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STARDUST and Interplanetary Dust Particles - Big Science from Small Samples

Comets are primitive bodies that are widely believed to be a reservoir of preserved interstellar and circumstellar grains, and molecular cloud materials (organics). Direct samples of cometary dust along with interstellar grains will be returned by the STARDUST Mission in 2006. Analyses of interplanetary dust particles (IDPs) and analogue materials in the laboratory provide constraints and serve as "ground truth" for evaluating various hypotheses on the nature of comets and interstellar grains. Anhydrous IDPs are the most primitive remnants of the primordial Solar System, and are our only known samples of comets. These cometary lDPs are rich in preserved interstellar organic compounds II]. In addition, abundant interstellar silicates have recently been discovered in cluster lDPs [2]. In some of these IDPs, the presolar silicate abundance reaches 1 wt %, exceeding the total presolar grain abundance in meteorites by three orders of magnitude, where presolar silicates are still notably absent. The results to date support the idea that comets are rich in presolar materials, but are at odds with the common perception that they are 'pristine aggregates of interstellar grains'. These results underscore the scientific importance of sample return missions to comets. The technology for the analysis of micrometer-sized samples is well advanced. The newest generation of ion probe instruments allow for isotopic analyses at the submicrometer level. The nature of the organic matter is analyzed using Infrared and soft X-ray spectroscopy techniques on synchrotron-based instruments, also at the micrometer-scale and smaller. Electron microscopy and spectroscopy provide details on the mineralogy and chemistry of constituent grains in !DPs at nearly the atomic scale. Novel sample preparation techniques have been developed such that all of these measurements can now be made on the same 10 micrometer diameter particle. Returned comet samples captured in aerogel will pose new challenges in sample analysis, but should provide a major leap in our understanding of the fundamental building blocks of our Solar System.

Keller, L. P.↗

Tool for Sampling Permafrost on a Remote Planet

A report discusses the robotic arm tool for rapidly acquiring permafrost (RATRAP), which is being developed for acquiring samples of permafrost on Mars or another remote planet and immediately delivering the samples to adjacent instruments for analysis. The prototype RATRAP includes a rasp that protrudes through a hole in the bottom of a container that is placed in contact with the permafrost surface. Moving at high speed, the rasp cuts into the surface and loads many of the resulting small particles of permafrost through the hole into the container. The prototype RATRAP has been shown to be capable of acquiring many grams of permafrost simulants in times of the order of seconds. In contrast, a current permafrost sampling system that the RATRAP is intended to supplant works by scraping with tines followed by picking up the scrapings in a scoop, sometimes taking hours to acquire a few grams. Also, because the RATRAP inherently pulverizes the sampled material, it is an attractive alternative to other sampling apparatuses that generate core or chunk samples that must be further processed by a crushing apparatus to make the sample particles small enough for analysis by some instruments.

Peters, Gregory↗

Emperical Tests of Acceptance Sampling Plans

Acceptance sampling is a quality control procedure applied as an alternative to 100% inspection. A random sample of items is drawn from a lot to determine the fraction of items which have a required quality characteristic. Both the number of items to be inspected and the criterion for determining conformance of the lot to the requirement are given by an appropriate sampling plan with specified risks of Type I and Type II sampling errors. In this paper, we present the results of empirical tests of the accuracy of selected sampling plans reported in the literature. These plans are for measureable quality characteristics which are known have either binomial, exponential, normal, gamma, Weibull, inverse Gaussian, or Poisson distributions. In the main, results support the accepted wisdom that variables acceptance plans are superior to attributes (binomial) acceptance plans, in the sense that these provide comparable protection against risks at reduced sampling cost. For the Gaussian and Weibull plans, however, there are ranges of the shape parameters for which the required sample sizes are in fact larger than the corresponding attributes plans, dramatically so for instances of large skew. Tests further confirm that the published inverse-Gaussian (IG) plan is flawed, as reported by White and Johnson (2011).

