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At least 721 records · Page 40

Single- and dual-variant atomic ordering in GaAsP compositionally graded buffers on GaP and Si substrates

Here, we investigate the material properties of GaAsP graded buffers on both GaP and Si substrates in order to determine limitations to dislocation glide in GaAsP. Phase separation is not observed in these GaAsP buffers, but CuPt B atomic ordering is present, and has an impact on the Burgers vector distribution of gliding dislocations. Tellurium surfactant eliminates ordering in GaAsP, allowing control over the glide plane distribution while highlighting the importance of the growth surface and choice of dopant. The impact of single-variant CuPtB ordering of GaAsP buffers grown on GaP substrates is investigated by monitoring the threading dislocation density throughout the buffer in sequential steps. The dislocation density rises steadily throughout the graded buffer, implying that factors other than ordering-induced glide plane switches play a dominant role in the final dislocation density. We observe an increase in surface roughness throughout the buffer and speculate that a dislocation nucleation source on the surface has a low activation energy and may lead to increased threading dislocation density. On Si substrates, the GaAsP buffer displays dual-variant CuPt B ordering rather than single-variant ordering due to the surface step geometry. We discuss how dual-variant ordering leads to a variable glide force, and thus has a different impact on dislocation dynamics than single-variant ordering. Because the III-V on Si nucleation procedure determines the step geometry, it also influences the dislocation dynamics.

36 MATERIALS SCIENCE↗

Gravitational scattering and beyond from extreme mass ratio effective field theory

We explore a recently proposed effective field theory describing electromagnetically or gravitationally interacting massive particles in an expansion about their mass ratio, also known as the self-force (SF) expansion. By integrating out the deviation of the heavy particle about its inertial trajectory, we obtain an effective action whose only degrees of freedom are the lighter particle together with the photon or graviton, all propagating in a Coulomb or Schwarzschild background. The 0SF dynamics are described by the usual background field method, which at 1SF is supplemented by a “recoil operator” that encodes the wobble of the heavy particle, and similarly computable corrections appearing at 2SF and higher. Our formalism exploits the fact that the analytic expressions for classical backgrounds and particle trajectories encode dynamical information to all orders in the couplings, and from them we extract multiloop integrands for perturbative scattering. As a check, we study the two-loop classical scattering of scalar particles in electromagnetism and gravity, verifying known results. We then present new calculations for the two-loop classical scattering of dyons, and of particles interacting with an additional scalar or vector field coupling directly to the lighter particle but only gravitationally to the heavier particle.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Convective Heat Transfer in the Reusable Solid Rocket Motor of the Space Transportation System

This simulation involved a two-dimensional axisymmetric model of a full motor initial grain of the Reusable Solid Rocket Motor (RSRM) of the Space Transportation System (STS). It was conducted with CFD (computational fluid dynamics) commercial code FLUENT. This analysis was performed to: a) maintain continuity with most related previous analyses, b) serve as a non-vectored baseline for any three-dimensional vectored nozzles, c) provide a relatively simple application and checkout for various CFD solution schemes, grid sensitivity studies, turbulence modeling and heat transfer, and d) calculate nozzle convective heat transfer coefficients. The accuracy of the present results and the selection of the numerical schemes and turbulence models were based on matching the rocket ballistic predictions of mass flow rate, head end pressure, vacuum thrust and specific impulse, and measured chamber pressure drop. Matching these ballistic predictions was found to be good. This study was limited to convective heat transfer and the results compared favorably with existing theory. On the other hand, qualitative comparison with backed-out data of the ratio of the convective heat transfer coefficient to the specific heat at constant pressure was made in a relative manner. This backed-out data was devised to match nozzle erosion that was a result of heat transfer (convective, radiative and conductive), chemical (transpirating), and mechanical (shear and particle impingement forces) effects combined.

