range 18–40 keV at the ELETTRA synchrotron radiation facility (Trieste, Italy) and with a polychromatic beam from a laboratory x-ray tube operated at 80, 100, and 120 kV. The film calibration curve was expressed as air kerma (measured free-in-air with an ionization chamber) versus the net optical reflectance change (netΔR) derived from the red channel of the RGB scanned film image. Four functional relationships (rational, linear exponential, power, and logarithm) were tested to evaluate the best curve for fitting the calibration data. The adequacy of the various fitting functions was tested by using the uncertainty analysis and by assessing the average of the absolute air kerma error calculated as the difference between calculated and delivered air kerma. The sensitivity of the film was evaluated as the ratio of the change in net reflectance to the corresponding air kerma. Results: The sensitivity of XR-QA2 films increased in the energy range 18–39 keV, with a maximum variation of about 170%, and decreased in the energy range 38–46.5 keV. The present results confirmed and extended previous findings by this and other groups, as regards the dose response of the radiochromic film XR-QA2 to monochromatic and polychromatic x-ray beams, respectively. Conclusions: The XR-QA2 radiochromic film response showed a strong dependence on beam energy for both monochromatic and polychromatic beams in the range of half value layer values from 0.55 to 6.1 mm Al and corresponding effective energies from 18 to 46.5 keV. In this range, the film response varied by 170%, from a minimum sensitivity of 0.0127 to a maximum sensitivity of 0.0219 at 10 mGy air kerma in air. The more suitable function for air kerma calibration of the XR-QA2 radiochromic film was the power function. A significant batch-to-batch variation, up to 55%, in film response at 120 kV (46.5 keV effective energy) was observed in comparison with published data.

61 RADIATION PROTECTION AND DOSIMETRY↗

In Pursuit of a High-Temperature, High-Pressure, High-Viscosity Standard: The Case of Tris(2-ethylhexyl) Trimellitate

This study presents a reference correlation for the viscosity of tris(2-ethylhexyl) trimellitate designed to serve in industrial applications for the calibration of viscometers at elevated temperatures and pressures such as those encountered in the exploration of oil reservoirs and in lubrication. Tris(2-ethylhexyl) trimellitate has been examined with respect to the criteria necessary for an industrial standard reference material such as toxicity, thermal stability, and variability among manufactured lots. The viscosity correlation has been based upon all of the data collected in a multinational project and is supported by careful measurements and analysis of all the supporting thermophysical property data that are needed to apply the standard for calibration to a wide variety of viscometers. The standard reference viscosity data cover temperatures from 303 to 473 K, pressures from 0.1 to 200 MPa, and viscosities from approximately 1.6 to 755 mPa s. The uncertainty in the data provided is of the order of 3.2% at 95% confidence level, which is thought to be adequate for most industrial applications.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

An Analysis of the Side Slither On-Orbit Calibration Technique Using the DIRSIG Model

Pushbroom-style imaging systems exhibit several advantages over line scanners when used on space-borne platforms as they typically achieve higher signal-to-noise and reduce the need for moving parts. Pushbroom sensors contain thousands of detectors, each having a unique radiometric response, which will inevitably lead to streaking and banding in the raw data. To take full advantage of the potential exhibited by push broom sensors, a relative radiometric correction must be performed to eliminate pixel-to-pixel non-uniformities in the raw data. Side slither is an on-orbit calibration technique where a 90-degree yaw maneuver is performed over an invariant site to flatten the data. While this technique has been utilized with moderate success for the QuickBird satellite and the RapidEye constellation, further analysis is required to enable its implementation for the Landsat 8 sensors, which have a 15-degree field-of-view and a 0.5% pixel-to-pixel uniformity requirement. This work uses the DIRSIG model to analyze the side slither maneuver as applicable to the Landsat sensor. A description of favorable sites, how to adjust the maneuver to compensate for the curvature of "linear" arrays, how to efficiently process the data, and an analysis to assess the quality of the side slither data, are presented.

