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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 739 records · Page 41
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Atomic resolution scanning transmission electron microscopy at liquid helium temperatures for quantum materials

Fundamental quantum phenomena in condensed matter, ranging from correlated electron systems to quantum information processors, manifest their emergent characteristics and behaviors predominantly at low temperatures. This necessitates the use of liquid helium (LHe) cooling for experimental observation. Atomic resolution scanning transmission electron microscopy combined with LHe cooling (cryo-STEM) provides a powerful characterization technique to probe local atomic structural modulations and their coupling with charge, spin and orbital degrees-of-freedom in quantum materials. However, achieving atomic resolution in cryo-STEM is exceptionally challenging, primarily due to sample drifts arising from temperature changes and noises associated with LHe bubbling, turbulent gas flow, etc. In this work, we demonstrate atomic resolution cryo-STEM imaging at LHe temperatures using a commercial side-entry LHe cooling holder. Firstly, we examine STEM imaging performance as a function of He gas flow rate, identifying two primary noise sources: He-gas pulsing and He-gas bubbling. Secondly, we propose two strategies to achieve low noise conditions for atomic resolution STEM imaging: either by temporarily suppressing He gas flow rate using the needle valve or by acquiring images during the natural warming process. Lastly, we show the applications of image acquisition methods and image processing techniques in investigating structural phase transitions in Cr 2 Ge 2 Te 6 , CuIr 2 S 4 , and CrCl 3 . In conclusion, our findings represent an advance in the field of atomic resolution electron microscopy imaging for quantum materials and devices at LHe temperatures, which can be applied to other commercial side-entry LHe cooling TEM holders.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Probing sub-5 Ångstrom micropores in carbon for precise light olefin/paraffin separation

Olefin/paraffin separation is an important but challenging and energy-intensive process in petrochemical industry. The realization of carbons with size-exclusion capability is highly desirable but rarely reported. Herein, we report polydopamine-derived carbons (PDA-Cx, where x refers to the pyrolysis temperature) with tailorable sub-5 Å micropore orifices together with larger microvoids by one-step pyrolysis. The sub-5 Å micropore orifices centered at 4.1–4.3 Å in PDA-C800 and 3.7–4.0 Å in PDA-C900 allow the entry of olefins while entirely excluding their paraffin counterparts, performing a precise cut-off to discriminate olefin/paraffin with sub-angstrom discrepancy. The larger voids enable high C 2 H 4 and C 3 H 6 capacities of 2.25 and 1.98 mmol g –1 under ambient conditions, respectively. Breakthrough experiments confirm that a one-step adsorption-desorption process can obtain high-purity olefins. Inelastic neutron scattering further reveals the host–guest interaction of adsorbed C 2 H 4 and C 3 H 6 molecules in PDA-Cx. This study opens an avenue to exploit the sub-5 Å micropores in carbon and their desirable size-exclusion effect.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRSDate not supplied

Direct Reconstruction of Ablative Thermal Protection System Aeroheating Using A Green's Function Approach

A Green’s function inverse heat transfer (IHT) approach is used to reconstruct the surface heating conditions on ablative thermal protection system (TPS) materials from embedded heat flux sensor and temperature probe measurements. The approach models the temperature time-history at the measurement location as a discrete linear system, allowing for the heat flux boundary condition to be recovered directly without the need for time-marching schemes. The effects of material decomposition and pyrolysis gas transport are modeled using an energy source/sink analogue. The performance of the reconstruction approach is analyzed on a 1D test case representative of an atmospheric entry heating scenario. The approach can recover the TPS surface heat flux to within 4% of the input heating condition with a computation time of 2-3 seconds (>3 orders of magnitude faster than current time-marching IHT methods). As a byproduct of the surface heating reconstruction, the algorithm also captures the surface pyrolysis gas mass flux and solid decomposition at multiple through-thickness locations within the TPS.

Kenneth McAfee↗
NASA NTRS1978

Measurement of the turbulence intensity behind a two-dimensional cascade and in a three-stage axial blower

Turbulence intensity (Tu) measurements were made in two-dimensional and rotating cascades of blades in a low-speed cascade wind tunnel using hot-wire probes as sensors. The local Tu at Re = 1.6x100000 was determined in the wake zone behind a two-dimensional cascade. Then the values were recomputed for a rotating cascade, giving a mean turbulence intensity of 6.5% at 1/10 chord downstream and 2.9% at one chord. Fans were used for measurements on the rotating cascade. Re was equal to 7x100000. Frequency analysis was employed to separate the actual Tu of the entry flow from the effects caused by interaction with the rotor blades, showing that the true Tu increased from a few tenths of a percent to 6.6% in the 1st rotor, and from 7.2 to 9.3% in the 2d rotor. The Tu behind the 3d rotor was equal to 8.9%.

