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DOE OSTI2026

Precision Polishing of Spheres Via In-Situ Process Monitoring and Machine-Learning-Based Optimization

In inertial confinement fusion (ICF) experiments seeking output gains of unity and beyond, the quality of the ablator capsule is paramount for minimizing hydrodynamic mix that quenches the central hot spot. Defects in the form of foreign particles or missing mass on the surface and within the wall of the capsule are primary offenders. High density carbon capsules made for ICF experiments on the National Ignition Facility (NIF) are precision polished to achieve the surface smoothness in the order of a few nm as well as to minimize isolated defects in the form of pits. Given the critical role of this process, we are developing smart manufacturing techniques with goal of elevating the efficiency of this process. Our approach is to use MEMS-based sensors to capture the fine vibrational signals generated during the polishing process and combine it with synchronized visual feedback as needed. Beyond using these sensors for process monitoring, we use specific deep learning methods to analyze the data and extract correlations with both the process parameters and the final performance of the polishing run. Here, we describe the multiple fronts that we have explored in this regard and the results we have gotten so far. This approach promises to have the potential to ultimately provide real-time feedback that can be used for ensuring the progress of the run as well as a means for faster optimization.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Inhibition of DNA methylation in P. soloecismus alters algae productivity

Eukaryotic organisms regulate the organization, structure, and accessibility of their genomes through chromatin remodeling that can be inherited as epigenetic modifications. These DNA and histone protein modifications are ultimately responsible for an organism’s molecular adaptation to the environment, resulting in distinctive phenotypes. Epigenetic manipulation of algae holds yet untapped potential for the optimization of biofuel production and bioproduct formation; however, epigenetic machinery and modes-of-action have not been well characterized in algae. We sought to determine the extent to which the biofuel platform species Picochlorum soloecismus utilizes DNA methylation to regulate its genome. We found candidate genes with domains for DNA methylation in the P. soloecismus genome. Whole-genome bisulfite sequencing revealed DNA methylation in all three cytosine contexts (CpG, CHH, and CHG). While global DNA methylation is low overall (~1.15%), it occurs in appreciable quantities (12.1%) in CpG dinucleotides in a bimodal distribution in all genomic contexts, though terminators contain the greatest number of CpG sites per kilobase. The P. soloecismus genome becomes hypomethylated during the growth cycle in response to nitrogen starvation. Algae cultures were treated daily across the growth cycle with 20 μM 5-aza-2'-deoxycytidine (5AZA) to inhibit propagation of DNA methylation in daughter cells. 5AZA treatment significantly increased optical density and forward and side scatter of cells across the growth cycle (16 days). This increase in cell size and complexity correlated with a significant increase (~66%) in lipid accumulation. Site specific CpG DNA methylation was significantly altered with 5AZA treatment over the time course, though nitrogen starvation itself induced significant hypomethylation in CpG contexts. Genes involved in several biological processes, including fatty acid synthesis, had altered methylation ratios in response to 5AZA; we hypothesize that these changes are potentially responsible for the phenotype of early induction of carbon storage as lipids. This is the first report to utilize epigenetic manipulation strategies to alter algal physiology and phenotype. Collectively, these data suggest these strategies can be utilized to fine-tune metabolic responses, alter growth, and enhance environmental adaption of microalgae for desired outcomes.

