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At least 793 records · Page 44

The hard x-ray nanotomography microscope at the advanced light source

Beamline 11.3.1 at the Advanced Light Source is a tender/hard (6–17 keV) x-ray bend magnet beamline recently re-purposed with a new full-field, nanoscale transmission x-ray microscope. The microscope is designed to image composite and porous materials possessing a submicrometer structure and compositional heterogeneity that determine materials’ performance and geologic behavior. The theoretical and achieved resolutions are 55 and <100 nm, respectively. The microscope is used in tandem with a <25 nm eccentricity rotation stage for high-resolution volume imaging using nanoscale computed tomography. The system also features a novel bipolar illumination condenser for the illumination of an ~100 μm spot of interest on the sample, followed by a phase-type zone plate magnifying objective of ~52 µm field of view and a phase detection ring. The zone plate serves as the system objective and magnifies the sample with projection onto an indirect x-ray detection system, consisting of a polished single crystal CsI(Tl) scintillator and a range of high-quality Plan Fluorite visible light objectives. The objectives project the final visible light image onto a water-cooled CMOS 2048 × 2048-pixel 2 detector. Here, in this paper, we will discuss the salient features of this instrument and describe early results from imaging the internal three-dimensional microstructure and nanostructure of target materials, including fiber-reinforced composites and geomaterials.

47 OTHER INSTRUMENTATION↗

A Bayesian approach to real-time 3D tumor localization via monoscopic x-ray imaging during treatment delivery

Purpose: Monoscopic x-ray imaging with on-board kV devices is an attractive approach for real-time image guidance in modern radiation therapy such as VMAT or IMRT, but it falls short in providing reliable information along the direction of imaging x-ray. By effectively taking consideration of projection data at prior times and/or angles through a Bayesian formalism, the authors develop an algorithm for real-time and full 3D tumor localization with a single x-ray imager during treatment delivery. Methods: First, a prior probability density function is constructed using the 2D tumor locations on the projection images acquired during patient setup. Whenever an x-ray image is acquired during the treatment delivery, the corresponding 2D tumor location on the imager is used to update the likelihood function. The unresolved third dimension is obtained by maximizing the posterior probability distribution. The algorithm can also be used in a retrospective fashion when all the projection images during the treatment delivery are used for 3D localization purposes. The algorithm does not involve complex optimization of any model parameter and therefore can be used in a ''plug-and-play'' fashion. The authors validated the algorithm using (1) simulated 3D linear and elliptic motion and (2) 3D tumor motion trajectories of a lung and a pancreas patient reproduced by a physical phantom. Continuous kV images were acquired over a full gantry rotation with the Varian TrueBeam on-board imaging system. Three scenarios were considered: fluoroscopic setup, cone beam CT setup, and retrospective analysis. Results: For the simulation study, the RMS 3D localization error is 1.2 and 2.4 mm for the linear and elliptic motions, respectively. For the phantom experiments, the 3D localization error is < 1 mm on average and < 1.5 mm at 95th percentile in the lung and pancreas cases for all three scenarios. The difference in 3D localization error for different scenarios is small and is not statistically significant. Conclusions: The proposed algorithm eliminates the need for any population based model parameters in monoscopic image guided radiotherapy and allows accurate and real-time 3D tumor localization on current standard LINACs with a single x-ray imager.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

A SEARCH FOR X-RAY EMISSION FROM COLLIDING MAGNETOSPHERES IN YOUNG ECCENTRIC STELLAR BINARIES

Among young binary stars whose magnetospheres are expected to collide, only two systems have been observed near periastron in the X-ray band: the low-mass DQ Tau and the older and more massive HD 152404. Both exhibit elevated levels of X-ray emission at periastron. Our goal is to determine whether colliding magnetospheres in young high-eccentricity binaries commonly produce elevated average levels of X-ray activity. This work is based on Chandra snapshots of multiple periastron and non-periastron passages in four nearby young eccentric binaries (Parenago 523, RX J1622.7-2325 Nw, UZ Tau E, and HD 152404). We find that for the merged sample of all four binaries the current X-ray data show an increasing average X-ray flux near periastron (at a ∼2.5-sigma level). Further comparison of these data with the X-ray properties of hundreds of young stars in the Orion Nebula Cluster, produced by the Chandra Orion Ultradeep Project (COUP), indicates that the X-ray emission from the merged sample of our binaries cannot be explained within the framework of the COUP-like X-ray activity. However, due to the inhomogeneities of the merged binary sample and the relatively low statistical significance of the detected flux increase, these findings are regarded as tentative only. More data are needed to prove that the flux increase is real and is related to the processes of colliding magnetospheres.

