Search NASA⌕ Search

SEARCH · Search NASA

Results for “POLISHING”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 811 records · Page 45
All sourcesNASA NTRSDOE OSTI
NASA NTRS1989

Fabrication of light-weighted Si/SiC lidar mirrors

Small models of lightweight Si/SiC lidar mirrors have been fabricated via a scalable and cost-effective chemical vapor deposition (CVD) process. These mirrors are about 7.5 cm in diameter and consist of a Si-cladded SiC faceplate and lightweight structure made of SiC. The lightweight structure consists of an outer hexagonal cell with six triangular inner cells. The mirrors were polished to a figure better than 1/5 of a wave and a finish of better than 5A rms. The CVD route to fabrication of mirrors is fast and has the potential to yield several mirrors in a few weeks time from a signel reactor.

Goela, Jitendra S.↗
NASA NTRS1990

Microstructure of a SiC/Ti-15-3 composite

A continuous SiC-fiber-reinforced titanium (Ti-15V-3Cr-3Sn-3A1) composite was metallographically examined. Several methods for examining composite materials were investigated and documented. Polishing techniques for this material are described. An interference layering method was developed to reveal the structure of the fiber, the reaction zone, and various phases within the matrix. Microprobe and TEM analyses were performed on the fiber-matrix interface. Detailed descriptions of the fiber distribution and the microstructure of the fiber and matrix are presented.

Lerch, B. A.↗
NASA NTRS1989

Large scale fabrication of lightweight Si/SiC lidar mirrors

An up-scalable CVD process has been used to fabricate 7.5-cm models of lightweight Si/SiC mirrors consisting of an f/1.6 concave face-plate of SiC coated with CVD Si, in conjunction with a lightweight backup structure of SiC. Due to CVD chamber fabrication, no bonding agent was required to attach the SiC backup structure to the face-plate. Upon up-scaling, the SiC deposition process has been able to produce 40-cm diameter f/1.6 concave mirror face-plates. The mirrors were polished to a 1/5-wave figure and 10 A rms surface finish. There appear to be no intrinsic physical limits to further up-scaling of this mirror-fabrication process.

Goela, Jitendra Singh↗
NASA NTRS1990

Dynamic fatigue of a lithia-alumina-silica glass-ceramic

A dynamic fatigue study was performed on a Li2O-Al2O3-SiO2 glass-ceramic in order to assess its susceptibility to delayed failure. Fracture mechanics techniques were used to analyze the results for the purpose of making lifetime predictions for optical elements made from this material. The material has reasonably good resistance (N = 20) to stress corrosion in ambient conditions. Analysis also indicated the elements should survive applied stresses incurred during grinding and polishing operations.

Tucker, Dennis S.↗
NASA NTRS1989

X-ray/EUV optics for astronomy and microscopy; Proceedings of the Meeting, San Diego, CA, Aug. 7-11, 1989

Topics included in these proceedings are on X-ray/EUV zone plates, filters, and windows; X-ray/EUV microscopes, telescopes, and monochromators; the design, characterization, and test of multilayer optics; the fabrication of X-ray/EUV multilayer optics; and the design, characterization, and test of grazing incidence X-ray optics. Other topics are on the fabrication of grazing incidence X-ray optics, X-ray/EUV space observatories and missions, the test and calibration of X-ray/EUV instruments, X-ray polarimetry, and X-ray/EUV spectroscopy and instruments. Papers are presented on 8-keV X-ray zone plates, a cylindrical X-ray multilayer monochromator, multilayer mirrors for 182 A, advanced flow polishing of exotic optical materials, and optical analysis of grazing incidence ring resonators for free-electron lasers. Attention is also given to X-ray mirrors for the European Synchrotron Radiation Facility, the XUV wide-field camera for Rosat, an optical test and alignment method for the XMM mirror module, Bragg crystal polarimeters, and a liftoff process for multilayer phase gratings.

Hoover, Richard B.↗
NASA NTRS1989

Availability of a library of infrared (2.1-25.0 microns) mineral spectra

All previously published libraries of infrared mineral spectra are in the form of transmitance. Reflectance spectra are, however, more useful for remote sensing and some potential laboratory applications, such as the use of an infrared microscope for mineral identification on polished sections. This note points out that construction of a new library of infrared (2.1-25.0 microns) mineral spectra is in progress. Both transmittance and reflectance measurements of a selection of 63 different, well-characterized minerals have been published to date. These data are available in both hard copy and digital form.

Salisbury, John W.↗
NASA NTRS1991

Fabrication Of Lightweight Mirrors Via CVD

New chemical-vapor deposition (CVD) process developed for fabricating lightweight Si/SiC mirrors. Process involves three CVD steps: to produce faceplate of mirror; to form lightweight back structure deposited integrally with faceplate; and to deposit layer of optical-grade material onto front surface of faceplate. Figure and finish of mirror fabricated into this latter material. Produces dense, highly pure polycrystalline materials polished to surface figures of high precision and finish.

