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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 865 records · Page 48
All sourcesNASA NTRSDOE OSTI
NASA NTRS1978

Rocket effluent size distributions made with a cascade quartz crystal microbalance

Airborne particulate size distribution measurements were made in the stabilized ground cloud from a Titan III C rocket just after launch from the Kennedy Space Center on May 12, 1977. The measurements were made from aboard a small twin engine aircraft instrumented with particle and gas sensors. The plume was followed for about 1 hour while making multiple passes through the cloud at varying altitudes. The results obtained with a ten-stage cascade quartz crystal microbalance impactor show that the mass concentration as a function of particle diameter is bimodal with the first maximum between 0.05 micrometers and 0.1 micrometers and the second maximum between 0.8 and 1.0 micrometer. Scanning electron microscope analysis were performed on the material collected and show distinctly different kinds of particles in the two modes.

Woods, D. C.↗
NASA NTRS1978

Origin and modal petrography of Luna 24 soils

Petrographic modal analyses of polished grain mounts of fractions in the 20 to 250 micron size range from Luna 24 soil samples are presented and used to infer the nature and relative contributions of source rocks. It is found that more than 90% of the identifiable rock fragments are mare basalts, with about 11% of the soil consisting of the crystalline form. Soil breccias, which make up nearly 10% of the soil, are found to be immature. Electron probe analysis of glass particles reveals principle clusters conforming to anorthosite, anorthositic gabbro and mare basalts. More than half of the soil is composed of monomineralic particles, with pyroxene as the most abundant mineral. It is concluded that 85% of the regolith is derived from local mare basalts and gabbros and about 10% is derived from early cumulates of local mare basalt magma. Highland sources are considered to contribute not more than 3% of the regolith.

Basu, A.↗
NASA NTRS1979

The petrogenesis of L-6 chondrites - Insights from the chemistry of minerals

Measurements of the major, minor and trace element abundances of the major minerals of the L-6 chondrites Alfianello, Colby (WI) and Leedey are used to investigate the formation mechanisms of L-6 chondrites. Electron microprobe analysis was performed on individual grains of each mineral, and separated minerals were analyzed by instrumental and radiochemical neutron activation analysis. The compositions of the three meteorites are observed to be generally uniform, however different abundances and distributions of rare earth elements and Co and Ni indicate that the meteorites have different petrogenetic histories. Alkali element distributions are found to be incompatible with internal equilibration of a closed system.

Curtis, D. B.↗
NASA NTRS1980

Metamorphism of the H-group chondrites - Implications from compositional and textural trends in chondrules

The paper discusses element bulk compositions of 373 chondrules from 18 H3 to H6 chondrites determined by broad-beam electron probe analysis. Bulk chondrule FeO and Al2O3 amounts increase and TiO2 and Cr2O3 decrease with increasing petrologic type; normative faylite, albite, and plagioclase amounts increase through the petrologic sequence. Chondrule diameters correlate with phenocryst sizes in porphyritic chondrules of type 3 chondrites, but this correlation is diminished in the higher petrologic types. The compositional trends in chondrules through the petrologic sequence are attributed to diffusion and equilibration among chondrules, and between chondrules and matrix in response to increasing degrees of thermal metamorphism. It is suggested that H-group chondrites are formed by accretion of high-temperature (chondrules) and low-temperature (matrix) materials. Internal reheating of the parent materials to different temperatures caused compositional equilibration, grain coarsening, and reduction of FeO to Fe(0) by carbon.

Lux, G.↗
NASA NTRS1980

Iodine monofluoride emission spectrum and formation kinetics in electron-beam-produced plasmas

The observation of intense blue-green spontaneous emission attributed to IF from electron-beam-excited Ar/CF3I/NF3 gas mixtures is reported. Intense emission from a structured band centered at a wavelength of 484 nm was observed when mixtures of 2000-4000 Torr AR (or He or Ne), 3 Torr CF3I and 1 Torr NF3 (or F2) were irradiated with a 3-nsec FWHM electron beam. Analysis of ICl and IBr spectra, which the present spectrum closely resembles, indicates that the 484-nm emission originates from the E to A 3 pi 1 transition of IF. Examination of the time dependence of metastable IF and I2 emission reveals that the IF (E) level is formed primarily by excitation transfer from metastable I(4P) states. The fluorescence efficiency of the E-A transition and the radiative lifetime of the metastable IF (E) state are estimated to be approximately 6% and 15 nsec, respectively, and it is suggested that metastable IF is an attractive candidate for a blue-green laser.