79 ASTRONOMY AND ASTROPHYSICS↗

Particle Simulation of High-Intensity X-Ray Laser Interaction

This Feasibility Study Project began with two goals: 1.) Develop the techniques needed to combine molecular dynamics (MD) particle simulation with atomic kinetics described by a "Collisional-Radiative" (CR) model. Investigate the computational requirements and possible physics improvements to the calculation, especially quantum corrections. The feasibility question is: "Can we do the calculation and will it run fast enough to be useful?" 2.) Test the calculations against X-ray Free-electron Laser interaction experiments on solid Fe targets performed by Prof. H. Yoneda et al. at the SACLA XFEL facility in the SPring-8 laboratory in Harima, Japan.

42 ENGINEERING↗

Calibrating X-ray Imaging Devices for Accurate Intensity Measurement

The purpose of the project presented is to develop methods to accurately calibrate X-ray imaging devices. The approach was to develop X-ray source systems suitable for this endeavor and to develop methods to calibrate solid state detectors to measure source intensity. NSTec X-ray sources used for the absolute calibration of cameras are described, as well as the method of calibrating the source by calibrating the detectors. The work resulted in calibration measurements for several types of X-ray cameras. X-ray camera calibration measured efficiency and efficiency variation over the CCD. Camera types calibrated include: CCD, CID, back thinned (back illuminated), front illuminated.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Vertical Habitability Layout Studies and Neutral Buoyancy/Parabolic Flight Habitat Studies

In the Summer of 2013, the University of Maryland was selected for two projects under the NASA X-Hab 2014 program, administered by the National Space Grant Foundation: Vertical Habitability Layout Studies (XHab201406) and Neutral Buoyancy/Parabolic Flight Habitat Studies (XHab201407). This document, at the direction of the NASA Technical Monitor, comprises the final report for both of these contracts. Recognizing from the outset the mismatch between the desired scope of research activities under the contracts and the severely limited funding and duration, the University of Maryland leveraged the X-Hab support by integrating the programs into a number of academic classes throughout the 2013-2014 academic year. By far the most significant interaction was with the Department of Aerospace Engineering Senior capstone experience in spacecraft design sequence, ENAE 483/484. Throughout the academic year, 42 students in this sequence worked on both projects in conjunction with their senior project to design an artificial gravity research station in a distant lunar retrograde orbit. As part of this research project, the students worked with previously created 1-G habitats and underwater simulations to better understand habitat design from microgravity to full Earth gravity, as well as at lunar and Mars gravity levels between those two endpoints.

David L. Akin↗

Development of Short-Pulse Laser-Based Diagnostics for Pulsed Power-Driven Warm Dense Matter

This report summarizes a research project conducted at the Physics Department’s Zebra Pulsed Power Laboratory (ZPPL) at the University of Nevada Reno, aimed at developing short-pulse laser-based diagnostics to probe pulsed-power-driven warm dense matter. ZPPL combines a MegaAmpere (MA) pulsed power generator, Zebra, and a relativistic intensity, short-pulse laser, Leopard, offering a unique university-scale platform for high energy density physics, laboratory astrophysics, and inertial fusion energy research. The project focused on establishing a hard X-ray radiographic capability using high-intensity, short-pulse laser-generated X-rays to probe warm dense matter created by the Zebra current. Initial experiments produced X-ray radiographs of a static (cold) aluminum wire using silver and gold foil and wire targets, but intense background radiation from Zebra shots overwhelmed the laser-produced X-rays. To mitigate this, a radiationhardened detector housing was designed and implemented. Additional diagnostic, including a filter stack bremsstrahlung spectrometer and an X-ray pinhole camera, were developed to characterize laser-produced hard X-ray spectra and locate hard X-ray sources in the vacuum chamber. These revealed that strong hard X-rays (> 20 keV) originated near the anode cap, bombarded by energetic electrons. Due to laser unavailability during some experiments, detector performance was successfully tested using hard X-ray sources from the Zebra current, demonstrating their readiness for coupled experiments. The project supported one Ph.D. student (Dr. Lei Chen), who conducted experimental and numerical research, and provided training opportunities and data for three undergraduate senior theses.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Localized phase contrast imaging at the Wendelstein 7-X stellarator

