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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 739 records · Page 41
All sourcesNASA NTRSDOE OSTI
NASA NTRS2001

A Study of the Electrostatic Interaction Between Insulators and Martian/Lunar Soil Simulants

Using our previous experience with the Mars Environmental Compatibility Assessment (MECA) electrometer, we have designed a new type of aerodynamic electrometer. The goal of the research was to measure the buildup of electrostatic surface charge on a stationary cylindrical insulator after windborne granular particles have collided with the insulator surface in a simulated dust storm. The experiments are performed inside a vacuum chamber. This allows the atmospheric composition and pressure to be controlled in order to simulate the atmospheric conditions near the equator on the Martian surface. An impeller fan was used to propel the dust particles at a cylindrically shaped insulator under low vacuum conditions. We tested the new electrometer in a 10 mbar CO2 atmosphere by exposing two types of cylindrical insulators, Teflon (1.9 cm diameter) and Fiberglass (2.5 cm diameter), to a variety of windborne granular particulate materials. The granular materials tested were JSC Mars-1 simulant, which is a mixture of coarse and fine (<5microns diameter) particle sizes, and some of the major mineral constituents of the Martian soil. The minerals included Ottawa sand (SiO2), iron oxide (Fe2O3), aluminum oxide (Al2O3) and magnesium oxide (MgO). We also constructed a MECA-like electrometer that contained an insulator capped planar electrode for measuring the amount of electrostatic charge produced by rubbing an insulator surface over Martian and lunar soil simulants. The results of this study indicate that it is possible to detect triboelectric charging of insulator surfaces by windborne Martian soil simulant, and by individual mineral constituents of the soil simulant. We have also found that Teflon and Fiberglass insulator surfaces respond in different ways by developing opposite polarity surface charge, which decays at different rates after the particle impacts cease.

Mantovani, James G.↗
NASA NTRS2017

Space Weathering Experiments on Spacecraft Materials

A project to investigate space environment effects on specific materials with interest to remote sensing was initiated in 2016. The goal of the project is to better characterize changes in the optical properties of polymers found in multi-layered spacecraft insulation (MLI) induced by electron bombardment. Previous analysis shows that chemical bonds break and potentially reform when exposed to high energy electrons like those seen in orbit. These chemical changes have been shown to alter a material's optical reflectance, among other material properties. This paper presents the initial experimental results of MLI materials exposed to various fluences of high energy electrons, designed to simulate a portion of the geosynchronous Earth orbit (GEO) space environment. It is shown that the spectral reflectance of some of the tested materials changes as a function of electron dose. These results provide an experimental benchmark for analysis of aging effects on satellite systems which can be used to improve remote sensing and space situational awareness. They also provide preliminary analysis on those materials that are most likely to comprise the high area-to-mass ratio (HAMR) population of space debris in the geosynchronous orbit environment. Finally, the results presented in this paper serve as a proof of concept for simulated environmental aging of spacecraft polymers that should lead to more experiments using a larger subset of spacecraft materials.

Engelhart, D. P.↗
DOE OSTI2022

Development of the TREAT M2 experiment as a transient benchmark

A transient benchmark based on the Transient Reactor Test Facility (TREAT) M2 Calibration experiment (M2-CAL) is under development. TREAT, at Idaho National Laboratory, is a graphite moderated air-cooled research reactor which has been used extensively for fuel material testing under extreme and accident conditions. Accurate benchmark models are a beneficial component in the operations, experimental planning, and development of TREAT. In this work, we present a transient benchmark model for the M2-CAL experiment core loading. The benchmark model incorporates the coupling between the Monte Carlo Code SERPENT and the computational fluid dynamics code OpenFOAM to capture the temperature feedback mechanism. The M2-CAL transient 2580 was simulated in this work. A pre-transient analysis was performed to determine the optimum core composition and conditions before the beginning of the transient. The analysis was validated against historic TREAT kinetic measurements and the worth of the transient rod T-2. The axial power distribution in the flux wire for the M2-CAL experiment was determined and contrasted with the experiment. The model was then used to simulate the M2-CAL transient 2580 experiment based on the reported pre-transient and transient conditions. Several transient observables were calculated and compared to the experiment. The model shows good agreement with the experimental power traces, period, and average increase of power at the power ramp (time > 7.8 s). Inverse point kinetics analysis was performed during the period of the power ramp for the model and the experiment based on that, the temperature feedback component was isolated and contrasted with the experimental feedback. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
NASA NTRS1988

