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At least 775 records · Page 43

Reliability Assessment of Graphite Specimens under Multiaxial Stresses

An investigation was conducted to predict the failure strength response of IG-100 nuclear grade graphite exposed to multiaxial stresses. As part of this effort, a review of failure criteria accounting for the stochastic strength response is provided. The experimental work was performed in the early 1990s at the Oak Ridge National Laboratory (ORNL) on hollow graphite tubes under the action of axial tensile loading and internal pressurization. As part of the investigation, finite-element analysis (FEA) was performed and compared with results of FEA from the original ORNL report. The new analysis generally compared well with the original analysis, although some discrepancies in the location of peak stresses was noted. The Ceramics Analysis and Reliability Evaluation of Structures Life prediction code (CARES/Life) was used with the FEA results to predict the quadrants I (tensile-tensile) and quadrant IV (compression-tension) strength response of the graphite tubes for the principle of independent action (PIA), the Weibull normal stress averaging (NSA), and the Batdorf multiaxial failure theories. The CARES/Life reliability analysis showed that all three failure theories gave similar results in quadrant I but that in quadrant IV, the PIA and Weibull normal stress-averaging theories were not conservative, whereas the Batdorf theory was able to correlate well with experimental results. The conclusion of the study was that the Batdorf theory should generally be used to predict the reliability response of graphite and brittle materials in multiaxial loading situations.

Sookdeo, Steven↗

Requirements for Auxiliary Stiffeners Attached to Panels Under Combined Compression and Shear

Panels of aluminum alloy sheets, framed by side and end stiffeners, were subjected to combined loading by means of offset knife edges applying loads to top and bottom end plates with reacting forces against the end plates supplied by laterally acting rollers. The test specimens were 17S-T aluminum alloy shoots 0.040 inch thick in panels of 10-inch width and three different lengths (approximately 10, 26, and 30 inch). Data were obtained for the bowing of transverse and longitudinal ribs of rectangular cross section and varying depths mounted on one side of the sheet only, for several ratios of compression to shear loads. Limiting values of the moments of inertia were calculated from these measurements. The experimental values exceed the theoretical values given by Timoshenko for the case of simply supported sheets with uniformly distributed boundary stresses. The work reported includes measurements of the effective shear moduli of the nine test panels with and without ribs. These data are compared with values published by Lahdo and Wagner.

ALUMINUM ALLOYS, SHEET - ALCOA 17ST - STRENGTH↗

Equation of state and strength of diamond in high-pressure ramp loading

Diamond is used extensively as a component in high-energy-density experiments, but existing equation of state (EOS) models do not capture its observed response to dynamic loading. In particular, in contrast with first-principles theoretical models of equilibrium multiphase EOS, no solid-solid phase changes have been detected, and no general-purpose EOS models match the measured ambient isotherm. We have performed density functional theory (DFT) calculations of the diamond phase to ~10 TPa, well beyond its predicted range of thermodynamic stability, and used these results as the basis of a Mie-Grüneisen EOS. We also performed DFT calculations of the elastic moduli, and calibrated an algebraic elasticity model for use in simulations. We then estimated the flow stress of diamond by comparison with the stress-density relation measured experimentally in ramp-loading experiments. Furthermore, the resulting constitutive model allows us to place a constraint on the Taylor-Quinney factor (the fraction of plastic work converted to heat) from the observation that diamond does not melt on ramp compression.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Vanishing dynamic strength measured in a transient high-pressure phase of tin

This work reports two independent experimental estimations of the dynamic strength of the body-centered tetragonal (bct) 𝛾 phase of tin, which occurs at pressures above about 9 GPa and transforms promptly back to the ambient 𝛽 phase upon pressure release. Measuring strength in such a transient high-pressure phase is challenging. One measurement used free-surface Richtmyer-Meshkov instabilities generated with gas gun impact. Another set of measurements used ramp-release loading in a pulsed-power facility. Strength estimations came from comparison to simulations using a comprehensive multiphase modeling framework that includes equation of state, shear moduli, and strength separately for each phase, and treats mixed-phase regions. Both experimental methods found the 𝛾-phase strength to be very low, within experimental uncertainty of zero. The existing literature on other materials, by contrast, almost universally reports higher strength in transient high-pressure phases compared with ambient phases. Recent Molecular-Dynamics simulations on tin in the literature showed almost zero deviatoric strength during a deformation-induced bct → bct transformation in which one of the 𝛾-phase 𝑎 axes “flips” to the 𝑐 axis. This reorientation currently provides the most plausible explanation for the low observed strength in 𝛾-phase tin.