White, K. Preston, Jr.↗

Status of Sample Return Propulsion Technology Development Under NASA's ISPT Program

The In-Space Propulsion Technology (ISPT) program was tasked in 2009 to start development of propulsion technologies that would enable future sample return missions. ISPT s sample return technology development areas are diverse. Sample Return Propulsion (SRP) addresses electric propulsion for sample return and low cost Discovery-class missions, propulsion systems for Earth Return Vehicles (ERV) including transfer stages to the destination, and low technology readiness level (TRL) advanced propulsion technologies. The SRP effort continues work on HIVHAC thruster development to transition into developing a Hall-effect propulsion system for sample return (ERV and transfer stages) and low-cost missions. Previous work on the lightweight propellant-tanks continues for sample return with direct applicability to a Mars Sample Return (MSR) mission with general applicability to all future planetary spacecraft. The Earth Entry Vehicle (EEV) work focuses on building a fundamental base of multi-mission technologies for Earth Entry Vehicles (MMEEV). The main focus of the Planetary Ascent Vehicles (PAV) area is technology development for the Mars Ascent Vehicle (MAV), which builds upon and leverages the past MAV analysis and technology developments from the Mars Technology Program (MTP) and previous MSR studies

Anderson, David J.↗

Satellite Sampling and Retrieval Errors in Regional Monthly Rain Estimates from TMI AMSR-E, SSM/I, AMSU-B and the TRMM PR

Passive and active microwave rain sensors onboard earth-orbiting satellites estimate monthly rainfall from the instantaneous rain statistics collected during satellite overpasses. It is well known that climate-scale rain estimates from meteorological satellites incur sampling errors resulting from the process of discrete temporal sampling and statistical averaging. Sampling and retrieval errors ultimately become entangled in the estimation of the mean monthly rain rate. The sampling component of the error budget effectively introduces statistical noise into climate-scale rain estimates that obscure the error component associated with the instantaneous rain retrieval. Estimating the accuracy of the retrievals on monthly scales therefore necessitates a decomposition of the total error budget into sampling and retrieval error quantities. This paper presents results from a statistical evaluation of the sampling and retrieval errors for five different space-borne rain sensors on board nine orbiting satellites. Using an error decomposition methodology developed by one of the authors, sampling and retrieval errors were estimated at 0.25 resolution within 150 km of ground-based weather radars located at Kwajalein, Marshall Islands and Melbourne, Florida. Error and bias statistics were calculated according to the land, ocean and coast classifications of the surface terrain mask developed for the Goddard Profiling (GPROF) rain algorithm. Variations in the comparative error statistics are attributed to various factors related to differences in the swath geometry of each rain sensor, the orbital and instrument characteristics of the satellite and the regional climatology. The most significant result from this study found that each of the satellites incurred negative longterm oceanic retrieval biases of 10 to 30%.

Fisher, Brad↗

Abundances of Volatile - Bearing Species from Evolved Gas Analysis of Samples from the Rocknest Aeolian Bedform in Gale Crater

The Sample Analysis at Mars (SAM) instrument suite on board the Mars Science Laboratory (MSL) recently ran four samples from an aeolian bedform named Rocknest. SAM detected the evolution of H2O, CO2, O2, and SO2, indicative of the presence of multiple volatile bearing species (Fig 1). The Rocknest bedform is a windblown deposit selected as representative of both the windblown material in Gale crater as well as the globally-distributed martian dust. Four samples of Rocknest material were analyzed by SAM, all from the fifth scoop taken at this location. The material delivered to SAM passed through a 150 m sieve and is assumed to have been well mixed during the sample acquisition/preparation/handoff process. SAM heated the Rocknest samples to approx.835 C at a ramp rate of 35 C/min with a He carrier gas flow rate of apprx.1.5 standard cubic centimeters per minute and at an oven pressure of ~30 mbar [1]. Evolved gases were detected by a quadrupole mass spectrometer (QMS). This abstract presents the molar abundances of H2O, CO2, O2, and SO2 as well as their concentration in rocknest samples using an estimated sample mass.