In its basic form, phase contrast imaging (PCI) provides line-integrated measurements of electron density fluctuations in plasmas. As turbulent fluctuations in magnetically confined plasmas have wave vectors almost perpendicular to the background magnetic field, the signals scattered by fluctuations from different parts of the PCI line-of-sight (LoS) are spatially separated in focal planes of the plasma. This allows localized PCI measurements by placing a mask in such a plane, to only permit signals from specific parts of the LoS to reach the PCI detectors. The present paper describes modeling and design of localization masks for the PCI system at the Wendelstein 7-X (W7-X) stellarator as well as the first results obtained using the masks in the recent long-pulse W7-X experimental campaign. During this project, we have extended the theory describing the mask response within the Fraunhofer diffraction model. As a novel development, we show from first principles that the mask response is determined by the fraction of power of the scattered beam spots that passes the mask. These insights have been used to select the W7-X mask design, consisting of a circular cutout, allowing the unscattered beam spot to pass the mask, with wedges covering a fixed angular range outside the central cutout. In the recent W7-X experimental campaign, the masks have verified the location of the main turbulence features observed by the PCI system and provided new information about the location of short-wavelength magnetohydrodynamic modes.

Physics↗

POSSIBLE CONSTRAINTS ON EXOPLANET MAGNETIC FIELD STRENGTHS FROM PLANET-STAR INTERACTION

A small percentage of normal stars harbor giant planets that orbit within a few tenths of an astronomical unit. At such distances, the potential exists for significant tidal and magnetic field interaction resulting in energy dissipation that may manifest as changes within the stellar corona. We examine the X-ray emission of stars hosting planets and find a positive correlation between X-ray luminosity and the projected mass of the most closely orbiting exoplanets. We investigate possible systematics and observational biases that could mimic or confuse this correlation but find no strong evidence for any, especially for planets more massive than {approx}0.1 M{sub J} . Luminosities and upper limits are consistent with the interpretation that there is a lower floor to stellar X-ray emission dependent on close-in planetary mass. Under the hypothesis that this is a consequence of planet-star magnetic field interaction, and energy dissipation, we estimate a possible field strength increase of a factor of {approx}8 between planets of 1 and 10 M{sub J} . Intriguingly, this is consistent with recent geodynamo scaling law predictions. The high-energy photon emission of planet-star systems may therefore provide unique access to the detailed magnetic, and hence geodynamic, properties of exoplanets.

79 ASTRONOMY AND ASTROPHYSICS↗

Deep learning reconstruction of attosecond X-ray pulses from an angularly streaked 2D photoelectron momentum distribution

The Linac Coherent Light Source (LCLS) at SLAC National Accelerator Laboratory produces intense X-ray pulses using a beam of accelerated electrons. The X-ray laser enhanced attosecond pulse generation (XLEAP) project at SLAC has enabled LCLS to produce much shorter X-ray pulses than previously possible, with durations of a few hundred attoseconds. To measure the time-profile of these extremely short pulses a velocity map imaging spectrometer (VMI) was developed. The pulse duration is measured with using an angular streaking method.

