Results for “CALIBRATION STANDARDS” — Page 45

NASA NTRS1971

Absolute ultraviolet spectrophotometry of: alpha CMa, gamma Ori, kappa Ori, and alpha Leo; and a continuing calibration program and some preliminary results

Spectral observations of the stars alpha CMa, gamma Ori, kappa Ori, and alpha Leo have been obtained in the range 1150 to 4000 Angstroms, using rocket borne spectrometers. The payloads have a 13-inch diameter telescope, a rotatable concave diffraction grating, and three pulse counting photomultiplier photometers. The laboratory standards used as photometric references derive their primary calibration directly or indirectly from the National Bureau of Standards. An error range of up to + or - 10 percent is attributed to these laboratory standards; + or - 8 percent to the calibration procedure; and + or - 10 percent is assigned as an accidental error range.

Evans, D. C.↗

DOE OSTI2015

Development of BATAN’s texture diffractometer (current status)

Texture Diffractometer, called DN2, is one of neutron diffractometers in BATAN which is dedicated for texture measurement using neutron diffraction method. To obtain better performance of the DN2, a flight tube goniometer have been installed between the monochromator and sample position. By adjusting the flight tube goniometer, defocusing effect at direct beam and background effect could be reduced significantly. Some experiments have been carried out to characterize DN2 performance. The flight tube goniometer alignment and neutron wavelength calibration were characterized using silicon standard sample Si640d. Data refinement of diffraction pattern was analyzed using MAUD software and it is obtained reliability factor with background, R{sub wpb}, reduced significantly, from 42.53 % to 19.36 % after setting of flight tube goniometer. Reliability factor without background (R{sub wp}) was reduced from 27.41% to 21.36%. Calibrated of neutron wavelengh, λ = 1,2799 Angstrom is obtained.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

NASA NTRS1988

Electron-Photon Coincidence Calibration Of Photon Detectors

Absolute and relative detector efficiencies measured. Apparatus uses coincidence-counting techniques to measure efficiency of ultraviolet or vacuum ultraviolet detector at very low radiation intensity. Crossed electron and atomic beams generate photons used to calibrate photon detector. Pulses from electron counter and photon detector(s) processed by standard coincidence-counting techniques. Used to calibrate other detectors or make absolute measurements of incident photon fluxes.

Srivastava, Santosh K.↗

DOE OSTI2015

Design and testing of a sensitive heat-flow calorimeter for measuring radioactive waste in 55-gallon (US) drums - 15334

A sensitive large volume calorimeter for measuring the thermal power generated by the radioactive decay of heat producing materials in 55-gallon drums has been developed and tested. The technology is applicable to the measurement of all radionuclides that decay by alpha or beta decay such as waste or product material containing plutonium, tritium and americium. It is also relevant to the measurement of drums where gamma rays from radioactive decay are captured locally in attenuating materials and the resulting rate of thermal energy deposition (sample thermal power) is of sufficient magnitude for a calorimetry measurement. The initial application of the drum calorimeter is for measuring and characterizing plutonium-bearing waste drums. The calorimeter design has optimised the two characteristics of high thermal sensitivity and reduced measurement times. In order to achieve these characteristics for large volume drums, the heat-flow method of operation was chosen in a single measurement chamber configuration. Using a drum-lifting device, the waste drum is positioned on a sliding platform and subsequently moved by the operator inside an octagonal inner chamber, which acts as the heat sink. The heat-sink chamber has significant thermal inertia and remains effectively at a constant temperature throughout the duration of a drum measurement. The octagonal inner measurement chamber is constructed inside a multi-layer external thermal enclosure, which provides both thermal insulation and significant thermal inertia. The external thermal enclosure isolates the measurement process from the effects of changes in the external ambient temperature. During a measurement, heat flows from the drum being measured to the heat sink. This heat-flow is measured by a series of thermopile sensor assemblies, which are positioned between the waste drum and the heat sink. A high sensitivity of greater than 200 μV/mW (microvolts per milliwatt) has been achieved using multiple close-coupled thermopile sensors in each assembly. Reduced measurement times are achieved by positioning the thermopile sensor assemblies close to the drum surface in order to reduce the thermal transport delay. The instrument incorporates a calibrated precision power supply, which requires annual recalibration and is traceable to national standards. It is used to power a calibration heater that has been built into a calibration and test drum. The calibration and test drum is used both to calibrate the instrument and provide periodic confirmation of correct operation. Measurements of calorimeter performance are reported for a range of drum thermal powers. Long-term temperature drift measurements are used to provide estimates of the minimum detectable drum thermal power and hence the minimum detectable activity for both plutonium and tritium. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