5-aza-2'-deoxycytidine↗

DOE OSTI2022

Phage K gp102 Drives Temperature-Sensitive Antibacterial Activity on USA300 MRSA

There is widespread interest in using obligately lytic bacteriophages (“phages”) to treat human bacterial infections. Among Staphylococcus aureus infections, the USA300 lineage is a frequent cause of invasive disease. We observed that phage K, a model S. aureus myophage, exhibits temperature-sensitive growth on USA300 strains, with the wild-type phage providing poorer growth suppression in broth and forming smaller and fainter plaques at 37 °C vs. 30 °C. We isolated 65 mutants of phage K that had improved plaquing characteristics at 37 °C when compared to the parental phage. In all 65 mutants, this phenotype was attributable to loss-of-function (LoF) mutations in gp102, which encodes a protein of unknown function that has homologs only among the Herelleviridae (SPO1-like myophages infecting gram-positive bacteria). Additional experiments with representative mutants consistently showed that the temperature-sensitive plaque phenotype was specific to USA300 MRSA strains and that Gp102 disruption was correlated with improved suppression of bacterial growth in broth and improved antibacterial activity in a mouse model of upper respiratory tract infection. The same genotype and in vitro phenotypes could be replicated in close relatives of phage K. Gp102 disruption did not have a detectable effect on adsorption but did delay cell culture lysis relative to wild-type under permissive infection conditions, suggesting that gp102 conservation might be maintained by selective pressure for more rapid replication. Expression of gp102 on a plasmid was toxic to both an MSSA and a USA300 MRSA strain. Molecular modeling predicts a protein with two helix-turn-helix domains that displays some similarity to DNA-binding proteins such as transcription factors. While its function remains unclear, gp102 is a conserved gene that is important to the infection process of Kayvirus phages, and it appears that the manner in which USA300 strains defend against them at 37 °C can be overcome by gp102 LoF mutations.

59 BASIC BIOLOGICAL SCIENCES↗

NASA NTRS1976

A study of some effects of vertical shear on thunderstorms

Evidence is presented for the existence of vortices and vortex pairs in thunderstorms. A preliminary parameterized model of the nonthermal generation of thunderstorm vortices derived from field observations of storms and laboratory observations of a jet in crossflow is reported, together with an explanation of how such a model might be used to guide analysis of mesoscale rawinsonde, radar, and satellite data toward an improved capability for prediction of thunderstorm motion and growth. Preliminary analyses of radar and satellite data from Atmospheric Variability Experiment IV are used with available rawinsonde data to develop a correlation between wind shears, instability, and thunderstorm motion and development. Specific studies are recommended for best development of concepts and utilization of data from Atmospheric Variability and Atmospheric Variability Severe Storms Experiments.

Connell, J.↗

NASA NTRS1981

Pilot-optimal multivariable control synthesis by output feedback

A control system design approach for optimal stability augmentation, systems, using limited state feedback theory with the specific inclusion of the human pilot in the loop is presented. The methodology is especially suitable for application to flight vehicles exhibiting nonconventional dynamic characteristics and for which quantitative handling qualities specifications are not available. The design is based on a correlation between pilot ratings and objective function of the optimal control model of the human pilot. Simultaneous optimization for augmentation and pilot gains are required.

Schmidt, D. K.↗

NASA NTRS1982

A preliminary study of crack initiation and growth at stress concentration sites

Crack initiation and propagation models for notches are examined. The Dowling crack initiation model and the E1 Haddad et al. crack propagation model were chosen for additional study. Existing data was used to make a preliminary evaluation of the crack propagation model. The results indicate that for the crack sizes in the test, the elastic parameter K gave good correlation for the crack growth rate data. Additional testing, directed specifically toward the problem of small cracks initiating and propagating from notches is necessary to make a full evaluation of these initiation and propagation models.

Dawicke, D. S.↗

NASA NTRS1985

Comparison of mesospheric ozone measurements using the LRIR and UVMCS satellite instruments

A comparison between mesospheric ozone profiles determined by two radically different satellite-borne instruments is presented for the period of July to November, 1975. The Limb Radiance Inversion Radiometer measured 9.6-micron O3 emission, while the Ultraviolet Multiple Channel Spectrometer measured the atmospheric attenuation of solar ultraviolet radiation during passage of the OSO-8 satellite across the terminator. Only nine near coincident measurements were found. The individual instruments have estimated precision errors of + or - 10 to 15 percent. Agreement between ozone values as measured by the two techniques for specific cases varies between 10 and 20 percent. The statistical correlation is positive and significant at all altitudes where both instruments had reasonable signal-to-noise ratio. A maximum correlation of 0.76 occurred at 0.3 mb (about 59 km).