Ahmad, Rashid A.↗

Amyloplasts are necessary for full gravitropic sensitivity in roots of Arabidopsis thaliana

The observation that a starchless mutant (TC7) of Arabidopsis thaliana (L.) Heynh. is gravitropic (T. Caspar and B.G. Pickard, 1989, Planta 177, 185-197) raises questions about the hypothesis that starch and amyloplasts play a role in gravity perception. We compared the kinetics of gravitropism in this starchless mutant and the wild-type (WT). Wild-type roots are more responsive to gravity than TC7 roots as judged by several parameters: (1) Vertically grown TC7 roots were not as oriented with respect to the gravity vector as WT roots. (2) In the time course of curvature after gravistimulation, curvature in TC7 roots was delayed and reduced compared to WT roots. (3) TC7 roots curved less than WT roots following a single, short (induction) period of gravistimulation, and WT, but not TC7, roots curved in response to a 1-min period of horizontal exposure. (4) Wild-type roots curved much more than TC7 roots in response to intermittent stimulation (repeated short periods of horizontal exposure); WT roots curved in response to 10 s of stimulation or less, but TC7 roots required 2 min of stimulation to produce a curvature. The growth rates were equal for both genotypes. We conclude that WT roots are more sensitive to gravity than TC7 roots. Starch is not required for gravity perception in TC7 roots, but is necessary for full sensitivity; thus it is likely that amyloplasts function as statoliths in WT Arabidopsis roots. Furthermore, since centrifugation studies using low gravitational forces indicated that starchless plastids are relatively dense and are the most movable component in TC7 columella cells, the starchless plastids may also function as statoliths.

NASA Discipline Plant Biology↗

Effects of Traveling Magnetic Field on Dynamics of Solidification

TMF is based on imposing a controlled phase-shift in a train of electromagnets, forming a stack. Thus, the induced magnetic field can be considered to be travelling along the axis of the stack. The coupling of this traveling wave with an electrically conducting fluid results in a basic flow in a form of a single axisymmetric roll. The magnitude and direction of this flow can be remotely controlled. Furthermore, it is possible to localize the effect of this force field though activating only a number of the magnets. This force field generated in the fluid can, in principle, be used to control and modify convection in the molten material. For example, it can be used to enhance convective mixing in the melt, and thereby modify the interface shape, and macrosegregation. Alternatively, it can be used to counteract thermal and/or solutal buoyancy forces. High frequency TMF can be used in containerless processing techniques, such as float zoning, to affect the very edge of the fluid so that Marangoni flow can be counter balanced. The proposed program consists of basic fundamentals and applications. Our goal in conducting the following experiments and analyses is to establish the validity of TMF as a new tool for solidification processes. Due to its low power consumption and simplicity of design, this tool may find wide spread use in a variety of space experiments. The proposed ground based experiments are intended to establish the advantages and limitations of employing this technique. In the fundamentals component of the proposed program, we will use theoretical tools and experiments with mercury to establish the fundamental aspects of TMF-induced convection through a detailed comparison of theoretical predictions and experimental measurements of flow field. In this work, we will conduct a detailed parametric study involving the effects of magnetic field strength, frequency, wave vector, and the fluid geometry. The applications component of this work will be focused on investigating the effect of TMF on the following solidification and pre-directional solidification processes: (1) Bridgman growth of Ga:Ge with the goal of counteracting the buoyancy-driven convection; (2) Mixing of Pb-Ga and Pb-Sn alloys with the aim of initiating and maintaining a uniform melt prior to solidification processing; and (3) Float Zone growth with the aim of identifying, through simulations and model experiments, conditions needed to counteract Marangoni flow in a microgravity environment. The proposed research has strong relevance to microgravity research and the objectives of the NRA. TMF can provide a unique and accurate mechanism for generation and control of desirable flow patterns for microgravity research. These attributes have significant relevance to 1) Alloy mixing prior to solidification in a microgravity environment. TMF can provide this mixing with a low level of power consumption; (2) TMF can offset the deleterious effects of Marangoni convection in microgravity containerless processing. Thus, TMF can be instrumental in further understanding this phenomena; (3) Generation of controlled flows will allow the investigation of the effect of these flows on growth morphology and growth kinetics; and (4) On Earth, TMF has the potential to significantly counter-balance thermosolutal convection, thereby creating conditions similar to those obtained in microgravity. Once demonstrated, this new tool for use in solidification has the strong potential to find applications in a host of microgravity material research projects.