The emittance of space radiator materials measured at elevated temperatures

The spectral emittances of textured space radiator materials between 1.7 and 14.7 micrometer have been evaluated at room temperature and elevated temperature (630 C) in air. Heating in air caused a permanent increase in spectral emittance for all materials tested: HCl/ion beam textured 304 stainless steel, untextured Ti (6 percent Al, 4 percent V), and sandblasted Ti (6 percent Al, 4 percent V). Changes in the surface chemistry and/or surface morphology of these materials were also observed. Elevated temperature spectral emittance was measured in an argon atmosphere and compared to the measurements in air. Similarity between the room temperature and elevated temperature spectral emittance measurements was also investigated, and limited agreement was found.

Mirtich, Michael J.↗
DOE OSTI2024

Instrumentation for the In-Core Real-Time Mechanical Testing of Structural Materials (INCREASE) Project

Idaho National Laboratory (INL), in collaboration with the Electric Power Research Institute (EPRI), the Nuclear Regulatory Commission (NRC), the French Atomic and Alternative Energies Commission (CEA), the Joint Research Center (JRC), the Nuclear Research and Consultancy Group (NRG), and the Research Center Rez (CVR), started a Joint Experimental Program (JEEP) project that operates within the Nuclear Energy Agency’s Framework for Irradiation Experiments (FIDES II) program in order to develop capabilities for the in-core real-time mechanical testing of structural materials. This effort will focus on designing a shared capsule capable of housing a variety of in-core mechanical testing instrumentation allowing enhanced experiments for the material science community. The outcome of the project would be high-priority, stress relaxation data for stainless-steel-based materials provided by EPRI and CEA. Stress relaxation is a major phenomenon that contributes to material degradation in nuclear reactor components. Currently, nuclear material stress relaxation is assessed both before and after irradiation, using complex and costly post-irradiation examination (PIE) activities. In-situ data would support the development of precision modeling and simulation of this degradation phenomena and would provide validation and benchmarking for existing models using the PIE data. As part of the U.S. Department of Energy Advanced Sensor and Instrumentation (ASI) program, INL has fabricated and tested out-of-core mechanical test instrumentation. This instrumentation was designed for easy adaptation to the irradiation capsule proposed under this JEEP, and can be deployed to measure real-time stress relaxation under pressurized-water reactor (PWR) conditions. This initial effort will partially serve to replace the testing capabilities lost because of shutting down the Halden Boiling Water Reactor (HBWR). The project would provide these capabilities to the international community via a shared capsule design that is easily adaptable to additional material test reactors. The design features will incorporate expansion to PWR and non-light-water reactor (LWR) environments that will be developed in future work. The capsule and instrumentation will be demonstrated in the Massachusetts Institute of Technology Reactor (MITR) for phase I and the Petten High Flux Reactor (HFR) for phase II irradiations to deliver real-time stress relaxation data on high priority stainless steel structural materials.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Achieving Atomic Dispersion of Highly Loaded Transition Metals in Small-Pore Zeolite SSZ-13: High-Capacity and High-Efficiency Low-Temperature CO and Passive NO x Adsorbers

Synthesis of small-pore zeolitic materials with realistic loadings of transition metals atomically dispersed in the micropores has been a formidable challenge. Herein, we demonstrate a new simple and scalable route to high Pd and Pt loadings (>1 wt%) atomically dispersed in the micropores of a small-pore zeolite, SSZ-13. Unlike all previous methods that require addition of expensive transition metal precursor complexes into the synthesis gel and produce low loading of atomically dispersed species, this method does not require any complicated synthetic proce-dures. We determine the factors that govern the stabilization of M(II) species in the micropores of SSZ-13. Using a combined spectroscopic and DFT approach, we offer a unifying explana-tion for the discrepancies existing in available M-zeolite litera-ture. Moreover, we highlight the difference between the behavior of Pt and Pd during synthesis, and demonstrate that ionically dispersed Pd/SSZ-13 shows superior performance as a new class of environmentally important passive NOx Adsorber (PNA) material under practically relevant conditions. It thus represents the 2nd known metal-small pore zeolite material that has immediate industrial application, and the only known met-al-small pore zeolite material in which metal is close to 100 % utilized. In addition to NO x , the material performs remarkably for CO removal during cold start as well due to the formation of a mixed carbonyl-nitrosyl complex Pd(II)(CO)(NO).