Millier, F.↗

NASA NTRS1985

Traffic scenario generation technique for piloted simulation studies

Piloted simulation studies of cockpit traffic display concepts require the development of representative traffic scenarios. With the exception of specific aircraft interaction issues, most research questions can be addressed using traffic scenarios consisting of prerecorded aircraft movements merged together to form a desired traffic pattern. Prerecorded traffic scenarios have distinct research advantages, allowing control of traffic encounters with repeatability of scenarios between different test subjects. A technique is described for generation of prerecorded jet transport traffic scenarios suitable for use in piloted simulation studies. Individual flight profiles for the aircraft in the scenario are created interactively with a computer program designed specifically for this purpose. The profiles are then time-correlated and merged into a complete scenario. This technique was used to create traffic scenarios for the Denver, Colorado area with operations centered at Stapleton International Airport. Traffic scenarios for other areas may also be created using this technique, with appropriate modifications made to the navigation fix locations contained in the flight profile generation program.

Williams, David H.↗

NASA NTRS1987

Liquid Engine Jet Atomization Workshop report

The workshop was oriented to disclose information and unsettled problems to understand the fundamental physical mechanism of the droplet formation process. Based on presentation and discussion of results, recommendations were made which should lead to associated future activities. To accomplish this task, existing observations and experiments, contributing to the basic knowledge, providing data for analytical concept verification, and forming a basis for empirical correlations were solicited. Advanced analytical modeling methods or results from specific studies were requested as well as the experience and advice from injector designers. All effort is directed to advance current analytical techniques, simulating the flow behavior downstream of the injection elements in a liquid rocket combustion chamber. Such a tool can be used to optimize injector designs with respect to short length weight savings, wall material protection, or large heat energy transport to a regenerative cooling fluid, while simultaneously achieving the maximum specific impulse in performance. The liquid atomization process also forms a sound basis for combustion instability analysis.

Gross, Klaus W.↗

NASA NTRS1990

A study of the scintillation light induced in liquid xenon by electrons and alpha particles

The time dependence and the intensity of the primary scintillation light in liquid Xe excited by Am-241 alpha particles and Bi-207 internal-conversion electrons were measured at different electric-field strengths. High-purity liquid Xe was used to fill a parallel-plate ionization chamber equipped with a CaF2 window coupled to a UV-sensitive photomultiplier tube. The effect of the specific ionization density on the scintillation light and the time correlation between the light signal and the charge signal is reported. It is demonstrated that the fast scintillation signal produced in liquid Xe by an ionizing particle provides an ideal trigger in a detector aiming at a complete three-dimensional event reconstruction with an excellent background rejection capability.

Aprile, Elena↗

NASA NTRS1999

Cyclic Oxidation of Single-Crystal NiAl-X Alloys

Several single-crystal NiAl-X alloys (X = Hf, Ti, Cr, Ga) were cyclically oxidized at 1000 C for up to 1000 1-hr cycles. The alloys all showed protective, adherent alpha-Al2O3 scale formation with positive weight change behavior throughout the test. There was no clear correlation between the composition of the various alloys and the specific weight gain although the ranking by weight change was relatively consistent for two duplicate series of samples. The presence of Hf (0.5 - 0.8 at.%) resulted in the internal formation of Al2O3/HfO2 "stringers." Diffusion of Hf to the growing oxide stringers resulted in the development of a near-surface layer depleted of these precipitates.

Nesbitt, James A.↗

NASA NTRS2001

Dust Trails of SP/Tuttle and the Unusual Outbursts of the Ursid Shower

Halley-type comets tend to have a series of dust trails that remain spatially correlated for extended periods of time, each dating from a specific return of the comet. Encounters with 1 - 9 revolution old individual dust trails of 55P/Tempel-Tuttle have led to well recognized Leonid shower maxim, the peak time of which was well predicted by recent models. Now. we used the same model to calculate the position of dust trails of comet Shuttle, a Halley-type comet in an (approximately) 13.6 year orbit passing just outside of Earth's orbit. We discovered that the meteoroids tend to be trapped in the 14:12 mean motion resonance with Jupiter, while the comet librates in a slightly shorter period orbit around the 13:15 resonance. It takes six centuries to change the orbit enough to intersect Earth's orbit. During that time, the meteoroids and comet separate in mean anomaly by six years. thus explaining the unusual aphelion occurrences of Ursid outbursts. The resonances also prevent dispersion, so that the dust trail encounters (specifically, from dust trails of AD 1378 - 1405) occur only in one year in each orbit. We predicted enhanced activity on December 22, 2000, at around 7:29 and 8:35 UT (universal time) from dust trails dating to the 1405 and 1392 return, respectively. This event was observed from California using video and photographic techniques. At the same time, five Global-MS-Net stations in Finland, Japan and Belgium counted meteors using forward meteor scatter. The outburst peaked at 8:06:07 UT, December 22, at Zenith Hourly Rate (approx.) 90 per hour. The Ursid rates were above half peak intensity during 4.2 hours. This is only the second Halley type comet for which a meteor outburst can be dated to a specific return of the parent comet, and traces their presence back form 9 to at least 45 revolutions of the comet. New orbital elements of Ursid meteoroids are presented. We find that most orbits do scatter around the anticipated positions, confirming the link with comet Shuttle and the epoch of ejection. The 1405 and.1392 dust trails appear to have contributed similar amounts to the activity profile. Some orbits provide a hint of much older debris being present as well. Some of the dispersion in the radiant position may reflect a true variation in inclinations, with two groupings at low and high values, which is not understood at present.