Goela, Jitendra S.↗
NASA NTRS1990

Determination of fiber volume in graphite/epoxy materials using computer image analysis

The fiber volume of graphite/epoxy specimens was determined by analyzing optical images of cross sectioned specimens using image analysis software. Test specimens were mounted and polished using standard metallographic techniques and examined at 1000 times magnification. Fiber volume determined using the optical imaging agreed well with values determined using the standard acid digestion technique. The results were found to agree within 5 percent over a fiber volume range of 45 to 70 percent. The error observed is believed to arise from fiber volume variations within the graphite/epoxy panels themselves. The determination of ply orientation using image analysis techniques is also addressed.

Viens, Michael J.↗
NASA NTRS1990

A quiet flow Ludwieg tube for study of transition in compressible boundary layers: Design and feasibility

Since Ludwieg tubes have been around for many years, and NASA has already established the feasibility of creating quiet-flow wind tunnels, the major question addressed was the cost of the proposed facility. Cost estimates were obtained for major system components, and new designs which allowed fabrication at lower cost were developed. A large fraction of the facility cost comes from the fabrication of the highly polished quiet-flow supersonic nozzle. Methods for the design of this nozzle were studied at length in an attempt to find an effective but less expensive design. Progress was sufficient to show that a quality facility can be fabricated at a reasonable cost.

Schneider, Steven P.↗
NASA NTRS1991

X ray imaging microscope for cancer research

The NASA technology employed during the Stanford MSFC LLNL Rocket X Ray Spectroheliograph flight established that doubly reflecting, normal incidence multilayer optics can be designed, fabricated, and used for high resolution x ray imaging of the Sun. Technology developed as part of the MSFC X Ray Microscope program, showed that high quality, high resolution multilayer x ray imaging microscopes are feasible. Using technology developed at Stanford University and at the DOE Lawrence Livermore National Laboratory (LLNL), Troy W. Barbee, Jr. has fabricated multilayer coatings with near theoretical reflectivities and perfect bandpass matching for a new rocket borne solar observatory, the Multi-Spectral Solar Telescope Array (MSSTA). Advanced Flow Polishing has provided multilayer mirror substrates with sub-angstrom (rms) smoothnesss for the astronomical x ray telescopes and x ray microscopes. The combination of these important technological advancements has paved the way for the development of a Water Window Imaging X Ray Microscope for cancer research.

Hoover, Richard B.↗
NASA NTRS1991

Ion microprobe elemental analyses of impact features on interplanetary dust experiment sensor surfaces

Hypervelocity impact features on several of the electro-active dust sensors utilized in the Interplanetary Dust Experiment (IDE) were subjected to elemental analysis using an ion microprobe. The negatively biased dust sensor surfaces acted as ion traps for cations produced in the plasma plumes of impacting particles. Impactor residue surrounds most impact features to two or three feature diameters. After etching away a layer of carbonaceous/silicaceous surface contamination, low mass resolution elemental survey scans are used to tentatively identify the presence of impactor debris. High mass resolution two-dimensional elemental maps and three dimensional depth profiling of the feature and surrounding area show the distribution and relative composition of the debris. The location of these sensors on the six primary Long Duration Exposure Facility (LDEF) sides provides a unique opportunity to further define the debris environment. Researchers applied the same techniques to impact and contaminant features on a set of ultra-pure, highly polished single crystal germanium wafer witness plates that were mounted on row 12 and exposed to the environment during the entire mission.

Hunter, Jerry L.↗
NASA NTRS1991

Interactions of atomic oxygen with material surfaces in low Earth orbit: Preliminary results from experiment A0114

The University of Alabama at Huntsville atomic oxygen experiment consisted of two trays of 64 one inch diameter solid samples. One tray was placed on the leading edge and one on the trailing edge of the spacecraft. Half of each sample was covered to provide a control. Thus it was intended that the effects of atomic oxygen and solar ultraviolet radiation on the surface properties of each material could be distinguised from each other and from the effects of aging. Sixteen of the samples were placed on a thermally isolated plate of highly polished aluminum, while the main plate was coated with the thermal control coating S13-GLO. Though the experiment was entirely passive, it was hoped that the effects of thermal activation might be observed, if present. The plates were expected to stabilize at temperatures differing by 20 to 30 C. The experiment also carried a device to measure the spacecraft altitude and several oxygen atom reflectometers which have not been analyzed to date. The samples included thin films of metals Os, Ir, Pt, Ni, W, Mo, and Al coated onto fused silica optical flats; metal carbides (WC, SiC), solid carbons of various types, eight polymers and some other coatings of various types.

Gregory, John C.↗
NASA NTRS1991

Patterns of discoloration and oxidation by direct and scattered fluxes, especially oxygen on silicon

A number of interesting discoloration patterns are clearly evident on M0002-1 which resides on three faces of LDEF: front face, rear face, and earth face. Most interesting is the pattern of blue oxidation on polished single crystal silicon apparently produced by once-scattered ram oxygen atoms along the earth face. Most of the other patterns are seen in the Thermal Control Paint. Also, severe oxidation of CR-39 polycarbonate occurred on the front face of LDEF, as expected. A complete explanation for the patterns has not yet been obtained.