36 MATERIALS SCIENCE↗

A real-time interferometer technique for compressible flow research

Strengths and shortcomings in the application of interferometric techniques to transonic flow fields are examined and an improved method is elaborated. Such applications have demonstrated the value of interferometry in obtaining data for compressible flow research. With holographic techniques, interferometry may be applied in large scale facilities without the use of expensive optics or elaborate vibration isolation equipment. Results obtained using holographic interferometry and other methods demonstrate that reliable qualitative and quantitative data can be acquired. Nevertheless, the conventional method can be difficult to set up and apply, and it cannot produce real-time data. A new interferometry technique is investigated that promises to be easier to apply and can provide real-time information. This single-beam technique has the necessary insensitivity to vibration for large scale wind tunnel operations. Capabilities of the method and preliminary tests on some laboratory scale flow fluids are described.

Bachalo, W. D.↗

Alleviation of Mechanical Anisotropy in Ultrafine/Nano-grained AZ31 Magnesium Alloy

An ultrafine/nano-grained AZ31 magnesium alloy was processed through multipass accumulative back extrusion at 280 and 380 °C. Texture analysis was conducted to determine preferred crystallographic orientations developed during multipass deformation. The anisotropy in mechanical properties of the processed materials was studied by compressive and tensile testing. The results implied that the accumulative back extrusion effectively reduces the anisotropy of yield strength, ultimate strength and strain-to-fracture during compressive and tensile loading. The operations of different twinning/slip systems during compressive and tensile deformation were discussed using Schmid factors measurements. A decrease in twinning-related anisotropy, as well as the contribution of different slip systems in strain accommodation, could reduce the mechanical anisotropy of ultrafine/nano-grained AZ31 alloy. The compressive strength of the two-pass processed material was lower along extrusion direction than transverse direction; however, the result was reverse after four passes. The tensile behavior implied that the contribution of basal slip might accommodate strain along length as well as the thickness of the specimen, while prismatic slip may assist in narrowing the width of the specimen and elongating the length.

36 MATERIALS SCIENCE↗

Physical Properties of the Stone Meteorites: Implications for the Properties of Their Parent Bodies

The physical properties of the stone meteorites provide important clues to understanding the formation and physical evolution of material in the Solar protoplanetary disk as well providing indications of the properties of their asteroidal parent bodies. Knowledge of these properties is essential for modeling a number of Solar System processes, such as bolides in planetary atmospheres, the thermal inertia of atmosphereless solid body surfaces, and the internal physical and thermal evolution of asteroids and rock-rich icy bodies. In addition, insight into the physical properties of the asteroids is important for the design of robotic and crewed reconnaissance, lander, and sample return spacecraft missions to the asteroids. One key property is meteorite porosity, which ranges from 0% to more than 40%, similar to the range of porosities seen in asteroids. Porosity affects many of the other physical properties including thermal conductivity, speed of sound, deformation under stress, strength, and response to impact. As a result of the porosity, the properties of most stone meteorites differ significantly from those of compact terrestrial rocks, whose physical properties have been used in many models of asteroid behavior. A few physical properties, such as grain density, magnetic susceptibility, and heat capacity are not functions of porosity. Taken together, the grain density and the magnetic susceptibility can be used to classify unweathered or minimally weathered ordinary chondrites. This provides a rapid screening technique to identify heterogeneous samples, classify new samples, and identify misclassified meteorites or interlopers in strewn fields.

Chondritic meteorites↗

At Extreme Strain Rates, Pure Metals Thermally Harden while Alloys Thermally Soften

When materials are deformed at extreme strain rates, >10 6 s -1 , a counterintuitive mechanical response is seen where the strength and hardness of pure metals increases with increasing temperature. This anti-thermal hardening is due to dislocations meeting resistance to their motion from phonons in the crystal lattice. However, here, using optically-driven microballistic impact testing to measure dynamic strength and hardness, we show that when the composition is systematically varied away from high purity, the mechanical response of metals transitions from phonon drag of dislocations back to thermally activated pinning of dislocations, even at the highest strain rates. This boundary from “hotter-is-stronger” to “hotter-is-softer” is observed and mapped for nickel, titanium and gold. Furthermore, the ability to tune between deformation mechanisms with very different temperature dependencies speaks to new directions for alloy design in extreme conditions.