Khivantsev, Konstantin↗
NASA NTRS1999

Alternatives to Silicon Rubber Thermal Barrier in RSRM Nozzle Joints

Thiokol Propulsion encountered a situation where gas path can form in the Filler material in joints between the phenolic in the Space Shuttle Reusable Solid Rocket Motor nozzle. An investigation determined that the method for injecting the filler material into the joint created a pressurized pocket of air that forced its way to the surface while the filler was curing. The path that the air took remained open some situations leaving a path for hot gas to get deep into the joint. The condition that created the gas path has been corrected by modifications to the manufacturing process, but a design solution that would reduce processing time is being pursued. A strip of open cell installed deep into the joint, can serve as a barrier to the Filler material. Testing indicates that the foam eliminates the pressure pocket, and does not prevent detection of leakage of the o-ring seals during leak test. Open cell foam does not have thermal resistance capability and mechanical structure, which would be required in the event of a gas path. A replacement to open cell foam is now being considered. Braided carbon fiber rope has the permeability characteristics of foam and it has thermal resistance characteristics as well. Braided carbon fiber rope (BCFR) has been tested in simulated joints in subscale rocket motor. Results of the testing indicate that braided carbon fiber rope can significantly reduce gas temperature by as much es 3000 F in a nozzle joint configuration. BCFR can be installed as a barrier to stop the joint filler material or it can used as the thermal barrier alone.

Totman, Peter D.↗
NASA NTRS2015

Space Environment Testing of Photovoltaic Array Systems at NASA's Marshall Space Flight Center

CubeSats, Communication Satellites, and Outer Planet Science Satellites all share one thing in common: Mission success depends on maintaining power in the harsh space environment. For a vast majority of satellites, spacecraft power is sourced by a photovoltaic (PV) array system. Built around PV cells, the array systems also include wiring, substrates, connectors, and protection diodes. Each of these components must function properly throughout the mission in order for power production to remain at nominal levels. Failure of even one component can lead to a crippling loss of power. To help ensure PV array systems do not suffer failures on-orbit due to the space environment, NASA's Marshall Space Flight Center (MSFC) has developed a wide ranging test and evaluation capability. Key elements of this capability include: Testing: a. Ultraviolet (UV) Exposure b. Charged Particle Radiation (Electron and Proton) c. Thermal Cycling d. Plasma and Beam Environments Evaluation: a. Electrostatic Discharge (ESD) Screening b. Optical Inspection and easurement c. PV Power Output including Large Area Pulsed Solar Simulator (LAPSS) measurements This paper will describe the elements of the space environment which particularly impact PV array systems. MSFC test capabilities will be described to show how the relevant space environments can be applied to PV array systems in the laboratory. A discussion of MSFC evaluation capabilities will also be provided. The sample evaluation capabilities offer test engineers a means to quantify the effects of the space environment on their PV array system or component. Finally, examples will be shown of the effects of the space environment on actual PV array materials tested at MSFC.

Schneider, Todd A.↗
NASA NTRS1972

Microwave emission from geological materials - Observations of interference effects.

Microwave radiometric field observations were conducted at wavelengths of 21, 2.8, and 0.95 cm to determine the microwave penetration depth of a number of sands and gravels as a function of particle size and moisture content. Observations of a reflecting plate covered with varying thicknesses of test material exhibit a pronounced oscillatory behavior that is consistent with established electromagnetic theory for plane-parallel layered mediums. Utilization of this interference effect is proposed as a microwave radiometric technique for determining the bulk electrical properties of geologic materials, snow, ice, and other materials readily adapted to layering experiments.

Blinn, J. C., III↗
DOE OSTI2022

Changes to the morphology and coefficient of thermal expansion in HDPE and UHMWPE following irradiation-based crosslinking

This work describes recent findings of the Los Alamos National Laboratory concerning the alterations to polyethylene’s (PE’s) mechanical and chemical properties after crosslinking via gamma irradiation. Three materials were examined as part of this study, including one HDPE and two UHMWPE specimens. Changes to degree of crystallinity (X C ) were qualitatively determined via measurements of density, and results suggest that X C is not necessarily correlated to crosslink density, depending on polymer manufacturing process and treatment following irradiation. TMA data suggests an anisotropic response in linear thermal expansion, and that the response may be more correlated to X C than crosslink density. Finally, FTIR analysis has led to the conclusion that oxidation occurs as a result of irradiation in open air, the degree of oxidation is proportional to the maximum radiation dose received, and that oxidation is largely a surface effect, penetrating no deeper than 1.5 mm. Due to time constraints, a full dataset could not be generated for changes in creep and thermal properties as a result of irradiation, and TMA analysis is only complete for one material tested in this study. These measurements are ongoing and will provide more context to the hypotheses drawn in this work.