Kiock, R.↗
NASA NTRS1951

Wind-tunnel investigation of six shielded total-pressure tubes at high angles of attack subsonic speeds

The effect of inclination of the air stream on the measured pressures of six shielded total-pressure tubes (all designed for end-mounting on a horizontal boom) has been determined for an angle-of-attack range of approximately -30° to 65°. The tests were conducted at a Mach number of 0.26 in the Langley stability tunnel and at Mach numbers of 0.50, 0.70, 0.90, and 0.95 in the Langley high-speed 7- by 10-foot tunnel. The results of the tests showed that curved venturi entries are less sensitive to inclination of the air stream than the conical entry of the standard Kiel design. Of the three curved entries tested, the tube having the bluntest entry proved the least sensitive to inclination. The critical angle (that is, the sngle.at which the total-pressure error equals 1 percent of the impact pressure) for this tube was ±63.2° at a Mach number of 0.26. The tests also showed that the critical angle of a shielded tube could be extended to higher positive angles of attack by means of a slant profile. The critical angle of a tube having a conical entry with a 10° slant profile, for example, was found to average 9° greater than that of a similar tube having a square profile. Although the critical angle of this tube at angles of yaw was less than that at angles of attack, the critical angle in yaw was equal to that of the tube with the square profile. Tests of the effect of varying the position of the total-pressure probe in the shield showed that, in general, no advantage was to be gained by changing from the position used in the standard Kiel design. Limited tests of the effect of varying the internal diameter of the shield showed that an increase in the diameter of the throat corresponding an increase in the internal area of 50 percent resulted in a relatively small increase (2.5°) in the critical angle. The effect of Mach number on the sensitivity of the tubes to inclination was shown to be appreciable. An increase in Mach number from 0.26 to 0.90, for example, resulted in a decrease in the critical angle of most of the tubes of about 4°.

Walter R Russell↗
NASA NTRS1973

A shock-tube study of radiation behind shock waves in CO2 with application to Venus entry

The arc-driven Langley 6-inch shock tube has been used to produce shock waves in CO2 in the speed range between 9 and 13 km/sec at ambient pressures between 0.1 and 5 torr. These pressures correspond approximately to equivalent Venus altitudes between 100 and 80 km. Radiation intensity profiles behind the shock waves have been observed for several wavelengths at which the important species emit. Observation and analysis of the luminosity profiles in the zone of chemical nonequilibrium have been given particular emphasis. The results of the measurements are employed in the prediction of nonequilibrium radiative heating to a typical blunt-body probe entering the Venus atmosphere on a ballistic trajectory.

Nealy, J. E.↗
NASA NTRSDate not supplied

Introduction to Trajectories

Presentation prepared for the 10th International Planetary Probe Workshop in 2013. The presentation was approved in the old approval system back in 2013. I am being asked to re-submit it for approval because the record of approval is no longer available. The presentation is being re-used for student seminars.

Trajectories↗
NASA NTRS1993

Observations of the nightside Venus ionosphere: Final encounter of the Pioneer Venus Orbiter Ion Mass Spectrometer

During the last orbital sequences of the Pioneer-Venus spacecraft prior to final encounter and atmospheric entry, data were obtained by the Orbiter Ion Mass Spectrometer (OIMS) at the lowest periapsis altitudes of the mission. These data verified OIMS observations of the nightside ionospheric peak reported earlier in the mission, and revealed additional details related to composition, energetics and maintenance of the nightside ionosphere. OIMS observations of the ion peak during the final encounter sequence are compared with radio occultation data and OIMS peak observations obtained earlier. OIMS ion density and Orbiter Electron Temperature Probe (OETP) electron density are found to correlate near the peak. Coupling of mass channels 30 and 32 during nightside passes is observed and its interpretation considered. Changes in high altitude composition of the nightside ionosphere, especially the relative changes in O(+) and H(+), are described.