Ballistic transport↗

A Study of the Efficiency of High-strength, Steel, Cellular-core Sandwich Plates in Compression

Structural efficiency curves are presented for high-strength, stainless-steel, cellular-core sandwich plates of various proportions subjected to compressive end loads for temperatures of 80 F and 600 F. Optimum proportions of sandwich plates for any value of the compressive loading intensity can be determined from the curves. The efficiency of steel sandwich plates of optimum proportions is compared with the efficiency of solid plates of high-strength steel and aluminum and titanium alloys at the two temperatures.

SANDWICH AND LAMINATES↗

Enhanced Mechanical, Tribological, and Thermal Properties of Fe{sub 3}Al Composites with Carbon Nanotubes

In this work, Fe{sub 3}Al-based composites reinforced with carbon nanotubes were fabricated by a hot-press sintering process under various sintering pressures. The effects of sintering pressure and additives (alumina and lanthanum) on both the physical and the mechanical properties were systematically investigated. Results showed that with the sintering pressure of 15 MPa and incorporation of carbon nanotubes (CNTs), the microhardness of Fe{sub 3}Al composite exhibited a peak value at 1038.1 HV, which was ~ 60% higher than those without the addition of carbon nanotubes (644.9 HV). Also, both the compressive yield strength and the thermal conductivity of Fe{sub 3}Al composite were also significantly improved. Results of wear test showed the Fe{sub 3}Al composite exhibited a low wearing rate (10{sup −6}-10{sup −5} order of magnitude) and a friction coefficient (0.53-0.67).

36 MATERIALS SCIENCE↗

Investigation on Equal-Channel Angular Pressing-Induced Grain Refinement in an Aluminum Matrix Composite Reinforced with Al-Cu-Ti Metallic Glass Particles

In the present study, a homogeneous ultrafine grain structure composite consisting of metallic glass particles reinforcements was developed by equal-channel angular pressing (ECAP) process. The microstructure of composite was characterized using x-ray diffraction (XRD), transmission electron microscopy (TEM) and electron backscatter diffraction (EBSD) techniques. The uniaxial compression test was used to determine the mechanical properties. The mechanisms of grain refinement during ECAP process were discussed based on the microstructural evolutions. A composite was successfully produced after four passes of ECAP, having an average grain size of 610 nm and compressive yield strength of 242 MPa. Also, the yield strength of composite after each pass was quantitatively estimated by considering all the effective strengthening mechanism. The findings showed that the dislocations strengthening mechanism with contribution of more than 50% plays a major role in strengthening the composite. There was a negligible gap between the experimental and theoretical values of yield strength for all ECAP pass numbers.

36 MATERIALS SCIENCE↗

Effect of Cobalt Content on Thermal, Mechanical, and Microstructural Properties of Al{sub 0.4}FeCrNiCo{sub x} (x = 0, 0.25, 0.5, 1.0 mol) High-Entropy Alloys

Al{sub 0.4}FeCrNiCo{sub x} (x = 0, 0.25, 0.5, 1.0 mol) high-entropy alloys are developed by arc melting route to investigate the effect of cobalt content on thermal, mechanical, and microstructural properties. The phase, microstructure, and chemical composition are analyzed using x-ray diffraction, transmission electron microscope, and scanning electron microscope with attached energy-dispersive x-ray spectrometer. The obtained results have shown that the Al{sub 0.4}FeCrNiCo{sub x} (x = 0-0.5 mol) high-entropy alloys form a simple FCC + BCC-type solid solution and Al{sub 0.4}FeCrNiCo{sub x=1} HEA forms a single-phase FCC structure. The compressive yield strength, microhardness, and thermal conductivity are observed to decrease from 965.22 to 233.37 MPa, 253.6 to 155.6 HV, and from 4.87 to 2.674 W/mK, respectively, whereas the electrical resistivity is observed to increase from 150.30 to 273.74 µΩ-cm with the addition of cobalt from x = 0-1 mol. Differential scanning calorimetry analysis has indicated that the Al{sub 0.4}FeCrNiCo{sub x} (x = 0, 0.25, 0.5, 1.0 mol) high-entropy alloys are thermally stable up to 1000 °C.