36 MATERIALS SCIENCE↗
NASA NTRS1976

Laboratory-scale uranium RF plasma confinement experiments

An experimental investigation was conducted using 80 kW and 1.2 MW RF induction heater facilities to aid in developing the technology necessary for designing a self-critical fissioning uranium plasma core reactor. Pure uranium hexafluoride (UF6) was injected into argon-confined, steady-state, RF-heated plasmas in different uranium plasma confinement tests to investigate the characteristics of plamas core nuclear reactors. The objectives were: (1) to confine as high a density of uranium vapor as possible within the plasma while simultaneously minimizing the uranium compound wall deposition; (2) to develop and test materials and handling techniques suitable for use with high-temperature, high-pressure gaseous UF6; and (3) to develop complementary diagnostic instrumentation and measurement techniques to characterize the uranium plasma and residue deposited on the test chamber components. In all tests, the plasma was a fluid-mechanically-confined vortex-type contained within a fused-silica cylindrical test chamber. The test chamber peripheral wall was 5.7 cm ID by 10 cm long.

Roman, W. C.↗
DOE OSTI2024

Assessment of Cementitious Composites for High-Temperature Geothermal Wells

High-temperature (HT) geothermal wells can provide green power 24 hours a day, 7 days a week. Under harsh environmental and operational conditions, the long-term durability requirements of such wells require special cementitious composites for well construction. This paper reports a comprehensive assessment of geothermal cement composites in cyclic pressure function laboratory tests and field exposures in an HT geothermal well (300–350 °C), as well as a numerical model to complement the experimental results. Performances of calcium–aluminate cement (CAC)-based composites and calcium-free cement were compared against the reference ordinary Portland cement (OPC)/silica blend. The stability and degradation of the tested materials were characterized by crystalline composition, thermo-gravimetric and elemental analyses, morphological studies, water-fillable porosity, and mechanical property measurements. All CAC-based formulations outperformed the reference blend both in the function and exposure tests. The reference OPC/silica lost its mechanical properties during the 9-month well exposure through extensive HT carbonation, while the properties of the CAC-based blends improved over that period. The Modified Cam-Clay (MCC) plasticity parameters of several HT cement formulations were extracted from triaxial and Brazilian tests and verified against the experimental results of function cyclic tests. These parameters can be used in well integrity models to predict the field-scale behavior of the cement sheath under geothermal well conditions.

15 GEOTHERMAL ENERGY↗
NASA NTRS1982

Metal shell technology based upon hollow jet instability

Spherical shells of submillimeter size are sought as ICF targets. Such shells must be dimensionally precise, smooth, of high strength, and composed of a high atomic number material. A technology for the production of shells based upon the hydrodynamic instability of an annular jet of molten metal is described. Shells in the 0.7-2.0 mm size range have been produced using tin as a test material. Specimens exhibit good sphericity, fair concentricity, and excellent finish over most of the surface. Work involving a gold-lead-antimony alloy is in progress. Droplets of this are amorphous and possess superior surface finish. The flow of tin models that of the alloy well; experiments on both metals show that the technique holds considerable promise.

Kendall, J. M.↗
NASA NTRS2013

Post-Flight Evaluation of PICA and PICA-X - Comparisons of the Stardust SRC and Space-X Dragon 1 Forebody Heatshield Materials

Phenolic Impregnated Carbon Ablator (PICA) was developed at NASA Ames Research Center. As a thermal protection material, PICA has the advantages of being able to withstand high heat fluxes with a relatively low density. This ablative material was used as the forebody heat shield material for the Stardust sample return capsule, which re-entered the Earths atmosphere in 2006. Based on PICA, SpaceX developed a variant, PICA-X, and used it as the heat shield material for its Dragon spacecraft, which successfully orbited the Earth and re-entered the atmosphere during the COTS Demo Flight 1 in 2010. Post-flight analysis was previously performed on the Stardust PICA heat shield material. Similarly, a near-stagnation core was obtained from the post-flight Dragon 1 heat shield, which was retrieved from the Pacific Ocean. Materials testing and analyses were performed on the core to evaluate its ablation performance and post-flight properties. Comparisons between PICA and PICA-X are made where applicable. Stardust and Dragon offer rare opportunities to evaluate materials post-flight - this data is beneficial in understanding material performance and also improves modeling capabilities.