Frederickson, A. R.↗
NASA NTRS1989

An investigation of some mechanical and thermal properties of lunar simulant materials heated at 2.45 GHz

Lunar simulant material was fabricated to simulate Apollo 11, Apollo 15, and Apollo 16 soils. The approximate compositions which these soils simulate are given. Samples of each soil simulate were fabricated into right circular cylinders, placed into a microwave reaction cavity, and heated using 2.45 GHz radiation to a particular processing temperature at which it was held for a prescribed length of time. Examples are given of two microwave heating programs for these simulant samples. Upon completion of thermal processing, each sample had its top and bottom surfaces polished. A technique was employed which looks at hardness data to determine the fracture toughness of a material and then relates this to thermal shock resistance. Some advantages of this technique are its low cost for analysis and thermal shock resistance as a function of initial sample orientation in the microwave field can be determined. Samples were prepared for testing and results are expected. At the same time, other samples are currently being investigated using scanning electron microscopy to determine their microstructures.

Meek, T. T.↗
NASA NTRS1991

A fundamental study of nucleate pool boiling under microgravity

An experimental study of incipient boiling in short-term microgravity and with a/g = +/- 1 for pool boiling was performed. Calibrated thin gold films sputtered on a smoothly polished quartz surface were used simultaneously for thermal resistance measurements and heating of the boiling surface. The gold films were used for both transient and quasi-steady heating surface temperature measurements. Two test vessels were constructed for precise measurement and control of fluid temperature and pressure: a laboratory pool boiling vessel for the a/g = +/- experiments and a pool boiling vessel designed for the 131 m free-fall in the NASA Lewis Research Center Microgravity Research Facility for the microgravity tests. Measurements included the heater surface temperature, the pressure near the heating surface, and the bulk liquid temperatures. High speed photography was used in the experiments. With high quality microgravity and the measured initial temperature of the quiescent test fluid, R113, the temperature distribution in the liquid at the moment of boiling inception resulting from an imposed step in heat flux is known with a certainty not possible previously. The types of boiling propagation across the large flat heating surface are categorized; the conditions necessary for their occurrence are described. Explosive boiling propagation with a striking pattern of small scale protuberances over the entire vapor mass periphery not observed previously at low heat flux levels is described. For the heater surface with a/g = -1, a step in the heater surface temperature of short duration was imposed. The resulting liquid temperature distribution at the moment of boiling inception was different from that obtained with a step in heat flux.

Ervin, Jamie S.↗
NASA NTRS1990

In situ measurement of interstellar silicon carbide in two CM chondrite meteorites

The first in situ observations of isotopically anomalous SiC are reported. The grains were found by X-ray mapping of polished sections of two chondritic meteorites, Cold Bokkeveld and Murchison. Ion microprobe measurements showed C-13 enrichments, delta C-13, from 199 to 2800 per mil, proving that the grains are indigenous. SiC grains are revealed only as isolated matrix particles, ruling out the possibility that SiC grains were brought into the solar system as inclusions in larger grains, which protected them from destruction in the solar nebula. Several of the SiC grains are cracked, suggesting that the etching treatment may result in size distributions biased toward smaller grains.

Alexander, C. M. O'D.↗
NASA NTRS1990

Measurement of birefringence of optical materials using a wedged plate interferometer

A nondestructive technique for measuring the birefringence of optical materials such as calcite using wedged plate interferometer is presented. The sample needed for measuring the refractive index must be polished in the form of a parallel plate. The method is based on the measurement of the longitudinal displacement of the focus when the parallel plate is inserted in a converging beam of light. The displacement of the focus is a measure of the refractive index of the optical material. In the case of a uniaxial crystal, the displacement of the focus for the extraordinary ray is different from the displacement of the focus for the ordinary ray. Hence the birefringence of the crystal is determined by measuring the difference between the two focii. It is possible to obtain an accuracy up to 0.0002 in the measurement of birefringence depending on the sample thickness. The method should find its application for the characterization of new crystals in various material research and crystal growth laboratories.

Shukla, R. P.↗
NASA NTRS1991

Interfacial reaction kinetics of coated SiC fibers with various titanium alloys

The kinetics of the reaction between the silicon carbide fibers and the titanium-based alloy matrix was investigated at temperatures from 800 to 1000 C for several titanium-based alloys (including Ti-1100 alloy and BETA 21S) and unalloyed Ti, reinforced with coated silicon carbide fiber SCS-6. The reaction zone growth kinetics was studied by exposing vacuum encapsulated samples to temperatures from 700 to 1000 C for times up to 150 hrs, followed by SAM observations of samples which were polished perpendicular to the fiber axis and etched. It was found that the reaction zone growth kinetics of the alpha (hcp) and beta (bcc) phases of unalloyed titanium reacting with SCS-6 fibers exhibited different values of the apparent activation energy and of the preexponential factor. Additions of other metals to Ti was found to slow down the reaction kinetics. Among the alloys studied, the Ti-1100 was the slowest reacting conventional alloy and the Ti-14Al-21Nb (in wt pct) was the slowest overall.

Gundel, D. B.↗