Mazuruk, Konstantin↗

Range Safety Flight Elevation Limit Calculation Software

This program was developed to fill a need within the Wallops Flight Facility workflow for automation of the development of vertical plan limit lines used by flight safety officers during the conduct of expendable launch vehicle missions. Vertical plane present-position-based destruct lines have been used by range safety organizations at numerous launch ranges to mitigate launch vehicle risks during the early phase of flight. Various ranges have implemented data submittal and processing workflows to develop these destruct lines. As such, there is significant prior art in this field. The ElLimits program was developed at NASA's Wallops Flight Facility to automate the process for developing vertical plane limit lines using current computing technologies. The ElLimits program is used to configure launch-phase range safety flight control lines for guided missiles. The name of the program derives itself from the fundamental quantity that is computed - flight elevation limits. The user specifies the extent and resolution of a grid in the vertical plane oriented along the launch azimuth. At each grid point, the program computes the maximum velocity vector flight elevation that can be permitted without endangering a specified back-range location. Vertical plane x-y limit lines that can be utilized on a present position display are derived from the flight elevation limit data by numerically propagating 'streamlines' through the grid. The failure turn and debris propagation simulation technique used by the application is common to all of its analysis options. A simulation is initialized at a vertical plane grid point chosen by the program. A powered flight failure turn is then propagated in the plane for the duration of the so-called RSO reaction time. At the end of the turn, a delta-velocity is imparted, and a ballistic trajectory is propagated to impact. While the program possesses capability for powered flight failure turn modeling, it does not require extensive user inputs of vehicle characteristics (e.g., thrust and aerodynamic data), nor does it require reams of turn data after the traditional fashion of the Air Force ranges. The program requires a nominal trajectory table (time, altitude, range, velocity, and flight elevation) and makes heavy use of it to initialize and model a failure turn.

Lanzi, Raymond J↗

Evaluation of Separation Mechanism Design for the Orion/Ares Launch Vehicle

As a part of the preliminary design work being performed for the Orion vehicle, the Orion to Spacecraft Adaptor (SA) separation mechanism was analyzed and sized, with findings presented here. Sizing is based on worst case abort condition as a result of an anomaly driving the launch vehicle engine thrust vector control hard-over causing a severe vehicle pitch over. This worst-case scenario occurs just before Upper Stage Main Engine Cut-Off when the vehicle is the lightest and the damping effect due to propellant slosh has been reduced to a minimum. To address this scenario and others, two modeling approaches were invoked. The first approach was a detailed Simulink model to quickly assess the Service Module Engine nozzle to SA clearance for a given separation mechanism. The second approach involved the generation of an Automatic Dynamic Analysis of Mechanical Systems (ADAMS) model to assess secondary effects due to mass centers of gravity that were slightly off the vehicle centerline. It also captured any interference between the Solar Arrays and the Spacecraft Adapter. A comparison of modeling results and accuracy are discussed. Most notably, incorporating a larger SA flange diameter allowed for a natural separation of the Orion and its engine nozzle even at relatively large pitch rates minimizing the kickoff force. Advantages and disadvantages of the Simulink model vs. a full geometric ADAMS model are discussed as well.