PICA-X↗
NASA NTRS1992

An automated system for creep testing

A completely automated data collection system was devised to measure, analyze, and graph creep versus time using a PC, a 16 channel multiplexed analog to digital converter, and low friction potentiometers to measure length. The sampling rate for each experiment can be adjusted in the software to meet the needs of the material tested. Data is collected and stored on a diskette for permanent record and also for later data analysis on a different machine.

Spiegel, F. Xavier↗
NASA NTRS1980

Argon/UF6 plasma experiments: UF6 regeneration and product analysis

An experimental and analytical investigation was conducted to aid in developing some of the technology necessary for designing a self-critical fissioning uranium plasma core reactors (PCR). This technology is applicable to gaseous uranium hexafluoride nuclear-pumped laser systems. The principal equipment used included 1.2 MW RF induction heater, a d.c. plasma torch, a uranium tetrafluoride feeder system, and batch-type fluorine/UF6 regeneration systems. Overall objectives were to continue to develop and test materials and handling techniques suitable for use with high-temperature, high-pressure, gaseous UF6; and to continue development of complementary diagnostic instrumentation and measurement techniques to characterize the effluent exhaust gases and residue deposited on the test chamber and exhaust system components. Specific objectives include: a development of a batch-type UF6 regeneration system employing pure high-temperature fluorine; development of a ruggedized time-of-flight mass spectrometer and associated data acquisition system capable of making on-line concentration measurements of the volatile effluent exhaust gas species in a high RF environment and corrosive environment of UF6 and related halide compounds.

Roman, W. C.↗
NASA NTRS2010

Ares V: Progress Toward Unprecedented Heavy Lift

Ares V represents the vehicle that will again make possible human exploration beyond low Earth orbit. The Ares V is part of NASA s Constellation Program architecture developed to support the International Space Station (ISS), establish a permanent human presence on the Moon, and explore it to an extent far greater than was possible with the Apollo Program. Ares V will carry the lunar lander to orbit where it will join the Orion crew spacecraft, launched by the smaller Ares I launch vehicle. Then the Ares V upper stage will send the Orion and lander to the Moon. Ares V is also intended to launch automated cargo landers to the Moon. The Ares vehicles are designed to employ the proven technologies and experience from the Space Shuttle, Delta IV, and earlier U.S. programs, as well as sharing common components where feasible. The Ares V is in an early stage of concept development. However, commonality allows it to benefit from development work already under way on the Ares I, including the first stage booster, and upper stage, J-2X upper stage engine. This paper will discuss progress to date on the Ares V and its potential for freeing payload designers from current mass and volume constraints. Progress includes development progress on Ares I elements that will be shared by the two launch vehicles. The Ares I first stage recently completed a successful test firing of Development Motor 1 (DM-1). The J-2X engine is proceeding with manufacturing of components for the first development engines that will be used for testing. Several component-level tests have been completed or are under way that will help verify designs and confirm solutions to design challenges. The Ares V Earth departure stage will benefit from the Ares I upper stage development, including design, manufacturing, and materials testing. NASA is also working with government and industry to collect data on flights and testing of the operational RS-68 engine and potential upgrades. The Ares V team continues to evaluate technical options, vehicle configurations, and operations concepts for the Ares V. The team recently completed a Fall Face-to-Face meeting that served as a stepping-stone to the Systems Requirements Review (SRR). This four-day meeting served as an information exchange for the various teams at several NASA field centers and supporting contractors.

Sumrall, Phil↗
DOE OSTI2023

The Innovation of I-Loop

The closing and decommissioning of Halden Boiling Water Reactor in Norway resulted in the loss of many nuclear irradiation testing facilities, notably those providing boiling water reactor (BWR) environments. To lighten the loss of such an important asset, the Advanced Test Reactor (ATR) is being called upon. The recent overhaul of the ATR’s core and the installation of the new Top Head Closure Plate now makes it possible to utilize the ATR’s I-loop locations for I-Loop Tube test facilities. Similar to the current in-pile tube facilities, these new I-Loop facilities will capitalize on the available space and neutron flux the ATR generates in this region of the core for fuels and materials testing. Current efforts are underway to add new PWR and BWR I-Loop Tube facilities to the I-Loop positions for these purposes.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