Franz, Paris↗

Electronic topological transitions in cadmium under pressure studied via theoretical and experimental x-ray absorption spectroscopy

Here, an electronic topological transition (ETT) in cadmium below 1 GPa is investigated in situ with experimental x-ray absorption spectroscopy and projecting calculated core-valence excitons onto the band structure. These projections are a useful application of the Bethe-Salpeter equation approach that considers many-body effects. The method described herein can be used for systems that are otherwise difficult to probe in situ; therefore, it provides a generalizable approach to identifying and understanding ETTs under high pressure. Although pressure-induced ETTs are often probed using indirect structural responses, our own x-ray diffraction and Raman studies suggest a second-order structural transition around 3 GPa but are largely insensitive to or inconclusive for the previously studied ETT in this region.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Molecular Environmental Science Using Synchrotron Radiation: Chemistry and Physics of Waste Form Materials

Production of defense-related nuclear materials has generated large volumes of complex chemical wastes containing a mixture of radionuclides. The disposition of these wastes requires conversion of the liquid and solid-phase components into durable, solid forms suitable for long-term immobilization. Specially formulated glass compositions and ceramics such as pyrochlores and apatites are the main candidates for these wastes. An important consideration linked to the durability of waste-form materials is the local structure around the waste components. Equally important is the local structure of constituents of the glass and ceramic host matrix. Knowledge of the structure in the waste-form host matrices is essential, prior to and subsequent to waste incorporation, to evaluate and develop improved waste-form compositions based on scientific considerations. This project used the soft-x-ray synchrotron-radiation-based technique of near-edge x-ray-absorption fine structure (NEXAFS) as a unique method for investigating oxidation states and structures of low-Z elemental constituents forming the backbones of glass and ceramic host matrices for waste-form materials. In addition, light metal ions in ceramic hosts, such as titanium, are also ideal for investigation by NEXAFS in the soft-x-ray region. Thus, one of the main objectives was to understand outstanding issues in waste-form science via NEXAFS investigations and to translate this understanding into better waste-form materials, followed by eventual capability to investigate “real” waste-form materials by the same methodology. We conducted several detailed structural investigations of both pyrochlore ceramic and borosilicate-glass materials during the project and developed improved capabilities at Beamline 6.3.1 of the Advanced Light Source (ALS) to perform the studies.

36 MATERIALS SCIENCE↗

X-Ray Emission from "Uranium" Stars

The project aims to secure XMM observations of two targets with extremely low abundances of the majority of heavy elements (e.g., log[Fe/H] $\sim$-4), but that show absorption lines of uranium. The presence of an r-process element such as uranium requires a binary star system in which the companion underwent a supernova explosion. A binary star system raises the distinct possibility of the existence of a compact object, most likely a neutron star, in the binary, assuming it survived the supernova blast. The presence of a compact object then suggests X-ray emission if sufficient matter accretes to the compact object. The observations were completed less than one year ago following a series of reobservations to correct for significant flaring that occurred during the original observations. The ROSAT all-sky survey was used to report on the initial assessment of X-ray emission from these objects; only upper limits were reported. These upper limits were used to justify the XMM observing time, but with the expectation that upper limits would merely be pushed lower. The data analysis hinges critically on the quality and degree of precision with which the background is handled. During the past year, I have spent some time learning the ins and outs of XMM data analysis. In the coming year, I can apply that learning to the analysis of the 'uranium' stars.

Schlegel, Eric↗

A rapid noninvasive characterization of CT x-ray sources

Purpose: The aim of this study is to generate spatially varying half value layers (HVLs) that can be used to construct virtual equivalent source models of computed tomography (CT) x-ray sources for use in Monte Carlo CT dose computations. Methods: To measure the spatially varying HVLs, the authors combined a cylindrical HVL measurement technique with the characterization of bowtie filter relative attenuation (COBRA) geometry. An apparatus given the name “HVL Jig” was fabricated to accurately position a real-time dosimeter off-isocenter while surrounded by concentric cylindrical aluminum filters (CAFs). In this geometry, each projection of the rotating x-ray tube is filtered by an identical amount of high-purity (type 1100 H-14) aluminum while the stationary radiation dose probe records an air kerma rate versus time waveform. The CAFs were progressively nested to acquire exposure data at increasing filtrations to calculate the HVL. Using this dose waveform and known setup geometry, each timestamp was related to its corresponding fan angle. Data were acquired using axial CT protocols (i.e., rotating tube and stationary patient table) at energies of 80, 100, and 120 kVp on a single CT scanner. These measurements were validated against the more laborious conventional step-and-shoot approach (stationary x-ray tube). Results: At each energy, HVL data points from the COBRA-cylinder technique were fit to a trendline and compared with the conventional approach. The average relative difference in HVL between the two techniques was 1.3%. There was a systematic overestimation in HVL due to scatter contamination. Conclusions: The described method is a novel, rapid, accurate, and noninvasive approach that allows one to acquire the spatially varying fluence and HVL data using a single experimental setup in a minimum of three scans. These measurements can be used to characterize the CT beam in terms of the angle-dependent fluence and energy spectra along the bowtie filter direction, which can serve as input for accurate CT dose computations.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