NASA NTRS1993

Compositional diversity of the lunar North Pole: Preliminary analyses of Galileo SSI data

In December 1992, the Galileo spacecraft passed through the Earth-Moon system for its final gravity assist to Jupiter. The SSI camera obtained several 6-color mosaics of the lunar north polar region and the sunlit nearside and eastern limb at approximately 1.3 km/pixel. Initial analyses have concentrated on the north polar areas to assess the composition of the crust in that region. Representative 6-color calibration SSI spectra (typically 5 x 5 pixels) are shown. Photometric corrections have not yet been applied, and all spectra are scaled to unity at 0.56 microns. The data were first calibrated relative to MS2, a standard are in Mare Serenitatis (18.7 deg N, 21.5 deg E), and the top four plots of highlands, highland craters, maria, and mare craters are displayed relative to MS2. SSI spectra of areas measured with telescopic data (mare MT1/MS2 and mare crater MSA/MS2) agree well with previous data, confirming that the calibration procedures and SSI data are spectrally accurate. The bottom three plots of craters/sun have been calibrated to reflectance using previously obtained telescopic spectra of Apollo 16/MS2 (shown with Highlands/MS2) and laboratory spectra of mature Apollo 16 soil (shown for reference with the Highland Craters/Sun). Although some variations in these spectra mimic previously observed spectra of lunar terrains, several characteristics are unusual. Familiar and unfamiliar properties are observed in these northern latitudes and both types merit further investigation in their geologic context.

Pieters, C. M.↗

DOE OSTI2016

WE-DE-201-05: Evaluation of a Windowless Extrapolation Chamber Design and Monte Carlo Based Corrections for the Calibration of Ophthalmic Applicators

Purpose: To test the validity of a windowless extrapolation chamber used to measure surface dose rate from planar ophthalmic applicators and to compare different Monte Carlo based codes for deriving correction factors. Methods: Dose rate measurements were performed using a windowless, planar extrapolation chamber with a {sup 90}Sr/{sup 90}Y Tracerlab RA-1 ophthalmic applicator previously calibrated at the National Institute of Standards and Technology (NIST). Capacitance measurements were performed to estimate the initial air gap width between the source face and collecting electrode. Current was measured as a function of air gap, and Bragg-Gray cavity theory was used to calculate the absorbed dose rate to water. To determine correction factors for backscatter, divergence, and attenuation from the Mylar entrance window found in the NIST extrapolation chamber, both EGSnrc Monte Carlo user code and Monte Carlo N-Particle Transport Code (MCNP) were utilized. Simulation results were compared with experimental current readings from the windowless extrapolation chamber as a function of air gap. Additionally, measured dose rate values were compared with the expected result from the NIST source calibration to test the validity of the windowless chamber design. Results: Better agreement was seen between EGSnrc simulated dose results and experimental current readings at very small air gaps (<100 µm) for the windowless extrapolation chamber, while MCNP results demonstrated divergence at these small gap widths. Three separate dose rate measurements were performed with the RA-1 applicator. The average observed difference from the expected result based on the NIST calibration was −1.88% with a statistical standard deviation of 0.39% (k=1). Conclusion: EGSnrc user code will be used during future work to derive correction factors for extrapolation chamber measurements. Additionally, experiment results suggest that an entrance window is not needed in order for an extrapolation chamber to provide accurate dose rate measurements for a planar ophthalmic applicator.