Archer, P. D., Jr.↗

Examining the Role of Environment in a Comprehensive Sample of Compact Groups

Compact groups, with their high number densities, small velocity dispersions, and an interstellar medium that has not been fully processed, provide a local analog to conditions of galaxy interactions in the earlier universe. The frequent and prolonged gravitational encounters that occur in compact groups affect the evolution of the constituent galaxies in a myriad of ways, for example, gas processing and star formation. Recently, a statistically significant "gap" has been discovered in the mid-infrared (MIR: 3.6-8 μm) IRAC color space of compact group galaxies. This gap is not seen in field samples and is a new example of how the compact group environment may affect the evolution of member galaxies. In order to investigate the origin and nature of this gap, we have compiled a larger sample of 37 compact groups in addition to the original 12 groups studied by Johnson et al. (yielding 174 individual galaxies with reliable MIR photometry). We find that a statistically significant deficit of galaxies in this gap region of IRAC color space is persistent in the full sample, lending support to the hypothesis that the compact group environment inhibits moderate specific star formation rates. Using this expanded sample, we have more fully characterized the distribution of galaxies in this color space and quantified the low-density region more fully with respect to MIR bluer and MIR redder colors. We note a curvature in the color-space distribution, which is fully consistent with increasing dust temperature as the activity in a galaxy increases. This full sample of 49 compact groups allows us to subdivide the data according to physical properties of the groups. An analysis of these subsamples indicates that neither projected physical diameter nor density shows a trend in color space within the values represented by this sample. We hypothesize that the apparent lack of a trend is due to the relatively small range of properties in this sample, whose groups have already been pre-selected to be compact and dense. Thus, the relative influence of stochastic effects (such as the particular distribution and amount of star formation in individual galaxies) becomes dominant. We analyze spectral energy distributions of member galaxies as a function of their location in color space and find that galaxies in different regions of MIR color space contain dust with varying temperatures and/or polycyclic aromatic hydrocarbon emission.

Environment↗

Search for Fluid Inclusions in a Carbonaceous Chondrite Using a New X-Ray Micro-Tomography Technique Combined with FIB Sampling

Early solar system aqueous fluids are preserved in some H chondrites as aqueous fluid inclusions in halite (e.g., [1]). Although potential fluid inclusions are also expected in carbonaceous chondrites [2], they have not been surely confirmed. In order to search for these fluid inclusions, we have developped a new X-ray micro-tomography technique combined with FIB sampling and applied this techniqu to a carbanaceous chondrite. Experimental: A polished thin section of Sutter's Mill meteorite (CM) was observed with an optical microscope and FE-SEM (JEOL 7001F) for chosing mineral grains of carbonates (mainly calcite) and sulfides (FeS and ZnS) 20-50 microns in typical size, which may have aqueous fluid inclusions. Then, a "house" similar to a cube with a roof (20-30 microns in size) is sampled from the mineral grain by using FIB (FEI Quanta 200 3DS). Then, the house was atached to a thin W-needle by FIB and imaged by a SR-based imaging microtomography system with a Fresnel zone plate at beamline BL47XU, SPring-8, Japan. One sample was imaged at two X-ray energies, 7 and 8 keV, to identify mineral phases (dual-enegy microtomography: [3]). The size of voxel (pixel in 3D) was 50-80 nm, which gave the effective spatial resolution of approx. 200 nm. A terrestrial quartz sample with an aqueous fluid inclusion with a bubble was also examined as a test sample by the same method. Results and discussion: A fluid inclusion of 5-8 microns in quartz was clearly identified in a CT image. A bubble of approx. 4 microns was also identified as refraction contrast although the X-ray absorption difference between fluid and bubble is small. Volumes of the fluid and bubble were obtained from the 3D CT images. Fourteen grains of calcite, two grains of iron sulfide and one grain of (Zn,Fe)S were examined. Ten calcite, one iron sulfide and one (Zn,Fe)S grains have inclusions >1 micron in size (the maximum: approx. 5 microns). The shapes are spherical or irregular. Tiny inclusions (<1 micron) are also present in all the grains examined. These results show that mineral grains have more inclusions than expected from 2D observations. The X-ray absorption of the inclusions shows that they are not solid inclusions. No bubbles were observed inside, indicating that we cannot determine whether they are really aqueous fluids or merely voids. One calcite grain has an inclusion approx. 2 microns in size, which seems to have a bubble and a tiny solid daughter crystal inside (three-phase inclusion). As we know the exact 3D position of the inclusion, we will anlyze the inclusion by SIMS after freezing the sample as has been done for a halite sample [3]. The present technique is useful for finding small inclusions not only in carbonaceous chondrites but also for terrestrial materials.

