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At least 811 records · Page 45
All sourcesNASA NTRSDOE OSTI
NASA NTRS1987

Nondestructive evaluation of structural ceramics

A review is presented on research and development of techniques for nondestructive evaluation and characterization of advanced ceramics for heat engine applications. Highlighted in this review are Lewis Research Center efforts in microfocus radiography, scanning laser acoustic microscopy (SLAM), scanning acoustic microscopy (SAM), scanning electron acoustic microscopy (SEAM), and photoacoustic microscopy (PAM). The techniques were evaluated by applying them to research samples of green and sintered silicon nitride and silicon carbide in the form of modulus-of-rupture bars containing seeded voids. Probabilities of detection of voids were determined for diameters as small as 20 microns for microfucus radiography, SLAM, and SAM. Strengths and limitations of the techniques for ceramic applications are identified. Application of ultrasonics for characterizing ceramic microstructures is also discussed.

Klima, Stanley J.↗
NASA NTRS1987

Creep behavior of niobium alloy PWC-11

The high vacuum creep and creep-rupture behavior of a Nb-1Zr-.1C alloy (PWC 11) was investigated at 1350 and 1400 K with an applied stress of 40 MPa. The material was tested in the following four conditions: annealed (1 hr 1755 K/2 hr 1475 K); annealed plus EB welded; annealed plus aged for 1000 hr at 1350 or 1400 K; and annealed, welded, and aged. It was found that the material in the annealed state was the most creep-resistant condition tested, and that aging the alloy for 1000 hr without an applied stress greatly reduced that strength; however, it was still approximately three times as creep resistant as Nb-1Zr. Additionally, the EB weld region was stronger than the base metal in each condition tested, and phase extraction of the dispersed precipitate revealed the presence of a 70%ZrC-30%NbC cubic monocarbide phase.

Titran, R. H.↗
NASA NTRS1986

The hydrogen coverage of interstellar PAHs

The rate at which the CH bond in interstellar Polycyclic Aromatic Hydrocarbons (PAHs) rupture due to the absorption of a UV photon has been calculated. The results show that small PAHs (less than or equal to 25 carbon atoms) are expected to be partially dehydrogenated in regions with intense UV fields, while large PAHs (greater than or equal to 25 atoms) are expected to be completely hydrogenated in those regions. Because estimate of the carbon content of interstellar PAHs lie in the range of 20 to 25 carbon atoms, dehydrogenation is probably not very important. Because of the absence of other emission features besides the 11.3 micrometer feature in ground-based 8 to 13 micrometer spectra, it has been suggested that interstellar PAHs are partially dehydrogenated. However, IRAS 8 to 22 micrometer spectra of most sources that show strong 7.7 and 11.2 micrometer emission features also show a plateau of emission extending from about 11.3 to 14 micrometer. Like the 11.3 micrometer feature, this new feature is attributed to the CH out of plane bending mode in PAHs. This new feature shows that interstellar PAHs are not as dehydrogenated as estimated from ground-based 8 to 13 micrometer spectra. It also constrains the molecular structure of interstellar PAHs. In particular, it seems that very condensed PAHs, such as coronene and circumcoronene, dominate the interstellar PAH mixture as expected from stability arguments.

Barker, J. R.↗
NASA NTRS1987

Experimental evidence for non-proportional growth of large craters

Evidence from laboratory impact experiments is indicating that increasing crater aspect ratios (diameter:depth) can result from increasing both velocity and projectile size without invoking unusual impactor conditions. An extensive data base of experimental impact cratering was analyzed for a variety of impactors and impact velocities for low strength targets. These data indicate a change in cratering efficiency that appears to be related to the onset of projectile deformation or rupture. When all projectile types and sizes are considered, one finds two contrasting relationships between crater aspect ratio and impactor parameter. These relationships are briefly considered.

Schultz, Peter H.↗
NASA NTRS1987

Application of scanning acoustic microscopy to advanced structural ceramics

A review is presentod of research investigations of several acoustic microscopy techniques for application to structural ceramics for advanced heat engines. Results obtained with scanning acoustic microscopy (SAM), scanning laser acoustic microscopy (SLAM), scanning electron acoustic microscopy (SEAM), and photoacoustic microscopy (PAM) are compared. The techniques were evaluated on research samples of green and sintered monolithic silicon nitrides and silicon carbides in the form of modulus-of-rupture bars containing deliberately introduced flaws. Strengths and limitations of the techniques are described with emphasis on statistics of detectability of flaws that constitute potential fracture origins.