07 ISOTOPE AND RADIATION SOURCES↗

DOE OSTI2022

Solar Radiation Research Laboratory (SRRL) Final Report: Fiscal Years 2019-2021

The Solar Radiation Research Laboratory (SRRL) at the National Renewable Energy Laboratory (NREL) is a world-leading solar calibration and measurement facility and maintains and disseminates the World Radiation Reference (essentially the W/m 2 ) for the United States, which is essential for traceable and accurate measurements of solar radiation at all solar generation facilities. SRRL operates two International Organization for Standardization (ISO)/International Electrotechincal Commission (IEC) 17025 calibration facilities that provide unique, high-quality calibrations to NREL and other U.S. Department of Energy laboratories. The Baseline Measurement System at SRRL provides a high-quality record of solar irradiance and surface meteorological conditions. SRRL capabilities are used to develop: improved methods for the calibration of solar radiometers; new standards through the ISO, the IEC, and ASTM International; models; advanced instrumentation and methods for operating solar measurement stations. The SRRL data sets are also critical for the validation of new models and data sets, such as the National Solar Radiation Database (NSRDB).

14 SOLAR ENERGY↗

DOE OSTI2023

Applications of Alternate Actinide Calibration on Inductively Coupled Plasma Mass Spectrometry (ICPMS) Analysis of H-Canyon Highly Enriched Uranium Legacy Material at the Savannah River Site (SRS)

The Savannah River National Laboratory (SRNL) uses Inductively Coupled Plasma Mass Spectrometry (ICPMS) to support numerous programs at the Savannah River Site (SRS). As part of an objective to prepare high assay low enriched uranium (HALEU), the SRS H-Canyon needed analysis of legacy uranyl nitrate that is stored at its Outside Facilities (HOF). With the application of a standard practice for alternate actinide calibration on ICP-MS, SRNL has successfully demonstrated its capability to characterize the uranium/actinide composition of the HOF tanks that are intended for consolidation prior to preparation of the HALEU. A comparison of the uranium analytical results between recently upgraded SRNL ICP-MS and Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES) instrumentation shows the alternate actinide calibration is a valid complementary method when used in conjunction with other analytical techniques (Davies-Gray Potentiometric Titration). The methods, instrumentation, and ongoing developments on ICP-MS at SRNL will be discussed.

Jones, Mark A.↗

DOE OSTI2016

MO-A-BRC-02: TG167 Report - Detailed Description

Although a multicenter, Phase III, prospective, randomized trial is the gold standard for evidence-based medicine, it is rarely used to evaluate innovative radiotherapy devices because of many practical and ethical reasons. It is usually sufficient to compare the dose distributions and dose rates for determining equivalence of the innovative device to an existing one. Thus, quantitative evaluation of the dosimetric characteristics of an innovative brachytherapy device or application is a critical part in which physicists are actively involved. The physicist’s role, along with physician colleagues, in this process is highlighted for innovative products or applications and includes evaluation of 1) dosimetric considerations for clinical implementation (including calibrations, dose calculations, and radiobiological aspects) to comply with existing societal dosimetric prerequisites for sources in routine clinical use, 2) risks and benefits from regulatory and safety perspectives, and 3) resource assessment and preparedness. Further, calibration methods should be traceable to a primary standards dosimetry laboratory such as NIST in the U.S. or to other primary standards dosimetry laboratory located elsewhere. Clinical users should follow standards as approved by their country’s regulatory agencies that approved such a brachytherapy device. Integration of this system into the medical source calibration infrastructure of secondary standard dosimetry laboratories such as the ADCLs is encouraged before a source is introduced into widespread routine clinical use. The AAPM and GEC-ESTRO have developed guidelines for the safe and consistent application of brachytherapy using innovative brachytherapy devices and applications. The current report covers regulatory approvals, calibration, dose calculations, radiobiological issues, and overall safety concerns that should be addressed during the commissioning stage preceding clinical use. These guidelines are based on review of requirements of the U.S. NRC, FDA, Department of Transportation, International Electrotechnical Commission Medical Electrical Equipment Standard 60601, European Commission for CE Marking, and institutional review boards and radiation safety committees. Learning Objectives: Understand the necessary dosimetric considerations for clinical implementation (including calibrations, dose calculations, and radiobiological aspects) to comply with existing societal dosimetric prerequisites for sources in routine clinical use. Evaluate risks and benefits from regulatory and safety perspectives. Identify necessary resources and create a plan for clinical introduction of innovative brachytherapy device or applications. Consultant for Theragenics Corp.; R. Nath, Consultant to Theragenics Corp.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2016