Tsuchiyama, A.↗

Nondestructive Analysis of Apollo Samples by Micro-CT and Micro-XRF Analysis: A PET Style Examination

An integral part of any sample return mission is the initial description and classification of returned samples by the preliminary examination team (PET). The goal of a PET is to characterize and classify the returned samples, making this information available to the general research community who can then conduct more in-depth studies on the samples. A PET strives to minimize the impact their work has on the sample suite, which often limits the PET work to largely visual measurements and observations like optical microscopy. More modern techniques can also be utilized by future PET to nondestructively characterize astromaterials in a more rigorous way. Here we present our recent analyses of Apollo samples 14321 and 14305 by micro-CT and micro-XRF (respectively), assess the potential for discovery of "new" Apollo samples for scientific study, and evaluate the usefulness of these techniques in future PET efforts.

Zeigler, Ryan A.↗

Investigating the Geological History of Asteroid 101955 Bennu Through Remote Sensing and Returned Sample Analyses

The NASA New Frontiers Mission OSRIS-REx will return surface regolith samples from near-Earth asteroid 101955 Bennu in September 2023. This target is classified as a B-type asteroid and is spectrally similar to CI and CM chondrite meteorites [1]. The returned samples are thus expected to contain primitive ancient Solar System materials that formed in planetary, nebular, interstellar, and circumstellar environments. Laboratory studies of primitive astromaterials have yielded detailed constraints on the origins, properties, and evolutionary histories of a wide range of Solar System bodies. Yet, the parent bodies of meteorites and cosmic dust are generally unknown, genetic and evolutionary relationships among asteroids and comets are unsettled, and links between laboratory and remote observations remain tenuous. The OSIRIS-REx mission will offer the opportunity to coordinate detailed laboratory analyses of asteroidal materials with known and well characterized geological context from which the samples originated. A primary goal of the OSIRIS-REx mission will be to provide detailed constraints on the origin and geological and dynamical history of Bennu through coordinated analytical studies of the returned samples. These microanalytical studies will be placed in geological context through an extensive orbital remote sensing campaign that will characterize the global geological features and chemical diversity of Bennu. The first views of the asteroid surface and of the returned samples will undoubtedly bring remarkable surprises. However, a wealth of laboratory studies of meteorites and spacecraft encounters with primitive bodies provides a useful framework to formulate priority scientific questions and effective analytical approaches well before the samples are returned. Here we summarize our approach to unraveling the geological history of Bennu through returned sample analyses.

Messenger, S.↗

3D-Laser-Scanning Technique Applied to Bulk Density Measurements of Apollo Lunar Samples

In order to better interpret gravimetric data from orbiters such as GRAIL and LRO to understand the subsurface composition and structure of the lunar crust, it is import to have a reliable database of the density and porosity of lunar materials. To this end, we have been surveying these physical properties in both lunar meteorites and Apollo lunar samples. To measure porosity, both grain density and bulk density are required. For bulk density, our group has historically utilized sub-mm bead immersion techniques extensively, though several factors have made this technique problematic for our work with Apollo samples. Samples allocated for measurement are often smaller than optimal for the technique, leading to large error bars. Also, for some samples we were required to use pure alumina beads instead of our usual glass beads. The alumina beads were subject to undesirable static effects, producing unreliable results. Other investigators have tested the use of 3d laser scanners on meteorites for measuring bulk volumes. Early work, though promising, was plagued with difficulties including poor response on dark or reflective surfaces, difficulty reproducing sharp edges, and large processing time for producing shape models. Due to progress in technology, however, laser scanners have improved considerably in recent years. We tested this technique on 27 lunar samples in the Apollo collection using a scanner at NASA Johnson Space Center. We found it to be reliable and more precise than beads, with the added benefit that it involves no direct contact with the sample, enabling the study of particularly friable samples for which bead immersion is not possible