Vary, Alex↗
NASA NTRS1986

Fiber-reinforced superalloy composites provide an added performance edge

Fiber reinforcements are being explored as a means to increasing the performance of superalloys past 980 C. Fiber-reinforced superalloys (FRS), particularly tungsten FRS (TFRS) are candidate materials for rocket-engine turbopump blades for advanced Shuttle engines and in airbreathing and other rocket engines. Refractory metal wires are the reinforcement of choice due to tolerance to fiber/matrix interactions. W alloy fibers have a maximum tensile strength of 2165 MPa at 1095 C and a 100 hr creep rupture strength at stresses up to 1400 MPa. A TFRS has the potential of a service temperature 110 C over the strongest superalloy. Manufacturing processes being evaluated to realize the FRS components are summarized, together with design features which will be introduced in turbine blades to take advantage of the FRS materials and to extend their surface life.

Petrasek, D. W.↗
NASA NTRS1986

SCARE - A postprocessor program to MSC/NASTRAN for reliability analysis of structural ceramic components

A computer program was developed for calculating the statistical fast fracture reliability and failure probability of ceramic components. The program includes the two-parameter Weibull material fracture strength distribution model, using the principle of independent action for polyaxial stress states and Batdorf's shear-sensitive as well as shear-insensitive crack theories, all for volume distributed flaws in macroscopically isotropic solids. Both penny-shaped cracks and Griffith cracks are included in the Batdorf shear-sensitive crack response calculations, using Griffith's maximum tensile stress or critical coplanar strain energy release rate criteria to predict mixed mode fracture. Weibull material parameters can also be calculated from modulus of rupture bar tests, using the least squares method with known specimen geometry and fracture data. The reliability prediction analysis uses MSC/NASTRAN stress, temperature and volume output, obtained from the use of three-dimensional, quadratic, isoparametric, or axisymmetric finite elements. The statistical fast fracture theories employed, along with selected input and output formats and options, are summarized. An example problem to demonstrate various features of the program is included.

Gyekenyesi, J. P.↗
NASA NTRS1986

Grain boundary oxidation and fatigue crack growth at elevated temperatures

Fatigue crack growth rate at elevated temperatures can be accelerated by grain boundary oxidation. Grain boundary oxidation kinetics and the statistical distribution of grain boundary oxide penetration depth were studied. At a constant delta K-level and at a constant test temperature, fatigue crack growth rate, da/dN, is a function of cyclic frequency, nu. A fatigue crack growth model of intermittent micro-ruptures of grain boundary oxide is constructed. The model is consistent with the experimental observations that, in the low frequency region, da/dN is inversely proportional to nu, and fatigue crack growth is intergranular.

Liu, H. W.↗
NASA NTRS1986

Preparation of silicon carbide-silicon nitride fibers by the pyrolysis of polycarbosilazane precursors - A review

The development of silicon carbide-silicon nitride fibers (SiC-Si3N4) by the pyrolysis of polycarbosilazane precursors is reviewed. Precursor resin, which was prepared by heating tris(N-methylamino)methylsilane or tris(N-methylamino)phenylsilane to about 520 C, was drawn into fibers from the melt and then made unmeltable by humidity conditioning at 100 C and 95 percent relative humidity. The humidity treated precursor fibers were pyrolyzed to ceramic fibers with good mechanical properties and electrical resistivity. For example, SiC-Si3N4 fibers derived from tris(N-methylamino)methylsilane had a tensile rupture modulus of 29 million psi and electrical resistivity of 6.9 x ten to the 8th power omega-cm, which is ten to the twelfth power times greater than that obtained for graphite fibers.