Cloutier, P. A.↗
NASA NTRS2018

Titan's Cold Case Files - Outstanding Questions After Cassini-Huygens

The entry of the Cassini-Huygens spacecraft into orbit around Saturn in July 2004 marked the start of a golden era in the exploration of Titan, Saturn's giant moon. During the prime mission (2004-2008), ground-breaking discoveries were made by the Cassini orbiter including the equatorial dune fields (flyby T3, 2005), northern lakes and seas (T16, 2006), and the large positive and negative ions (T16 & T18, 2006), to name a few. In 2005 the Huygens probe descended through Titan's atmosphere, taking the first close-up pictures of the surface, including large networks of dendritic channels leading to a dried-up seabed, and also obtaining detailed profiles of temperature and gas composition during the atmospheric descent. The discoveries continued through the Equinox mission (2008-2010) and Solstice mission (2010-2017) totaling 127 targeted flybys of Titan in all. Now at the end of the mission, we are able to look back on the high-level scientific questions from the start of the mission, and assess the progress that has been made towards answering these. At the same time, new scientific questions regarding Titan have emerged from the new discoveries that have been made. In this paper we review a cross-section of important scientific questions that remain partially or completely unanswered, ranging from Titan's deep interior to the exosphere. Our intention is to help formulate the science goals for the next generation of planetary missions to Saturn and Titan, and to stimulate new experimental, observation and theoretical investigations in the interim, before such missions arrive again at Titan.

Nixon, C. A.↗
NASA NTRS1991

Development of a relatchable cover mechanism for a cryogenic IR-sensor

A cover mechanism for use on the Infrared Background Signature Survey (IBSS) cryostat was developed. The IBSS IR-instrument is scheduled for STS launch in early 1991 as a payload of the Shuttle Payload Satellite (SPS) 2. The cover is hinged, with a motorized rope drive. During ground processing, launch, entry, and landing, the cryostat, which houses the IR-instrument, is required to be a sealed vacuum tight container for cooling purposes and contamination prevention. When on orbit, the cover is opened to provide an unobstructed field of view for the IR-instrument. A positive seal is accomplished through the use of latch mechanism. The cover and the latch are driven by a common redundant actuator consisting of dc motors, spur gears, and a differential gear. Hall probe limit switches and position sensors (rotary variable transformer) are used to determine the position of the cover and the latch. The cover mechanism was successfully qualified for thermal vacuum (-25 to 35 C), acoustic noise, vibration (6 Gs sine, 9.7 G RMS) and life cycles. Constricting requirements, mechanical and electronic control design, specific design details, test results of functional performance, and environmental and life tests are described.

Birner, R.↗
NASA NTRS1993

Observations of the Nightside Venus Ionosphere: Final Encounter of the Pioneer Venus Orbiter Ion Mass Spectrometer

During the last orbital sequences of the Pioneer Venus spacecraft prior to final encounter and atmospheric entry, data were obtained by the Orbiter Ion Mass Spectrometer (OIMS) at the lowest periapsis altitudes of the mission. These data verified OIMS observations of the nightside ionospheric peak reported-earlier in the mission, and revealed additional details related to composition, energetics and maintenance of the nightside ionosphere. OIMS observations of the ion peak during the final encounter sequence are compared with radio occultation data and OIMS peak observations obtained earlier. OIMS ion density and Orbiter Electron Temperature Probe (OETP) electron density are found to correlate near the peak. Coupling of mass channels 30 and 32 during nightside passes is observed and its interpretation considered. Changes in high altitude composition of the nightside ionosphere, especially the relative changes in O(+) and H(+), are described.