36 MATERIALS SCIENCE↗

Effect of Y{sub 2}O{sub 3} Addition on the Microstructure, Wear Resistance, and Corrosion Behavior of W-4.9Ni-2.1Fe Heavy Alloy

Binding and particle phases are the two important parameters influencing materials properties. In this study, a series of novel W-4.9Ni-2.1Fe-xY{sub 2}O{sub 3} (in weight%) alloys with different Y{sub 2}O{sub 3} contents are prepared by secondary ball milling and spark plasma sintering (SPS) techniques to obtain uniformly distributed γ-(Ni, Fe) binding phases and finer grains. The microstructure, mechanical, wear resistance, and corrosion behavior of the sintered bodies with different Y{sub 2}O{sub 3} were obtained by x-ray diffraction, scanning electron microscopy, Rockwell hardness tester, friction wear tester, and three-dimensional profile instruments. The results showed that a certain addition of Y{sub 2}O{sub 3} led to refined grains and uniformed microstructures; but, if excessive, a weak grain refinement would be appeared. Moreover, the grain size tends to be stable with enhancing of the Y{sub 2}O{sub 3} content. Considering properties such as density, hardness, compression yield strength, grain size, and uniform distribution of tungsten hard phase and γ-(Ni, Fe) binding phase, the comprehensive optimal amount of 0.7 wt.% of Y{sub 2}O{sub 3} was attained for the alloy. Meanwhile, the SPS sintered body also exhibited the best friction, wear behavior, and corrosion resistance in 3.5% of NaCl solution.

36 MATERIALS SCIENCE↗

Strengthening Mechanisms and Deformation Behavior of Industrially-Cast and Lab-Cast Dual-Phase High Entropy Alloy

An iron-rich high entropy alloy Al 0.65 CoCrFe 2 Ni comprising of both FCC and BCC phases was designed and fabricated using induction melting at a large industrial scale and suction casting at a small lab scale. Spinodally decomposed interdendritic regions were uniformly distributed in the industrially melted alloy, and a finer dendritic structure with smaller sized spinodal structures was observed in the alloy suction cast at lab scale. The suction cast alloy fabricated at the lab scale exhibited significantly higher compressive yield strength compared to the industrially cast alloy. The relative strengthening contributions in the alloys due to solid solution, grain boundary, dislocation interactions and interphase boundary were analyzed. Dislocation hardening was the major contributor responsible for the higher strength of the SC alloy. The deformation behavior in the alloys was examined with the help of orientation image mapping. Finally, intense slip band formation at large strains in the industrially melted alloy indicates that cold working can be an effective technique to enhance the strength of the dual-phase high entropy alloy processed at a large scale.

36 MATERIALS SCIENCE↗

Comparison of three state-of-the-art crystal plasticity based deformation twinning models for magnesium alloys

In magnesium alloys, deformation twinning and its interactions with dislocation slip are responsible for a sigmoidal shape stress–strain behavior and an asymmetrical tension–compression yield strength in magnesium alloys. The sensitivity of twinning to the underlying microstructure renders the crystal plasticity method the most commonly adopted modeling approach for magnesium-twinning. This paper compares three state-of-the-art crystal plasticity-based twinning models from the literature, namely the elastic-viscoplastic self-consistent twinning-detwinning (EVPSC-TDT) model, crystal plasticity finite element model based on enhanced predominate twin reorientation approach (CPFE-ePTR), and the crystal plasticity finite element model based on “discrete twinning” approach (CPFE-DT). A polycrystalline microstructure is simulated with all three methods to compare the resulting stress–strain curves and lattice strains to those from the experimentally measured data. All three methods showed the capability of capturing the experimental results with different levels of accuracy. Additionally, the EVPSC-TDT method avoids solving the finite element matrices and showed the highest computational efficiency. The CPFE-ePTR model shows a higher accuracy in capturing the lattice strain. The CPFE-DT relies on high-resolution finite element mesh and is much slower than the other two methods, but it captured the local deformation concentration and stress reversal phenomena near the twin band, which was not possible with the other two methods. Based on the comparison, guidance for the selection of the appropriate model based on the specific modeling target is provided in this paper.

36 MATERIALS SCIENCE↗

Development of high-early-strength fiber-reinforced self-compacting concrete

High-early-strength fiber-reinforced self-compacting concrete (FRSCC) is a practical material for the precast concrete industry to double its production capacity. In this study, we developed high-early-strength FRSCC mixtures that achieved a compressive and flexural strength of at least 24 MPa and 3.5 MPa, respectively, at 6 h, using commercially available components, typical mixing procedures, and air curing. A mix design process was developed based on the literature and experimental results. The effect of six different fiber reinforcements on the fresh and mechanical properties of concrete was analyzed. The cost limit was set at 523 USD/m 3 to make the concrete mix cost-effective.

36 MATERIALS SCIENCE↗