Jenniskens, Peter↗

NASA NTRS2003

Consumer Expectations of Capacity Constrains and Their Effect on the Demand for Multi-Class Air Travel

This paper argues that a consumer's decision on ticket class takes into account the expected likelihood of obtaining a seat in a particular class which, in turn, partially depends on an optimum "transaction cost". Taking into account the preferences of the consumer and the information that the consumer is endowed with, the consumer will select a ticket that includes its own optimal transaction cost. This motivates the inclusion of the capacity constraint as a proxy independent variable for these consumer expectations This then forms the basis of a model of air-travel demand with specific reference to Australia. A censored likelihood function allowing for correlation in the disturbance term across k classes is introduced. The correlation in the disturbances arises as a result of the interdependence of the capacity constraints in k different ticket classes on each flight.

Battersby, Bryn D.↗

NASA NTRS2003

Using a Portfolio of Algorithms for Planning and Scheduling

The Automated Scheduling and Planning Environment (ASPEN) software system, aspects of which have been reported in several previous NASA Tech Briefs articles, includes a subsystem that utilizes a portfolio of heuristic algorithms that work synergistically to solve problems. The nature of the synergy of the specific algorithms is that their likelihoods of success are negatively correlated: that is, when a combination of them is used to solve a problem, the probability that at least one of them will succeed is greater than the sum of probabilities of success of the individual algorithms operating independently of each other. In ASPEN, the portfolio of algorithms is used in a planning process of the iterative repair type, in which conflicts are detected and addressed one at a time until either no conflicts exist or a user-defined time limit has been exceeded. At each choice point (e.g., selection of conflict; selection of method of resolution of conflict; or choice of move, addition, or deletion) ASPEN makes a stochastic choice of a combination of algorithms from the portfolio. This approach makes it possible for the search to escape from looping and from solutions that are locally but not globally optimum.

Sherwood, Robert↗

DOE OSTI2021

MULTIPHYSICS-MODELING OF FIRE-INDUCED URANIUM AEROSOL FORMATION – A-POSTERIORI BENCHMARKING OF EXPERIMENTS

The formulation and solution of a model that properly described the temperature profiles of uranium in fire conditions was prepared, verified and validated, to support a-posteriori benchmarking of historical experiments. Data from the multi-physics model combined with data regression from the experiments provides a useful tool for exploring sources of potential bias in historical experiments. The approaches used are augmented by visual observations and photographic evidence allowing for correlations between various phenomena, independent of whether or not that specific phenomena are part of the validated model. In this manner, the validated model is a tool for a-posteriori benchmarking, and not a model designed to replicate the experimental output exactly for any specific experiment. For experiments like the Clark (2015) experiments, this integrated model (including chemistry) demonstrated that the largest bias was associated in the metallurgy of the coupons. The model developed does serve as a basis for defending which of the historical alloys tested are the most appropriate for any other alloy being considered (e.g., one that has not yet been tested). The model identifies key reactions that impact uranium chemistry and can significantly bias experimental results. Through use of the model and energy balances, data from historical experiments by Elder and Tinkle (1980) were regressed and benchmarked. This study identifies that all uranium alloys are not equal and that there are distinct differences between the dominant alloys representing distinct metallurgical phases.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2022

Quantifying deformation during Zry-4 burst testing: a comparison of BISON and a combined in-situ digital image correlation and infrared thermography method