Macke, R. J.↗

Priority Science Targets for Future Sample Return Missions within the Solar System Out to the Year 2050

The Astromaterials Acquisition and Curation Office (henceforth referred to herein as NASA Curation Office) at NASA Johnson Space Center (JSC) is responsible for curating all of NASA's extraterrestrial samples. JSC presently curates 9 different astromaterials collections: (1) Apollo samples, (2) LUNA samples, (3) Antarctic meteorites, (4) Cosmic dust particles, (5) Microparticle Impact Collection [formerly called Space Exposed Hardware], (6) Genesis solar wind, (7) Star-dust comet Wild-2 particles, (8) Stardust interstellar particles, and (9) Hayabusa asteroid Itokawa particles. In addition, the next missions bringing carbonaceous asteroid samples to JSC are Hayabusa 2/ asteroid Ryugu and OSIRIS-Rex/ asteroid Bennu, in 2021 and 2023, respectively. The Hayabusa 2 samples are provided as part of an international agreement with JAXA. The NASA Curation Office plans for the requirements of future collections in an "Advanced Curation" program. Advanced Curation is tasked with developing procedures, technology, and data sets necessary for curating new types of collections as envisioned by NASA exploration goals. Here we review the science value and sample curation needs of some potential targets for sample return missions over the next 35 years.

McCubbin, F. M.↗

Correlated Amino Acid and Mineralogical Analyses of Milligram and Submilligram Samples of Carbonaceous Chondrite Lonewolf Nunataks 94101

Amino acids, the building blocks of proteins, have been found to be indigenous in the eight carbonaceous chondrite groups. The abundances, structural, enantiomeric and isotopic compositions of amino acids differ significantly among meteorites of different groups and petrologic types. These results suggest parent-body conditions (thermal or aqueous alteration), mineralogy, and the preservation of amino acids are linked. Previously, elucidating specific relationships between amino acids and mineralogy was not possible because the samples analyzed for amino acids were much larger than the scale at which petrologic heterogeneity is observed (sub mm-scale differences corresponding to sub-mg samples); for example, Pizzarello and coworkers measured amino acid abundances and performed X-ray diffraction (XRD) on several samples of the Murchison meteorite, but these analyses were performed on bulk samples that were 500 mg or larger. Advances in the sensitivity of amino acid measurements by liquid chromatography with fluorescence detection/time-of-flight mass spectrometry (LC-FD/TOF-MS), and application of techniques such as high resolution X-ray diffraction (HR-XRD) and scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS) for mineralogical characterizations have now enabled coordinated analyses on the scale at which mineral heterogeneity is observed. In this work, we have analyzed samples of the Lonewolf Nunataks (LON) 94101 CM2 carbonaceous chondrite. We are investigating the link(s) between parent body processes, mineralogical context, and amino acid compositions in meteorites on bulk samples (approx. 20mg) and mineral separates (< or = 3mg) from several of spatial locations within our allocated samples. Preliminary results of these analyses are presented here.