MO-A-BRC-00: TG167: Clinical Recommendations for Innovative Brachytherapy Devices and Applicators

Although a multicenter, Phase III, prospective, randomized trial is the gold standard for evidence-based medicine, it is rarely used to evaluate innovative radiotherapy devices because of many practical and ethical reasons. It is usually sufficient to compare the dose distributions and dose rates for determining equivalence of the innovative device to an existing one. Thus, quantitative evaluation of the dosimetric characteristics of an innovative brachytherapy device or application is a critical part in which physicists are actively involved. The physicist’s role, along with physician colleagues, in this process is highlighted for innovative products or applications and includes evaluation of 1) dosimetric considerations for clinical implementation (including calibrations, dose calculations, and radiobiological aspects) to comply with existing societal dosimetric prerequisites for sources in routine clinical use, 2) risks and benefits from regulatory and safety perspectives, and 3) resource assessment and preparedness. Further, calibration methods should be traceable to a primary standards dosimetry laboratory such as NIST in the U.S. or to other primary standards dosimetry laboratory located elsewhere. Clinical users should follow standards as approved by their country’s regulatory agencies that approved such a brachytherapy device. Integration of this system into the medical source calibration infrastructure of secondary standard dosimetry laboratories such as the ADCLs is encouraged before a source is introduced into widespread routine clinical use. The AAPM and GEC-ESTRO have developed guidelines for the safe and consistent application of brachytherapy using innovative brachytherapy devices and applications. The current report covers regulatory approvals, calibration, dose calculations, radiobiological issues, and overall safety concerns that should be addressed during the commissioning stage preceding clinical use. These guidelines are based on review of requirements of the U.S. NRC, FDA, Department of Transportation, International Electrotechnical Commission Medical Electrical Equipment Standard 60601, European Commission for CE Marking, and institutional review boards and radiation safety committees. Learning Objectives: Understand the necessary dosimetric considerations for clinical implementation (including calibrations, dose calculations, and radiobiological aspects) to comply with existing societal dosimetric prerequisites for sources in routine clinical use. Evaluate risks and benefits from regulatory and safety perspectives. Identify necessary resources and create a plan for clinical introduction of innovative brachytherapy device or applications. Consultant for Theragenics Corp.; R. Nath, Consultant to Theragenics Corp.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2016