The XMM-BCS galaxy cluster survey: I. The X-ray selected cluster catalog from the initial 6 deg$^2$

The XMM-Newton - Blanco Cosmology Survey project (XMM-BCS) is a coordinated X-ray, optical and mid-infrared cluster survey in a field also covered by Sunyaev-Zel dovich effect (SZE) surveys by the South Pole Telescope and the Atacama Cosmology Telescope. The aim of the project is to study the cluster population in a 14 deg{sup 2} field (center: {alpha} {approx} 23:29:18.4, {delta} {approx} -54:40:33.6). The uniform multi-wavelength coverage will also allow us for the first time to comprehensively compare the selection function of the different cluster detection approaches in a single test field and perform a cross-calibration of cluster scaling relations. In this work, we present a catalog of 46 X-ray selected clusters from the initial 6 deg{sup 2} survey core.We describe the XMM-BCS source detection pipeline and derive physical properties of the clusters. We provide photometric redshift estimates derived from the BCS imaging data and spectroscopic redshift measurements for a low redshift subset of the clusters. The photometric redshift estimates are found to be unbiased and in good agreement with the spectroscopic values. Our multi-wavelength approach gives us a comprehensive look at the cluster and group population up to redshifts z {approx} 1. The median redshift of the sample is 0.47 and the median mass M{sub 500} {approx} 1 x 10{sup 14} M{sub {circle_dot}} ({approx} 2 keV). From the sample, we derive the cluster log N - log S using an approximation to the survey selection function and find it in good agreement with previous studies. We compare optical mass estimates from the Southern Cosmology Survey available for part of our cluster sample with our estimates derived from the X-ray luminosity. Weak lensing masses available for a subset of the cluster sample are in agreement with our estimates. Optical masses based on cluster richness and total optical luminosity are found to be significantly higher than the X-ray values. The present results illustrate the excellent potential of medium-deep, X-ray surveys to deliver cluster samples for cosmological modelling. In combination with available multi-wavelength data in optical, near-infrared and SZE, this will allow us to probe the dependence of the selection functions on relevant cluster observables and provide thus an important input for upcoming large-area multi-wavelength cluster surveys.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Galaxy Cluster Shapes and Systematic Errors in the Hubble Constant as Determined by the Sunyaev-Zel'dovich Effect

Imaging of the Sunyaev-Zei'dovich (S-Z) effect in galaxy clusters combined with the cluster plasma x-ray diagnostics can measure the cosmic distance scale to high accuracy. However, projecting the inverse-Compton scattering and x-ray emission along the cluster line-of-sight will introduce systematic errors in the Hubble constant, H$-O$, because the true shape of the cluster is not known. This effect remains present for clusters that are otherwise chosen to avoid complications for the S-Z and x-ray analysis, such as plasma temperature variations, cluster substructure, or cluster dynamical evolution. In this paper we present a study of the systematic errors in the value of H$-0$, as determined by the x-ray and S-Z properties of a theoretical sample of triaxial isothermal 'beta-model' clusters, caused by projection effects and observer orientation relative to the model clusters' principal axes. The model clusters are not generated as ellipsoids of rotation, but have three independent 'core radii', as well as a random orientation to the plane of the sky.