Penn, B. G.↗
NASA NTRS1987

Starvation effects on the hydrodynamic lubrication of rigid nonconformal contacts in combined rolling and normal motion

The effect of inlet starvation on the hydrodynamic lubrication of lightly loaded rigid nonconformal contacts in combined rolling and normal motion is determined through a numerical solution of the Reynolds' equation for an isoviscous, incompressible lubricant. Starvation is effected by systematically reducing the fluid inlet level. The pressures are taken to be ambient at the inlet meniscus boundary and Reynolds' boundary condition is applied for film rupture in the exit region. Results are presented for the dynamic performance of the starved contacts in combined rolling and normal motion for both normal approach and separation. During normal approach the dynamic load ratio (i.e. ratio of dynamic to steady state load capacity) increases considerably with increase in the inlet starvation. The effect of starvation on the dynamic peak pressure ratio is relatively small. Further, it has been observed that with increasing starvation, film thickness effects become significant in the dynamic behavior of the nonconformal contacts. For significantly starved contacts the dynamic load ratio increases with increase in film thickness during normal approach and a similar reduction is observed during separation. A similar effect is noted for the dynamic peak pressure ratio.

Ghosh, M. K.↗
NASA NTRS1986

Understanding single-crystal superalloys

The unique properties of single crystals are considered. The anisotropic properties of single crystals, and the relation between crystal orientation and the fatigue life and slip systems of the crystals are examined. The effect of raft formation on the creep-rupture life of the crystals is studied. Proposed research on the properties of and new applications for single crystals is discussed.

Dreshfield, Robert L.↗
NASA NTRS1987

The hydrogen coverage of interstellar PAHs

The rate at which the CH bond in interstellar Polycyclic Aromatic Hydrocarbons (PAHs) rupture due to the absorption of a UV photon has been calculated. The results show that small PAHs (less than or equal to 25 carbon atoms) are expected to be partially dehydrogenated in regions with intense UV fields, while large PAHs (greater than or equal to 25 atoms) are expected to be completely hydrogenated in those regions. Because estimate of the carbon content of interstellar PAHs lie in the range of 20 to 25 carbon atoms, dehydrogenation is probably not very important. Because of the absence of other emission features besides the 11.3 micrometer feature in ground-based 8 to 13 micrometer spectra, it has been suggested that interstellar PAHs are partially dehydrogenated. However, IRAS 8 to 22 micrometer spectra of most sources that show strong 7.7 and 11.2 micrometer emission features also show a plateau of emission extending from about 11.3 to 14 micrometer. Like the 11.3 micrometer feature, this new feature is attributed to the CH out of plane bending mode in PAHs. This new feature shows that interstellar PAHs are not as dehydrogenated as estimated from ground-based 8 to 13 micrometer spectra. It also constrains the molecular structure of interstellar PAHs. In particular, it seems that very condensed PAHs, such as coronene and circumcoronene, dominate the interstellar PAH mixture as expected from stability arguments.

Tielens, A. G. G. M.↗
NASA NTRS1987

NDE reliability and process control for structural ceramics

The reliability of microfocus X-radiography and scanning laser acoustic microscopy for detecting microvoids in silicon nitride and silicon carbide was statistically evaluated. Materials- and process-related parameters that influenced the statistical findings in research samples are discussed. The use of conventional X-radiography in controlling and optimizing the processing and sintering of an Si3N4-SiO2-Y2O3 composition designated NASA 6Y is described. Radiographic evaluation and guidance helped develop uniform high-density Si3N4 modulus-of-rupture bars with improved four-point flexural strength (857, 544, and 462 MPa at room temperature, 1200 C, and 1370 C, respectively) and reduced strength scatter.

Baaklini, G. Y.↗
NASA NTRS1987

Surface flaw reliability analysis of ceramic components with the SCARE finite element postprocessor program

The SCARE (Structural Ceramics Analysis and Reliability Evaluation) computer program on statistical fast fracture reliability analysis with quadratic elements for volume distributed imperfections is enhanced to include the use of linear finite elements and the capability of designing against concurrent surface flaw induced ceramic component failure. The SCARE code is presently coupled as a postprocessor to the MSC/NASTRAN general purpose, finite element analysis program. The improved version now includes the Weibull and Batdorf statistical failure theories for both surface and volume flaw based reliability analysis. The program uses the two-parameter Weibull fracture strength cumulative failure probability distribution model with the principle of independent action for poly-axial stress states, and Batdorf's shear-sensitive as well as shear-insensitive statistical theories. The shear-sensitive surface crack configurations include the Griffith crack and Griffith notch geometries, using the total critical coplanar strain energy release rate criterion to predict mixed-mode fracture. Weibull material parameters based on both surface and volume flaw induced fracture can also be calculated from modulus of rupture bar tests, using the least squares method with known specimen geometry and grouped fracture data. The statistical fast fracture theories for surface flaw induced failure, along with selected input and output formats and options, are summarized. An example problem to demonstrate various features of the program is included.