Konno, Kevin E.↗

Evaluation of Separation Mechanism Design for the Orion/Ares Launch Vehicle

As a part of the preliminary design work being performed for the Orion vehicle, the Orion to Spacecraft Adaptor (SA) separation mechanism mechanism was analyzed and sized, with findings presented here. Sizing is based on worst case abort condition as a result of an anomaly driving the launch vehicle engine thrust vector control hard-over causing a severe vehicle pitch over. This worst case scenario occurs just before Upper Stage Main Engine Cut-Off (MECO) when the vehicle is the lightest and the damping effect due to propellant slosh has been reduced to a minimum. To address this scenario and others, two modeling approaches were invoked. The first approach was a detailed Simulink model to quickly assess the Service Module Engine nozzle to SA clearance for a given separation mechanism. The second approach involved the generation of an Automatic Dynamic Analysis of Mechanical Systems (ADAMS) model to assess secondary effects due to mass centers of gravity that were slightly off the vehicle centerline. It also captured any interference between the Solar Arrays and the Spacecraft Adapter. A comparison of modeling results and accuracy are discussed. Most notably, incorporating a larger SA flange diameter allowed for a natural separation of the Orion and its engine nozzle even at relatively large pitch rates minimizing the kickoff force. Advantages and disadvantages of the Simulink model vs. a full geometric ADAMS model are discussed as well.

Konno, Kevin E.↗

Recent Developments and Status of the Langley Single Vector Balance Calibration System (SVS)

The Langley Research Center (LaRC) Single Vector Balance Calibration System (SVS) was first introduced in 2000 by Peter Parker. The SVS combines the Design of Experiments (DOE) methodology with a novel load application system. Since that time three systems have been designed and developed with different load range capabilities (ranging from 2 pounds to 3,000 pounds). Approximately fifteen balances have been calibrated and their data compared to conventional techniques. This paper will present results of these comparisons, based on the mathematical models and accuracies, and discuss differences that were observed. In addition, changes in the implementation of the initial load schedules developed using DOE will be highlighted. One of the principles behind DOE is randomization. The initial loading schedules used to date have been randomized in the traditional DOE sense but not for repeat calibrations or experiments. Implementation of this randomization within blocks and its impact on data quality will be reviewed. Areas of potential future development will be presented which include changes in the centers to include loads with the force position system in the pure error estimates.

Jones, Shirley M.↗

Evaluation of Separation Mechanism Design for the Orion/Ares Launch Vehicle

As a part of the preliminary design work being performed for the Orion vehicle, the Orion to Spacecraft Adaptor (SA) separation mechanism was analyzed and sized, with findings presented here. Sizing is based on worst case abort condition as a result of an anomaly driving the launch vehicle engine thrust vector control hard-over causing a severe vehicle pitch over. This worst case scenario occurs just before Upper Stage Main Engine Cut-Off (MECO) when the vehicle is the lightest and the damping effect due to propellant slosh has been reduced to a minimum. To address this scenario and others, two modeling approaches were invoked. The first approach was a detailed Simulink model to quickly assess the Service Module Engine nozzle to SA clearance for a given separation mechanism. The second approach involved the generation of an Automatic Dynamic Analysis of Mechanical Systems (ADAMS) model to assess secondary effects due to mass centers of gravity that were slightly off the vehicle centerline. It also captured any interference between the Solar Arrays and the Spacecraft Adapter. A comparison of modeling results and accuracy are discussed. Most notably, incorporating a larger SA flange diameter allowed for a natural separation of the Orion and it's engine nozzle even at relatively large pitch rates minimizing the kickoff force. Advantages and disadvantages of the Simulink model vs. a full geometric ADAMS model are discussed as well.