Sulkanen, Martin E.↗

Development of a broadband hard x-ray radiography platform for pulsed-power experiments

In this article, we develop and demonstrate a broadband hard x-ray radiography platform at the Zebra Pulsed Power Laboratory that integrates point-projection radiography, bremsstrahlung measurements, and hard x-ray pinhole imaging, designed to diagnose current-driven, cylindrically compressed matter. Initial laser-pulsed-power coupled experiments revealed that intense background radiation generated during 1 MA Zebra current shots overwhelmed laser-produced hard x-rays, obscuring radiographic images. Using combined spectral and spatial diagnostics, we identify energetic electrons accelerated by return currents as the dominant source of background hard x-rays, with electron energies inferred to be 3–4 MeV based on Monte Carlo simulations, and demonstrate mitigation through modifications to the radiation shielding and return-current configuration. The diagnostic platform was validated using a wire-pinch hard x-ray source, allowing radiographs of static 1-mm-diameter aluminum wires to be obtained while simultaneously measuring x-ray source spectra and spatial emission distributions within a single shot. Measured wire transmission profiles were quantitatively reconstructed using radiation transport simulations that incorporate an experimentally inferred two-temperature exponential x-ray spectrum from bremsstrahlung signal analysis and spatially distributed emission sources identified by pinhole imaging. Agreement between measured and simulated transmission profiles demonstrates the validity of the radiographic and x-ray source characterization approach, establishing this diagnostic platform as a promising tool for diagnosing magnetically driven, high-density plasmas relevant to warm dense matter and inertial fusion energy research.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Advancing Aviation Security

Air travel is a popular mode of transportation. Each year, more than 600 million people board U.S. flights for business or pleasure. As demonstrated on 9/11, a coordinated terrorist strike on commercial airlines has devastating consequences where many lives could be lost and the nation’s economy could be crippled. The Transportation Security Administration (TSA) has worked diligently to enhance security at airports and on flights so that people and cargo can continue to move freely. Today, all passengers and every piece of checked or carry-on luggage are screened before they are permitted on an aircraft. X-ray systems and walk-through metal detectors allow security personnel to identify dangerous metal objects, such as guns and knives. A more complex problem is the detection of explosives, where detection technologies such as multiple-energy X-ray radiography, computed tomography (CT), full body scanners using millimeter wave and X-ray backscatter and other techniques are used to screen for explosives hidden in luggage, in cargo and on the people boarding the aircraft. Scientists and engineers at the Lawrence Livermore National Laboratory (LLNL) are working with the Department of Homeland Security (DHS), Science and Technology Directorate (S&T), Explosives Division (EXD) to help improve aviation security by evaluating and enhancing the performance of next-generation explosives detection technologies. LLNL is providing subject matter expertise to TSA for their multi-billion dollar procurements of explosive detection system (EDS) for the nation’s airports and provides recommendations for process and system improvements. To further improve aviation security, EXD is funding research at LLNL to develop advanced explosives detection technologies that can more accurately discriminate between a wide range of explosives and non-threat materials. One challenge with scanning for explosives is that some nonthreatening materials share similar characteristics with actual threats, leading to false positives or false alarms. When an alarm is generated, security personnel must review the scan images to clear the alarm or manually open and verify the bag’s contents, which can increase labor costs and lead to passenger delays. The Livermore efforts currently focus on CT-based applications. First developed for the medical field as a method for diagnosing disease, X-ray CT has become instrumental in various industrial Non-Destructive Evaluation (NDE) applications. Explosives detection equipment that incorporates CT uses a broad-spectrum X-ray beam to capture projections of an object, in particular, the objects inside a piece of luggage. The CT system then applies complex reconstruction algorithms to the projections to produce a three-dimensional representation of the luggage and its contents. Automated threat-detection algorithms (also referred to as threat-recognition algorithms) further process the images to separate each item and flag potential threats for further review (see Figure 1). Transportation security officers can then examine these images and the relevant data to determine whether further interrogation is needed. LLNL has also performed research on advanced X-ray carry-on bag inspection systems and is helping to better understand the performance of X-ray backscatter and millimeter wave passenger screening systems.

42 ENGINEERING↗