Cloutier, P. A.↗
NASA NTRS2016

Mars Cube One (MarCO) Shifting the Paradigm in Relay Deep Space Operations

A very significant challenge in the planetary mission design and operations is communications with ground control teams during critical events and highly risky maneuvers. These include entry, descent, and landing (EDL) and orbit insertion, which should not be carried out in the blind. Although vast planetary distances and long round-trip light times disallow real-time intervention from controllers, acquiring the relevant event performance parameters in near real-time can be imperative for determining the corrective actions needed immediately following or, in the case of significant anomalies, aid in the diagnostic analysis. During several previous Mars missions landing events, and the Huygens probe landing on Titan, the communications strategy relied on proximity links to planetary orbiters, which then relayed the data to the Deep Space Network (DSN). In addition, attempts were successfully made in parallel to receive the signal carrier directly at Earth often using large radio telescopes when the wavelength was outside the DSN’s reception bands. This Direct-to-Earth (DTE) back-up method was only possible due to special techniques utilizing the DSN’s open-loop Radio Science Receivers. In every case, it was very challenging since the link budget of a landing vehicles were designed for proximity orbiter relays and not for distances across the solar system. A new method is introduced since not all future missions can rely on the presence of pre-existing orbiters at their planetary targets to relay their critical data ad, furthermore, most missions would not likely have the resources to implement a reliable DTE link at acceptable data rates, bypassing a need for a relay asset. With the advent CubeSat form-factor spacecraft, one or more, for added reliability, CubeSats can be launched with the primary mission, travel to the target, and be positioned to view the critical event, such as EDL, and carry out real-time relay of the data to the DSN at higher rates. CubeSats have flown in the Earth environment but never flown or been operated in deep space or planetary environment so careful design as well as flight experience are needed. The relay function requires the development of radio and antenna systems to meet challenging specifications. After initial technical demonstration of the concept and operational experience, the cost can decrease as systems become more standardized with increased reliability. This paper describes the invention of the “carry your own relay” concept and the formulation of the mission likely to be the first planetary CubeSat mission called Mars Cube One (MarCO). It also describes the operational concept of relay small spacecraft and their role reducing mission risk as well as overall mission cost.

Asmar, Sami↗
NASA NTRS2019

White Papers for the Next Decadal Survey: Thermal Protection Systems and Instrumentation

NASA is anticipated to commission the next Planetary Science Decadal Survey (PSDS) with preparation expected in early calendar year 2020. The new PSDS will outline the priorities of science missions for the decade spanning 2023-2032. For the previous PSDS, the science and technology communities have been invited to submit white papers to the PSDS sub-panels as background information to guide the PSDS recommendations. The National Research Council has previously stated that white papers that represent the opinion of many authors from different institutions carried more significant and weight, and the recommendations from the previous PSDS attempted to reflect more of a consensus opinion.In 2009, a total of 4 white papers were submitted to the PSDS panels regarding thermal protection system (TPS) readiness for missions, as well as one on TPS instrumentation. The TPS readiness papers were co-authored by 90 individuals from many institutions. These white papers surveyed the TPS materials for both forebody and afterbody of a probe and analyzed the suitability of materials for missions to each destination. In addition, each paper outlined the ground testing required and ongoing technology development. Recommendations were provided for further technology development and ground test capability in order to fulfill future missions. Planning for the next PSDS: Many improvements and changes have occurred in the past 10 years with regard to TPS materials and instrumentation. New materials have been developed and tested, such as the high density material Heatshield for Extreme Entry Environment Technology (HEEET), and new capabilities for ground testing for high heating and high pressures have been added such as the 3” nozzle at the Ames arc jet. NASA has also flown several TPS instrumentation suites, such as MEDLI and EFT-1.In order to provide the PSDS sub-panels with the most current information about the state-of-the-art suit-ability for TPS materials for entry missions, we are be-ginning to update and draft new white papers. We will present the outline for material to be covered in the white papers, and we invite all IPPW attendees to parti-ciate in co-authoring these papers.

Hwang, H. H.↗
NASA NTRS1972

Prediction of electron concentration reductions in re-entry flow fields due to electrophilic liquid and water injection.

Discussion of an analytical model which leads to predictions of reductions in electron concentrations in reentry flow fields due to the injection of electrophilic liquids and water. The processes incorporated into the model are: penetration and breakup of the liquid jet, droplet acceleration and vaporization, expansion of the liquid spray due to droplet vaporization, electrophilic vapor diffusion, heterogeneous and homogeneous charged species recombination kinetics and homogeneous electron attachment kinetics. Spray boundary calculations are shown to be in good agreement with photographic observations of water and Freon E-3 sprays in wind tunnel tests of a scale model RAM C-III flight vehicle. Fixed-bias electrostatic probe data taken during the RAM C-III flight are interpreted in terms of effective jet penetration distances - which are shown to be consistent with calculations using the present model.