Konno, Kevin E.↗

Analysis of Three Body Decays in Quasi-Real Photoproduction

This thesis presents preliminary measurements of the moments of angular distribution for the K?K+ mesonic final state using a quasi-real, linearly polarised photon. Two of the main points of focus for this analysis were the development of the formalism for photoproduced vector-pseudoscalar decay and the tools by which the analysis was carried out. The formalism described how the moments of angular distribution could be extracted from the angular decay variables, and how they related to resonance decays in terms of partial waves. In extracting the moments, it was found that adapted Markov Chain Monte Carlo (MCMC) methods proved to be more effective in terms of extracting results from the data compared to the sole use of gradient descent based fitting algorithms. These measurements are complementary to other decay channels and production mechanisms, with the global aim of probing the existence of exotic mesons. Data from this analysis was taken by the CLAS collaboration at the Thomas Jefferson National Accelerator Facility (JLab) by scattering from a liquid hydrogen target using a 10.6 GeV electron. This work was done within the MesonEx program at CLAS12 that aims to map the spectrum of mesons, and in doing so, gain a greater understanding of Quantum ChromoDynamics (QCD) and the strong force.

Wishart, Robert↗

TOPEX/Poseidon orbit maintenance for the first five years

The TOPEX/Poseidon orbit maintenance strategy was changed following launch to include the effects of observed unmodeled, and hence anomalous, along-track accelerations. The anomalous force causes the semi-major axis, a, to either increase (called "boost") or decrease ("deboost" or "decay") depending on the satellite attitude and solar array pitch angle offset. Although this force is the most uncertain parameter in ground track prediction, it has been used as a passive technique for orbit maintenance, thereby reducing the number of propulsive maneuvers, enhancing maneuver spacing, and to place maneuvers at convenient times. This passive technique was first demonstrated in May 1993. The TOPEX/Poseidon orbit has been uniquely maintained using both passive (non-propulsive) and active (propulsive) maneuvers. Furthermore, the orbit has been maintained using only the passive technique since the ninth orbit maintenance maneuver on January 15, 1996. Only nine orbit maintenance maneuvers have been required to maintain the ground track, including verification site over flights, since achieving the operational orbit on September 21, 1992 (mission requirement: 95% within +/- l km). During this period, a has varied within 7,714,429 +/- 7 m, while the inclination i periodically fluctuated in the range 66.0408 deg. +/- 0.0040 deg. The frozen orbit (required e < 0.001 and omega approximately equals to 90 deg.) has been maintained without any dedicated eccentricity maneuvers. The frozen eccentricity vector has completed two periodic cycles and it is currently tracing its third cycle (period approximately equals 26.7 months).

Bhat, R. S.↗

Evaluation of Separation Mechanism Design for the Orion/Ares Launch Vehicle

As a part of the preliminary design work being performed for the Orion vehicle, the Orion to Spacecraft Adaptor (SA) separation mechanism was analyzed and sized, with findings presented here. Sizing is based on worst case abort condition as a result of an anomaly driving the launch vehicle engine thrust vector control hard-over causing a severe vehicle pitch over. This worst case scenario occurs just before Upper Stage Main Engine Cut-Off (MECO) when the vehicle is the lightest and the damping effect due to propellant slosh has been reduced to a minimum. To address this scenario and others, two modeling approaches were invoked. The first approach was a detailed 2-D (Simulink) model to quickly assess the Service Module Engine nozzle to SA clearance for a given separation mechanism. The second approach involved the generation of an Automatic Dynamic Analysis of Mechanical Systems (ADAMS) model to assess secondary effects due to mass centers of gravity that were slightly off the vehicle centerline. It also captured any interference between the Solar Arrays and the Spacecraft Adapter. A comparison of modeling results and accuracy are discussed. Most notably, incorporating a larger SA flange diameter allowed for a natural separation of the Orion and its engine nozzle even at relatively large pitch rates minimizing the kickoff force. Advantages and disadvantages of the 2-D model vs. a full 3-D (ADAMS) model are discussed as well.