LONEWOLF NUNATAKS 94101↗

Effects of Sample Holder Edge Geometry on Atomic Oxygen Erosion Yield of Pyrolytic Graphite Exposed in Low Earth Orbit

The measurement of the erosion yield (volume lost per incident atom) of polymers and carbon using low Earth orbital (LEO) atomic oxygen exposure has typically involved placing small samples in holders that have chamfered edges. The chamfered edges have sometimes cause the samples to tear by their perimeters. This paper reports an evaluation of the erosion profile of a LEO atomic oxygen exposed pyrolytic graphite sample to determine the extent to which the erosion yield is altered by the chamfer and what the expected erosion yield would be for large area samples. The results indicate that the durability of large area samples would be approx. 5.2% lower than predicted based on mass loss of small samples with exposed diameters of 0.838 inch (2.13 cm) and chamfered sample holders.

erosion yield↗

Analysis of Sample Acquisition Dynamics Using Discrete Element Method

The analysis presented in this paper is conducted in the framework of the Ocean Worlds Autonomy Testbed for Exploration Research and Simulation (OceanWATERS) project, currently under development at NASA Ames Research Center. OceanWATERS aims at designing a simulation environment which allows for testing autonomy of scientific lander missions to the icy moons of our solar system. Mainly focused on reproducing the end effector interaction with the inherent terrain, this paper introduces a novel discrete element method (DEM)-based approach to determine forces and torques acting on the lander’s scoop during the sample acquisition process. An accurate force feedback from the terrain on the scoop is required by fault-detection and autonomous decision-making algorithms to identify when the requested torque on the robotic arm’s joints exceeds the maximum available torque. Knowledge of the terrain force feedback significantly helps evaluating the arm’s links structural properties and properly selecting actuators for the joints. Models available in literature constitute a partial representation of the dynamics of the interaction. As an example, Balovnev derived an analytical expression of the vertical and horizontal force acting on a bucket while collecting a sample as a function of its geometry and velocity, soil parameters and reached depth. Although the model represents an adequate approximation of the two force components, it ignores the direction orthogonal to the scoop motion and neglects the torque. This work relies on DEM analysis to compensate for analytical models’ deficiencies and inaccuracies, i. e. provide force and torque 3D vectors, defined in the moving reference (body) frame attached to the scoop, at each instant of the sample collection process. Results from the first presented analysis relate to the specific OceanWATERS sampling strategy, which consists of collecting the sample through five consecutive passes with increasing depth, each pass following the same circularlinear- circular trajectory. Data is collected given a specific scoop design interacting with two types of bulk materials, which may characterize the surface of icy planetary bodies: snow and ice. Although specifically concerned with the OceanWATERS design, this first analysis provides the expected force trends for similar sampling strategies and allows to deduce phenomenological information about the general scooping process. In order to further instruct the community on the use of DEM tools as a solution to the sampling collection problem, two more analyses have been carried out, mainly focused on reducing the DEM computation time, which increases with a decrease in particle size. After running a set of identical simulations, where the only changing parameter is the size of the spherical particle, it is observed that the resulting force trajectories, starting from a given particle size, converge to the true trend. It is deducible that a further decrease in size yields negligible improvements in the accuracy, while it sensibly increases computation time. A final analysis aims at discussing limitations of approximating bulk material particles having a complex shape, e. g. ice fragments, with spheres, by comparing force trends resulting in the two cases for the same simulation scenario.

Catanoso, Damiana↗

Adapting Apollo-Era Instrumentation for Cold Sample Processing While Maintaining Curatorial Standard Practices

The goal of the Apollo Next Generation Sample Analysis (ANGSA) Program is to study “specially curated samples,” that is, unstudied Apollo samples that have been preserved under unique conditions. A subset of the funded ANGSA work includes the study of Apollo samples stored under cold conditions since their return from the Moon. Ongoing ANGSA processing and future returned samples require cold curation strategies to preserve the integrity of organic and other temperature-sensitive constituents within those samples. Standard Apollo curation processing hardware and procedures are designed for room temperature operations, not cold conditions. This abstract details the major modifications of a heritage lunar cabinet in preparation for the first cold curation processing at Johnson Space Center. Future publications will provide greater detail on the low temperature materials and operation procedures. This work not only supports Apollo but also future cold sample return missions.