Pergament, H. S.↗
NASA NTRSDate not supplied

Backshell Radiative Heating and Shock Layer Kinetic Measurement in NASA’s Electric Arc Shock Tube Facility

A methodology for creating incident shocks with similarity to the backshell radiative heating environment on planetary probes is presented. Two test series were carried out in the Electric Arc Shock Tube (EAST) at NASA Ames to quantify the backshell environment for planned and executed missions entering the atmospheres of Mars and Titan. The comparison of measured radiance in the shock tube to predicted post shock radiation levels is used to quantify the uncertainty in the model. This model uncertainty may then be related back to the flight condition to assess the error in the flight heating prediction. Tests for Mars entry show the shock tube measurements to be bracketed between two kinetic models by 2-7%. This suggests an 8% error in predicting the measured heating cannot be attributed to radiation. Comparisons to planned Titan entry suggest a substantial overprediction of the backshell radiation, which suggests opportunity for future refinement of radiative heating models.

radiation↗
NASA NTRS2011

Ares I-X First Stage Internal Aft Skirt Re-Entry Heating Data and Modeling

The CLVSTATE engineering code is being used to predict Ares-I launch vehicle first stage reentry aerodynamic heating. An engineering analysis is developed which yields reasonable predictions for the timing of the first stage aft skirt thermal curtain failure and the resulting internal gas temperatures. The analysis is based on correlations of the Ares I-X internal aft skirt gas temperatures and has been implemented into CLVSTATE. Validation of the thermal curtain opening models has been accomplished using additional Ares I-X thermocouple, calorimeter and pressure flight data. In addition, a technique which accounts for radiation losses at high altitudes has been developed which improves the gas temperature measurements obtained by the gas temperature probes (GTP). Updates to the CLVSTATE models are shown to improve the accuracy of the internal aft skirt heating predictions which will result in increased confidence in future vehicle designs

Schmitz, Craig P.↗
NASA NTRS2007

KLASS: Kennedy Launch Academy Simulation System

Software provides access to many sophisticated scientific instrumentation (Scanning Electron Microscope (SEM), a Light Microscope, a Scanning Probe Microscope (covering Scanning Tunneling, Atomic Force, and Magnetic Force microscopy), and an Energy Dispersive Spectrometer for the SEM). Flash animation videos explain how each of the instruments work. Videos on how they are used at NASA and the sample preparation. Measuring and labeling tools provided with each instrument. Hands on experience of controlling the virtual instrument to conduct investigations, much like the real scientists at NASA do. Very open architecture. Open source on SourceForge. Extensive use of XML Target audience is high school and entry-level college students. "Many beginning students never get closer to an electron microscope than the photos in their textbooks. But anyone can get a sense of what the instrument can do by downloading this simulator from NASA's Kennedy Space Center." Science Magazine, April 8th, 2005

Garner, Lesley C.↗
NASA NTRS2013

Parametric Thermal Soak Model for Earth Entry Vehicles

The analysis and design of an Earth Entry Vehicle (EEV) is multidisciplinary in nature, requiring the application many disciplines. An integrated tool called Multi Mission System Analysis for Planetary Entry Descent and Landing or M-SAPE is being developed as part of Entry Vehicle Technology project under In-Space Technology program. Integration of a multidisciplinary problem is a challenging task. Automation of the execution process and data transfer among disciplines can be accomplished to provide significant benefits. Thermal soak analysis and temperature predictions of various interior components of entry vehicle, including the impact foam and payload container are part of the solution that M-SAPE will offer to spacecraft designers. The present paper focuses on the thermal soak analysis of an entry vehicle design based on the Mars Sample Return entry vehicle geometry and discusses a technical approach to develop parametric models for thermal soak analysis that will be integrated into M-SAPE. One of the main objectives is to be able to identify the important parameters and to develop correlation coefficients so that, for a given trajectory, can estimate the peak payload temperature based on relevant trajectory parameters and vehicle geometry. The models are being developed for two primary thermal protection (TPS) materials: 1) carbon phenolic that was used for Galileo and Pioneer Venus probes and, 2) Phenolic Impregnated Carbon Ablator (PICA), TPS material for Mars Science Lab mission. Several representative trajectories were selected from a very large trade space to include in the thermal analysis in order to develop an effective parametric thermal soak model. The selected trajectories covered a wide range of heatload and heatflux combinations. Non-linear, fully transient, thermal finite element simulations were performed for the selected trajectories to generate the temperature histories at the interior of the vehicle. Figure 1 shows the finite element model that was used for the simulations. The results indicate that it takes several hours for the thermal energy to soak into the interior of the vehicle and achieve maximum payload temperatures. In addition, a strong correlation between the heatload and peak payload container temperature is observed that will help establishing the parametric thermal soak model.

Agrawal, Parul↗