Konno, Kevin E.↗

Evaluation of Separation Mechanism Design for the Orion/Ares Launch Vehicle

As a part of the preliminary design work being performed for the Orion vehicle, the Orion to Spacecraft Adaptor (SA) separation mechanism was analyzed and sized, with findings presented here. Sizing is based on worst case abort condition as a result of an anomaly driving the launch vehicle engine thrust vector control hard-over causing a severe vehicle pitch over. This worst case scenario occurs just before Upper Stage Main Engine Cut-Off (MECO) when the vehicle is the lightest and the damping effect due to propellant slosh has been reduced to a minimum. To address this scenario and others, two modeling approaches were invoked. The first approach was a detailed 2-D (Simulink) model to quickly assess the Service Module Engine nozzle to SA clearance for a given separation mechanism. The second approach involved the generation of an Automatic Dynamic Analysis of Mechanical Systems (ADAMS) model to assess secondary effects due to mass centers of gravity that were slightly off the vehicle centerline. It also captured any interference between the Solar Arrays and the Spacecraft Adapter. A comparison of modeling results and accuracy are discussed. Most notably, incorporating a larger SA flange diameter allowed for a natural separation of the Orion and its engine nozzle even at relatively large pitch rates minimizing the kickoff force. Advantages and disadvantages of the 2-D model vs. a full 3-D (ADAMS) model are discussed as well.

Konno, Kevin E.↗

Scatterometer Observes Extratropical Transition of Pacific Typhoons

From September 15 to 25, 1996, NASA's scatterometer (NSCAT) monitored the evolution of twin typhoons, Violet and Tom, as they moved north from the western tropical Pacific, acquiring features of mid-latitude storms. The typhoons developed frontal structures, increased asymmetry, and dry air was introduced into their cores. Violet hit Japan, causing death and destruction (Figure 1), and Tom merged with a mid-latitude trough and evolved into a large extratropical storm with gale-force winds (Figure 2). We understand relatively little about the extratropical transition of tropical cyclones because of the complex thermodynamics involved [e.g., Sinclair, 1993], but we do know that the mid-latitude storms resulting from tropical cyclones usually generate strong winds and heavy precipitation. Since the transition usually occurs over the ocean, few measurements have been made. The transition is a fascinating science problem, but it also has important economic consequences. The transition occurs over the busiest trans-ocean shipping lanes, and when the resulting storms hit land, they usually devastate populated areas. NSCAT was successfully launched into a near-polar, sun-synchronous orbit on the Japanese Advanced Earth Observing Satellite (ADEOS) in August 1996 from Tanegashima Space Center in Japan. NSCAT's six antennas send microwave pulses at a frequency of 14 GHz to the Earth's surface and measure the backscatter. The antennas scan two 600-km bands of the ocean, which are separated by a 330-km data gap. From NSCAT observations, surface wind vectors can be derived at 25-km spatial resolution, covering 77% of the ice-free ocean in one day and 97% of the ocean in two days, under both clear and cloudy conditions.

Liu, W. Timothy↗

High-Performance Reaction Wheel Optimization for Fine-Pointing Space Platforms: Minimizing Induced Vibration Effects on Jitter Performance plus Lessons Learned from Hubble Space Telescope for Current and Future Spacecraft Applications