Side slither↗

CATLAC - Calibration and Validation Analysis Tool of Local Area Coverage for the SeaWiFS Mission

Calibration and validation Analysis Tool of Local Area Coverage (CATLAC) is an analysis package for selecting and graphically displaying Earth and space targets for calibration and validation activities on a polar orbiting satellite. The package is written in the Interactive Data Language (IDL) and includes a graphical user interface. Although it is designed specifically for the Sea-viewing Wide Field-of-view Sensor (SeaWiFS) mission, the package can be used for analysis on other Earth-viewing missions. An individual can use text or graphical methods in CATLAC to select Earth targets to be scanned by a satellite. Additional onboard calibration activities (such as observations of the moon, or solar irradiance from a solar diffuser), which use data recorder time, can also be specified. All information pertinent to the creation of a command schedule can be written to a file which is read by a command scheduler. The scheduler can be invoked and the Local Area Coverage (LAC) recording periods can be visually verified using CATLAC. The schedule can also be verified by examining record and error files written by the scheduler.

Woodward, Robert H.↗

Kinetic model development and Bayesian uncertainty quantification for the complete reduction of Fe-based oxygen carriers with CH 4 , CO, and H 2 for chemical looping combustion

In this work, three kinetic models are developed and calibrated for the complete multi-step reduction of an Fe-based oxygen carrier (OC) particle with CH 4 , CO, and H 2 , using data from thermogravimetric analysis. The complete reduction rate profiles exhibit complex dynamics whose trajectory is significantly different depending on the reducing gas. A Bayesian model building and parameter estimation framework is applied for simultaneous parameter and model structure uncertainty quantification. The final models show excellent agreement between model predictions and calibration data, as well as new data not used for calibration (for the reduction of the OC with CH 4 ). Parameter uncertainty is quantified by determining joint posterior distribution, and model structure uncertainty is addressed by incorporating Gaussian process stochastic functions (represented by Bayesian smoothing splines) into the kinetic models. The final kinetic models with discrepancy functions are readily employable in equation-oriented simulation and optimization platforms.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Extension and Statistical Analysis of the GACP Aerosol Optical Thickness Record.

The primary product of the Global Aerosol Climatology Project (GACP) is a continuous record of the aerosol optical thickness (AOT) over the oceans. It is based on channel-1 and -2 radiance data from the Advanced Very High Resolution Radiometer (AVHRR) instruments flown on successive National Oceanic and Atmospheric Administration (NOAA) platforms. We extend the previous GACP dataset by four years through the end of 2009 using NOAA-17 and -18 AVHRR radiances recalibrated against MODerate resolution Imaging Spectroradiometer (MODIS) radiance data, thereby making the GACP record almost three decades long. The temporal overlap of over three years of the new NOAA-17 and the previous NOAA-16 record reveals an excellent agreement of the corresponding global monthly mean AOT values, thereby confirming the robustness of the vicarious radiance calibration used in the original GACP product. The temporal overlap of the NOAA-17 and -18 instruments is used to introduce a small additive adjustment to the channel-2 calibration of the latter resulting in a consistent record with increased data density. The Principal Component Analysis (PCA) of the newly extended GACP record shows that most of the volcanic AOT variability can be isolated into one mode responsible for ~12% of the total variance. This conclusion is confirmed by a combined PCA analysis of the GACP, MODIS, andMulti-angle Imaging SpectroRadiometer (MISR) AOTs during the volcano-free period fromFebruary 2000 to December 2009.We show that the modes responsible for the tropospheric AOT variability in the three datasets agree well in terms of correlation and spatial patterns. A previously identified negative AOT trend which started in the late 1980s and continued into the early 2000s is confirmed. Its magnitude and duration indicate that it was caused by changes in tropospheric aerosols. The latest multi-satellite segment of the GACP record shows that this trend tapered off, with no noticeable AOT change after 2002. This result is consistent with the MODIS andMISR AOT records as well as with the recent gradual reversal frombrightening to dimming revealed by surface flux measurements in many aerosol producing regions. Thus the robustness of the GACP record is confirmed, increasing our confidence in the validity of the negative trend. Although the nominal negative GACP AOT trend could partially be an artifact of increasing aerosol absorption, we argue that the time dependence of the GACP record, including the latest flat period, is more consistent with the actual decrease in the tropospheric AOT.