MO-A-BRC-01: TG167 Report - Introduction

Although a multicenter, Phase III, prospective, randomized trial is the gold standard for evidence-based medicine, it is rarely used to evaluate innovative radiotherapy devices because of many practical and ethical reasons. It is usually sufficient to compare the dose distributions and dose rates for determining equivalence of the innovative device to an existing one. Thus, quantitative evaluation of the dosimetric characteristics of an innovative brachytherapy device or application is a critical part in which physicists are actively involved. The physicist’s role, along with physician colleagues, in this process is highlighted for innovative products or applications and includes evaluation of 1) dosimetric considerations for clinical implementation (including calibrations, dose calculations, and radiobiological aspects) to comply with existing societal dosimetric prerequisites for sources in routine clinical use, 2) risks and benefits from regulatory and safety perspectives, and 3) resource assessment and preparedness. Further, calibration methods should be traceable to a primary standards dosimetry laboratory such as NIST in the U.S. or to other primary standards dosimetry laboratory located elsewhere. Clinical users should follow standards as approved by their country’s regulatory agencies that approved such a brachytherapy device. Integration of this system into the medical source calibration infrastructure of secondary standard dosimetry laboratories such as the ADCLs is encouraged before a source is introduced into widespread routine clinical use. The AAPM and GEC-ESTRO have developed guidelines for the safe and consistent application of brachytherapy using innovative brachytherapy devices and applications. The current report covers regulatory approvals, calibration, dose calculations, radiobiological issues, and overall safety concerns that should be addressed during the commissioning stage preceding clinical use. These guidelines are based on review of requirements of the U.S. NRC, FDA, Department of Transportation, International Electrotechnical Commission Medical Electrical Equipment Standard 60601, European Commission for CE Marking, and institutional review boards and radiation safety committees. Learning Objectives: Understand the necessary dosimetric considerations for clinical implementation (including calibrations, dose calculations, and radiobiological aspects) to comply with existing societal dosimetric prerequisites for sources in routine clinical use. Evaluate risks and benefits from regulatory and safety perspectives. Identify necessary resources and create a plan for clinical introduction of innovative brachytherapy device or applications. Consultant for Theragenics Corp.; R. Nath, Consultant to Theragenics Corp.

60 APPLIED LIFE SCIENCES↗

NASA NTRS2001

Aerosol Measurements by the Globally Distributed Micro Pulse Lidar Network

Full time measurements of the vertical distribution of aerosol are now being acquired at a number of globally distributed MP (micro pulse) lidar sites. The MP lidar systems provide full time profiling of all significant cloud and aerosol to the limit of signal attenuation from compact, eye safe instruments. There are currently eight sites in operation and over a dozen planned. At all sited there are also passive aerosol and radiation measurements supporting the lidar data. Four of the installations are at Atmospheric Radiation Measurement program sites. The network operation includes instrument operation and calibration and the processing of aerosol measurements with standard retrievals and data products from the network sites. Data products include optical thickness and extinction cross section profiles. Application of data is to supplement satellite aerosol measurements and to provide a climatology of the height distribution of aerosol. The height distribution of aerosol is important for aerosol transport and the direct scattering and absorption of shortwave radiation in the atmosphere. Current satellite and other data already provide a great amount of information on aerosol distribution, but no passive technique can adequately resolve the height profile of aerosol. The Geoscience Laser Altimeter System (GLAS) is an orbital lidar to be launched in early 2002. GLAS will provide global measurements of the height distribution of aerosol. The MP lidar network will provide ground truth and analysis support for GLAS and other NASA Earth Observing System data. The instruments, sites, calibration procedures and standard data product algorithms for the MPL network will be described.

Spinhirne, James↗

NASA NTRS1977

Vacuum ultraviolet radiometry. III - The argon mini-arc as a new secondary standard of spectral radiance

A miniature argon arc has been designed and tested as a new transfer standard of spectral radiance for the wavelength range from 114 nm to 330 nm. Calibration has been performed using two primary standard sources: the hydrogen arc from 130 nm to 330 nm and the blackbody line radiator from 114 nm to 130 nm. The mini-arc provides an intense, stable, and reproducible UV continuum with dc power requirements of less than 1.5 kW. The arc characteristics have been investigated, and the sensitivity of the radiant power output to various operating parameters has been measured. The rms uncertainty in the spectral radiance is estimated to be 5.3% above 140 nm and 10.1% between 114 nm and 140 nm, due primarily to uncertainties in the primary standard sources.