The Hubble Space Telescope (HST) applies large-diameter optics (2.5-m primary mirror) for diffraction-limited resolution spanning an extended wavelength range (approx. 100-2500 nm). Its Pointing Control System (PCS) Reaction Wheel Assemblies (RWAs), in the Support Systems Module (SSM), acquired an unprecedented set of high-sensitivity Induced Vibration (IV) data for 5 flight-certified RWAs: dwelling at set rotation rates. Focused on 4 key ratios, force and moment harmonic values (in 3 local principal directions) are extracted in the RWA operating range (0-3000 RPM). The IV test data, obtained under ambient lab conditions, are investigated in detail, evaluated, compiled, and curve-fitted; variational trends, core causes, and unforeseen anomalies are addressed. In aggregate, these values constitute a statistically-valid basis to quantify ground test-to-test variations and facilitate extrapolations to on-orbit conditions. Accumulated knowledge of bearing-rotor vibrational sources, corresponding harmonic contributions, and salient elements of IV key variability factors are discussed. An evolved methodology is presented for absolute assessments and relative comparisons of macro-level IV signal magnitude due to micro-level construction-assembly geometric details/imperfections stemming from both electrical drive and primary bearing design parameters. Based upon studies of same-size/similar-design momentum wheels' IV changes, upper estimates due to transitions from ground tests to orbital conditions are derived. Recommended HST RWA choices are discussed relative to system optimization/tradeoffs of Line-Of-Sight (LOS) vector-pointing focal-plane error driven by higher IV transmissibilities through low-damped structural dynamics that stimulate optical elements. Unique analytical disturbance results for orbital HST accelerations are described applicable to microgravity efforts. Conclusions, lessons learned, historical context/insights, and perspectives on future applications are given; these previously unpublished data and findings represents a valuable resource for fine-pointing spacecraft or space-based platforms using RWAs, Control Moment Gyros (CMGs), Momentum Wheels, or other ball-bearing-based rotational units.

Hasha, Martin D.↗

Study of the doubly charmed tetraquark $\mathrm{T}$ $^+_{cc}$

Quantum chromodynamics, the theory of the strong force, describes interactions of coloured quarks and gluons and the formation of hadronic matter. Conventional hadronic matter consists of baryons and mesons made of three quarks and quark-antiquark pairs, respectively. Particles with an alternative quark content are known as exotic states. Here a study is reported of an exotic narrow state in the D 0 D 0 π + mass spectrum just below the D *+ D 0 mass threshold produced in proton-proton collisions collected with the LHCb detector at the Large Hadron Collider. The state is consistent with the ground isoscalar T$^{+}_{cc}$ tetraquark with a quark content of cc$\bar{u}\bar{d}$ and spin-parity quantum numbers J P = 1 + . Study of the DD mass spectra disfavours interpretation of the resonance as the isovector state. The decay structure via intermediate off-shell D *+ mesons is consistent with the observed D 0 π+ mass distribution. To analyse the mass of the resonance and its coupling to the D*D system, a dedicated model is developed under the assumption of an isoscalar axial-vector T$^{+}_{cc}$ state decaying to the D*D channel. Using this model, resonance parameters including the pole position, scattering length, effective range and compositeness are determined to reveal important information about the nature of the T$^{+}_{cc}$ state. In addition, an unexpected dependence of the production rate on track multiplicity is observed.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Structural, Magnetic and Microwave Absorption Properties of Ba{sub 0.5}Sr{sub 0.5}Ni{sub 2−x} (MgZn) {sub x/2}Fe{sub 16}O{sub 27} Hexaferrite Nanoparticles Prepared by the Sol-Gel Combustion Method

In this study, Sr–Ba hexaferrite nanoparticles (Ba{sub 0.5}Sr{sub 0.5}Ni{sub 2−x}(MgZn){sub (x/2)}Fe{sub 16}O{sub 27}, x = –0.6, in the step of 0.2) was synthesized by the sol-gel method. The influence of Mg–Zn substitution on the structure and microwave absorption properties of Ni–W-type hexaferrite were investigated by technical methods such as x-ray diffraction, vector network analyzer, transmission electron micrograph and vibrating sample magnetometer. TEM images illustrated almost spherical particles with an average size of 35–52 nm. The M–H loops for all samples were measured at room temperature by vibrating sample magnetometer. Saturation magnetization (M{sub s}) and coercivity (H{sub c}) were derived from the hysteresis loops. The maximum field used in this measurement was 9 kilo-Oersted (kOe) Finally, the microwave absorption properties of these samples were investigated in Ku band range. The thickness of the composites was 2 mm in microwave absorption measurements. The results showed that the synthesized samples have a great potential in many fields of industry.

77 NANOSCIENCE AND NANOTECHNOLOGY↗