Amick, Cecilia L.↗

Reflectance spectra measurement plan of captured samples from Ryugu: current status

Hayabusa2 spacecraft is equipped with Optical Navigation Camera (ONC) andNear-infrared Spectrometer (NIRS3), and has obtained reflectance spectra of the C-type near-Earth asteroid Ryugu over a wavelength range of 0.40–0.95 μm and 1.8–3.2 μm, respectively. It was revealed that Ryugu exhibits globally very low albedo (less than 0.02 at 0.55 and 2.0 μm), a slightly positive spectral slope, and an ubiquitous weak but sharp OH absorption band centered at 2.72 μm,showing a little regional heterogeneities. Thus, the surface material of Ryugu can be estimated as relatively similar to moderately heated carbonaceous chondrites, e.g., moderately dehydrated CI and CM, and enriched in carbon (Kitazato et al., 2019; Sugita et al., 2019; Tatsumi et al., 2020).Hayabusa2 successfully has performed twice touch down operations, and the captured sample will be brought back to the Earth in late 2020 (Morota et al., 2020; Tachibana et al., in preparation). To clarify Ryugu’s mineralogical and physicochemical properties and their varieties, effective for spectral characteristics obtained by ONC and NIRS3, several grains are planned to be distributed to several primary analysis groups. In this study, we report the current status of our spectral analysis plan in Hayabusa2 MINeralogy and PETrology of coarse grains (MIN-PET CG) team led by T. Nakamura, and the latest rehearsal analysis result using carbonaceous chondrite samples. MIN-PET CG rehearsal measurements have been performed to obtain detailed spectral properties of Ryugu grains with diverse spatial resolutions ranging from μm to mm scale or larger; using a few mm size polished CM sample with several microscopic imaging spectrometers covering various spatial range; with 200 μmor finer spatial resolution at Institut d’Astrophysique Spatiale, ~50 and 150 μm spatial resolution invisible and IR ranges at Brown University, and with 40 μm or larger spatial resolution at Tohoku University, and using mm-size CM and CI grains with a diffuse reflectance spectrometer with a few mm resolution at Tohoku University. Diffuse reflectance spectroscopy measurements undergo to use several mm-size CM or CI chondrite grains with Bruker VERTEX 70v, which covers ~0.38–15 μm in wavelength. To keep returned samples out of atmosphere avoiding any terrestrial contamination, wehave prepared an air shutoff cell to put samples and standard materials together kept in a N2 purged condition (Amano et al., 2020). Samples are Murchison CM chondrite showing typically ~5%reflectance with a strong OH absorption band at ~2.8 μm, and laboratory heated CI chondrite showing~3% reflectance, and a weak OH absorption band at ~2.7 μm. We will perform (1) fixed angle condition as laboratory standard setting at incident, emission, and phase angles of 30°, 0°, 30°, or 0°,30°, 30°, and (2) various angle conditions for photometric corrections. Future lab analyses of samples returned from Ryugu will provide direct and detailed information on the mineralogical and physicochemical properties of Ryugu, and relationship of spectral characteristics obtained by remote sensing and laboratory instruments.

M. Matsuoka↗

Mars Sample Return Conceptual Mission Overview

This talk will provide an overview of an overall Mars Sample Return campaign architecture, and the current concepts and options for the architecture and design of a Mars Sample Retrieval Lander (called Sample Retrieval Lander, SRL). The overall SRL mission concept and key mission objectives will be described, including the mission’s concept of operations and a notional timeline from launch to entry, through surface operations, to delivery of the samples to Mars orbit. The overall lander vehicle concept will be described, including current options being evaluated. Key lander element options will be discussed, including a Mars Ascent Vehicle (MAV), Fetch Rover, Orbiting Sample container (OS), and tube transfer robotics systems. Details of the notional Fetch Rover functions, constraints and operations will be discussed. Specific challenges and approaches for addressing those challenges will be discussed, including key technical margins and planetary protection. Major trade studies and implementation approaches and a proposed schedule will also be discussed. The information provided about possible Mars sample return architectures and concepts is for planning and discussion purposes only. NASA and ESA have made no official decisions to implement Mars Sample Return.

Beyer, Friederike↗