aerosols↗

Analysis of aircraft microwave measurements of the ocean surface

A data system was developed to process, from calibrated brightness temperature to computation of estimated parameters, the microwave measurements obtained by the NASA CV-990 aircraft during the 1972 Meteorological Expedition. A primary objective of the study was the implementation of an integrated software system at the computing facility of NASA/GSFC, and its application to the 1972 data. A single test case involving measurements away from and over a heavy rain cell was chosen to examine the effect of clouds upon the ability to infer ocean surface parameters. The results indicate substantial agreement with those of the theoretical study; namely, that the values obtained for the surface properties are consistent with available ground-truth information, and are reproducible except within the heaviest portions of the rain cell, at which nonlinear (or saturation) effects become apparent. Finally, it is seen that uncorrected instrumental effects introduce systematic errors which may limit the accuracy of the method.

Willand, J. H.↗

Measuring SNM Isotopic Distributions using FRAM

The first group of slides provides background information on the isotopic composition of plutonium. It is shown that 240 Pu is the critical isotope in neutron coincidence/multiplicity counting. Next, response function analysis to determine isotopic composition is discussed. The isotopic composition can be determined by measuring the net peak counts from each isotope and then taking the ratio of the counts for each isotope relative to the total counts for the element. Then FRAM (Fixed energy Response function Analysis with Multiple efficiencies) is explained. FRAM can control data acquisition, automatically analyze newly acquired data, analyze previously acquired data, provide information on the quality of the analysis, and facilitate analysis in unusual situations (non-standard energy calibrations, gamma rays from non-SNM isotopes, poor spectra (within limits)).

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

TRMM-Based Merged Precipitation Analyses

This paper describes results of using Tropical Rainfall Measuring Mission (TRMM) information as the key calibration tool in a merged analysis on a 1X1 latitude/longitude monthly scale based on multiple satellite sources and raingauge analyses. The TRMM-based product is compared with surface-based validation data sets and the community-based 20-year Global Precipitation Climatology Project (GPCP)monthly analyses. The TRMM-based merged analysis uses the TRMM information to calibrate the estimates from SSM/I and geosynchronous IR observations and merges those estimates together with the TRMM and gauge information to produce accurate rainfall estimates with the increased sampling provided by the combined satellite information. This TRMM merged analysis uses the combined instrument (Precipitation Radar [PR] and TRMM Microwave Imager [TMI]) retrieval of Haddad as the TRMM estimate with which to calibrate the other satellite estimates. This TRMM Combined instrument (TCI) estimate is shown to produce very similar absolute values to the other main TRMM products. The TRMM and other satellites merged analysis compares favorably to the atoll data set of Morrissey for the months of 1998 with a very small positive bias of 2%. However, comparison with the preliminary results from the TRMM ground validation radar information at Kwajalein atoll in the western Pacific Ocean shows a 26% positive bias. Therefore, absolute magnitudes from TRMM and/or the ground validation need to be treated with care at this point. A month by month comparison of the TRMM merged analysis and the GPCP analysis indicates very similar patterns, but with subtle differences in magnitude. Focusing on the Pacific Ocean ITCZ one can see the TRMM-based estimates having higher peak values and lower values in the ITCZ periphery. These attributes also show up in the statistics, where GPCP>TRMM at low values (below 10 mm/d) and TRMM>GPCP at high values (greater than 15 mm/d). Integrated over the 37N-37S belt for all of 1998 the TRMM value is 3.1 mm/day compared to 2.9 mm/day for GPCP, with the results when confined to ocean being 3.3 and 3.0, respectively. Therefore, TRMM has approximately 10% higher tropical oceanic precipitation than GPCP. Examples of TRMM monthly fields in analysis of geographic and temporal variations will also be discussed. Results for 1998 indicate that TRMM has a different ratio of western Pacific to eastern Pacific rainfall than GPCP, perhaps indicating that TRMM's ability to discern the vertical structure of the rain may lead to better estimates in the eastern Pacific. In addition the rainfall anomalies associated with the '98-'99 ENSO event are shown to be larger with the TRMM results as compared to the GPCP analyses.

Adler, Robert↗