The development and verification of nuclear fuel-cladding performance codes require extensive testing to establish empirical correlations, necessitating more accelerated testing methods that can replace large validation studies. Here, in the present work, a technique was developed and implemented to experimentally quantify the relationship between temperature, cladding internal pressure, and strain in-situ during a burst test, with the specific aim of generating data for code validation and model refinement. Digital image correlation was used to measure hoop, axial, and radial strain, and infrared thermography to quantify axial temperature gradients. Several key experimental modifications to traditional LOCA burst testing were necessary, but are shown to effectively have little impact on burst temperatures. The time/temperature dependent pressure and time/spatially dependent thermal gradient data were used with BISON to simulate cladding burst and strain rates. Although the measured DIC strains reach appreciable amounts at slightly lower temperatures than BISON simulated strains, there is good agreement between the measured and simulated strains in terms of magnitude and rates leading up to burst. However, in the few seconds prior to and during burst, the BISON simulated strains are significantly lower than the measured strains, indicating the potential for model improvement. The combined experiment and simulation technique may be applied to any new cladding concept to accelerate fuel qualification.

36 MATERIALS SCIENCE↗

DOE OSTI2023

Enhanced Dynamics and Charge Transport at the Eutectic Point: A New Paradigm for the Use of Deep Eutectic Solvent Systems

Deep eutectic solvents (DESs) are a class of versatile solvents with promise for a wide range of applications, from separation processes to electrochemical energy storage technologies. A fundamental understanding of the correlation among the structure, thermodynamics, and dynamics of these materials necessary for targeted rational design for specific applications is still nascent. Here, we employ differential scanning calorimetry (DSC), broadband dielectric spectroscopy (BDS), and femtosecond transient absorption spectroscopy (fs-TAS) to investigate the correlation among thermodynamics, dynamics, and charge transport in mixtures comprising a wide range of compositions of choline chloride (ChCl) and ethylene glycol (EG). Detailed analyses reveal that (i) the eutectic composition of this prototypical DES occurs in the 15–20 mol % ChCl in the EG range rather than the previously assumed 33 mol %, and (ii) both rotational dynamics and charge transport at the eutectic composition are enhanced in this composition range. These findings highlight the fundamental interplay between thermodynamics and dynamics in determining the properties of DESs that are relevant to many applications.

25 ENERGY STORAGE↗

NASA NTRS2002

Variability of Winter Air Temperature in Mid-Latitude Europe

The aim of this paper is to report extreme winter/early-spring air temperature (hereinafter temperature) anomalies in mid-latitude Europe, and to discuss the underlying forcing to these interannual fluctuations. Warm advection from the North Atlantic in late winter controls the surface-air temperature, as indicated by the substantial correlation between the speed of the surface southwesterlies over the eastern North Atlantic (quantified by a specific Index Ina) and the 2-meter level air temperatures (hereinafter Ts) over Europe, 45-60 deg N, in winter. In mid-March and subsequently, the correlation drops drastically (quite often it is negative). This change in the relationship between Ts and Ina marks a transition in the control of the surface-air temperature: absorption of insolation replaces the warm advection as the dominant control. This forcing by maritime-air advection in winter was demonstrated in a previous publication, and is re-examined here in conjunction with extreme fluctuations of temperatures in Europe. We analyze here the interannual variability at its extreme by comparing warm-winter/early-spring of 1989/90 with the opposite scenario in 1995/96. For these two December-to-March periods the differences in the monthly mean temperature in Warsaw and Torun, Poland, range above 10 C. Short-term (shorter than a month) fluctuations of the temperature are likewise very strong. We conduct pentad-by-pentad analysis of the surface-maximum air temperature (hereinafter Tmax), in a selected location, examining the dependence on Ina. The increased cloudiness and higher amounts of total precipitable water, corollary effects to the warm low-level advection. in the 1989/90 winter, enhance the positive temperature anomalies. The analysis of the ocean surface winds is based on the Special Sensor Microwave/Imager (SSM/I) dataset; ascent rates, and over land wind data are from the European Centre for Medium-Range Weather Forecasts (ECMWF); maps of 2-m temperature, cloud cover and precipitable water are from the National Centers for Environmental Prediction (NCEP) Reanalysis.

Otterman, J.↗