Gyekenyesi, J. P.↗
NASA NTRS1987

Defects in nickel-base superalloys

The presence of substantial amounts of the sigma phase in Ni-base superalloys can drastically reduce the alloy's stress rupture life. No predictive system exists which is entirely successful in anticipating the formation of sigma, mu, and similar phases in new and substantially different alloys. Freckles are defects due to the segregation of elements in quantities that can lead to phase precipitation, and are caused by gravity-driven fluid motion that yields microsegregation in the ingots typically used in the fabrication of structures based on these alloys. Also noted are the effects of porosity and grain boundaries on superalloy mechanical properties.

Dreshfield, Robert L.↗
NASA NTRS1984

Cellular interface morphologies in directional solidification. II - The effect of grain boundaries

A singular perturbation analysis valid for small grain-boundary slopes is used with the one-sided model for solidification to show that grain boundaries introduce imperfections into the symmetry of the developing cellular interfaces which rupture the junction between the family of planar shapes and the bifurcating cellular families. Undulating interfaces are shown to develop first near grain boundaries, and to evolve with decreasing temperature gradient either by a smooth transition from the almost planar family or by a sudden jump to moderate-amplitude cellular forms, depending on the growth rate.

Ungar, Lyle H.↗
NASA NTRS1987

The friction and wear of TPS fibers

The sliding friction behavior of single filaments of SiO2, SiC, and an aluminoborosilicate has been determined. These fibers are used in thermal protection systems (TPS) and are subject to damage during weaving and aero-maneuvering. All fibers exhibited stick-slip friction indicating the successive formation and rupture of strong junctions between the contacting filaments. The static frictional resistance of the sized SiC filament was 4X greater than for the same filament after heat cleaning. This result suggests that the sizing is an organic polymer with a high shear yield strength. Heat cleaning exposes the SiC surface and/or leaves an inorganic residue so that the adhesional contact between filaments has a low fracture energy and frictional sliding occurs by brittle fracture. The frictional resistances of the sized and heat cleaned SiO2 and glass filaments were all comparable to that of the heat cleaned SiC. It would appear that the sizings as well as the heat cleaned surfaces of the silica and glass have low fracture energies so that the sliding resistance is determined by brittle fracture.

Bascom, W. D.↗
NASA NTRS1987

Transform fault earthquakes in the North Atlantic: Source mechanisms and depth of faulting

The centroid depths and source mechanisms of 12 large earthquakes on transform faults of the northern Mid-Atlantic Ridge were determined from an inversion of long-period body waveforms. The earthquakes occurred on the Gibbs, Oceanographer, Hayes, Kane, 15 deg 20 min, and Vema transforms. The depth extent of faulting during each earthquake was estimated from the centroid depth and the fault width. The source mechanisms for all events in this study display the strike slip motion expected for transform fault earthquakes; slip vector azimuths agree to 2 to 3 deg of the local strike of the zone of active faulting. The only anomalies in mechanism were for two earthquakes near the western end of the Vema transform which occurred on significantly nonvertical fault planes. Secondary faulting, occurring either precursory to or near the end of the main episode of strike-slip rupture, was observed for 5 of the 12 earthquakes. For three events the secondary faulting was characterized by reverse motion on fault planes striking oblique to the trend of the transform. In all three cases, the site of secondary reverse faulting is near a compression jog in the current trace of the active transform fault zone. No evidence was found to support the conclusions of Engeln, Wiens, and Stein that oceanic transform faults in general are either hotter than expected from current thermal models or weaker than normal oceanic lithosphere.

Bergman, Eric A.↗