Bridges, J. M.↗

NASA NTRS1983

The solar absolute spectral irradiance 1150-3173 A - May 17, 1982

The full-disk solar spectral irradiance in the spectral range 1150-3173 A was obtained from a rocket observation above White Sands Missile Range, NM, on May 17, 1982, half way in time between solar maximum and solar minimum. Comparison with measurements made during solar maximum in 1980 indicate a large decrease in the absolute solar irradiance at wavelengths below 1900 A to approximately solar minimum values. No change above 1900 A from solar maximum to this flight was observed to within the errors of the measurements. Irradiance values lower than the Broadfoot results in the 2100-2500 A spectral range are found, but excellent agreement with Broadfoot between 2500 and 3173 A is found. The absolute calibration of the instruments for this flight was accomplished at the National Bureau of Standards Synchrotron Radiation Facility which significantly improves calibration of solar measurements made in this spectral region.

Mount, G. H.↗

DOE OSTI2017

Energy Efficiency and Emissions Intensity Standards

We investigate the role of energy efficiency in rate-based emissions intensity standards, a particularly policy-relevant consideration given that the Environmental Protection Agency's Clean Power Plan allows crediting of electricity savings as a means of complying with state-specific emissions standards. We show that with perfectly inelastic energy services demand, crediting efficiency measures can recover the first-best allocation. However, when demand for energy services exhibits some elasticity, crediting energy efficiency can no longer recover first-best. While crediting removes the relative distortion between energy generation and energy efficiency, it distorts the absolute level of energy services. Building on these results, we derive the conditions determining the second-best intensity standard and crediting rule. Simulations calibrated to the electricity sector in Texas find that while some form of crediting is generally welfare-improving, the proposed one-for-one crediting of energy savings is unlikely to achieve efficient outcomes.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

NASA NTRS2004

Solar Cell Calibration and Measurement Techniques

The increasing complexity of space solar cells and the increasing international markets for both cells and arrays has resulted in workshops jointly sponsored by NASDA, ESA and NASA. These workshops are designed to obtain international agreement on standardized values for the AMO spectrum and constant, recommend laboratory measurement practices and establish a set of protocols for international comparison of laboratory measurements. A working draft of an ISO standard, WD15387, "Requirements for Measurement and Calibration Procedures for Space Solar Cells" was discussed with a focus on the scope of the document, a definition of primary standard cell, and required error analysis for all measurement techniques. Working groups addressed the issues of Air Mass Zero (AMO) solar constant and spectrum, laboratory measurement techniques, and te international round robin methodology. A summary is presented of the current state of each area and the formulation of the ISO document.

Bailey, Sheila↗

DOE OSTI2014

Development of a semi-adiabatic isoperibol solution calorimeter

A semi-adiabatic isoperibol solution calorimeter has been indigenously developed. The measurement system comprises modules for sensitive temperature measurement probe, signal processing, data collection, and joule calibration. The sensitivity of the temperature measurement module was enhanced by using a sensitive thermistor coupled with a lock-in amplifier based signal processor. A microcontroller coordinates the operation and control of these modules. The latter in turn is controlled through personal computer (PC) based custom made software developed with LabView. An innovative summing amplifier concept was used to cancel out the base resistance of the thermistor. The latter was placed in the dewar. The temperature calibration was carried out with a standard platinum resistance (PT100) sensor coupled with an 8½ digit multimeter. The water equivalent of this calorimeter was determined by using electrical calibration with the joule calibrator. The experimentally measured values of the quantum of heat were validated by measuring heats of dissolution of pure KCl (for endotherm) and tris (hydroxyl methyl) amino-methane (for exotherm). The uncertainity in the measurements was found to be within ±3%.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS1985

Historical Cost Curves for Hydrogen Masers and Cesium Beam Frequency and Timing Standards

Historical cost curves were developed for hydrogen masers and cesium beam standards used for frequency and timing calibration in the Deep Space Network. These curves may be used to calculate the cost of future hydrogen masers or cesium beam standards in either future or current dollars. The cesium beam standards are decreasing in cost by about 2.3% per year since 1966, and hydrogen masers are decreasing by about 0.8% per year since 1978 relative to the National Aeronautics and Space Administration inflation index.

Remer, D. S.↗