Hutchison, S. B.↗
NASA NTRS1981

Adhesion and friction of transition metals in contact with nonmetallic hard materials

Sliding friction experiments were conducted with the metals yttrium, titanium, tantalum, zirconium, vanadium, neodymium, iron, cobalt, nickel, tungsten, platinum, rhenium, ruthenium, and rhodium in sliding contact with single crystal diamond, silicon carbide, pyrolytic boron nitride, and ferrite. Auger electron spectroscopy analysis was conducted with the metals and nonmetals to determine the surface chemistry and the degree of surface cleanliness. The results of the investigation indicate the adhesion and friction of the transition metals in contact with diamond, silicon carbide, boron nitride, and ferrite are related to the relative chemical activity of the metals. The more chemically active the metal, the higher the coefficient of friction and the greater amount of transfer to the nonmetals.

Miyoshi, K.↗
NASA NTRS1981

High resolution angular sensor

Specifications for the pointing stabilization system of the large space telescope were used in an investigation of the feasibility of reducing ring laser gyro output quantization to the sub-arc-second level by the use of phase locked loops and associated electronics. Systems analysis procedures are discussed and a multioscillator laser gyro model is presented along with data on the oscillator noise. It is shown that a second order closed loop can meet the measurement noise requirements when the loop gain and time constant of the loop filter are appropriately chosen. The preliminary electrical design is discussed from the standpoint of circuit tradeoff considerations. Analog, digital, and hybrid designs are given and their applicability to the high resolution sensor is examined. the electrical design choice of a system configuration is detailed. The design and operation of the various modules is considered and system block diagrams are included. Phase 1 and 2 test results using the multioscillator laser gyro are included.

Gneses, M. I.↗
NASA NTRS1979

Space Telescope digicon technology

The objective of this program was to develop the technology and construct a number of tubes conforming to the chosen configuration. A total of ten starts were made and ten tubes went through to test. Of the ten tubes three were CsI on LiF, six were CsTe on MgF2 and one was KNaCsSb on SiO2. All three faceplate crystals sealed successfully using indium as the sealant. In addition, a number of test seals were made and two photocathode sample runs were made. The tasks E-field, faceplate, anti-corona and electron optical analysis were actively pursued and the results integrated into the BASD HRS project.

Alting-Mees, H. R.↗
NASA NTRS1981

Metallic minerals, thermal histories and parent bodies of some xenolithic, ordinary chondrite meteorites

The metal grains were investigated in the hosts and lithic fragments of various petrologic types in four xenolithic chondrites using reflected-light microscopy and electron-probe analysis. The kamacite, taenite, tetrataenite, and troilite in Weston and Fayetteville have many textures; on a Wood plot of the central Ni content vs dimensions, the taenite content shows scatter if metal grains had cooled at rates of 10-1000 and 1-100 K/Myr through 700 K. In contrast, metallic minerals in Bhola and Mezo-Madaras have uniform textures and plot coherently, indicating cooling rates of 0.1 and 1 K/Myr, respectively, in the 700-600 K range. It is concluded that the host and xenoliths in these chondrites were cooled slowly after compaction; their clasts underwent peak metamorphic temperatures and slow cooling through 700 K in different environments.

Scott, E. R. D.↗
NASA NTRS1981

The mineralogy and the isotopic composition of sulfur in hydrothermal sulfide/sulfate deposits on the East Pacific Rise, 21 deg N latitude

The mineralogy and isotopic composition of sulfur found in hydrothermal deposits associated with five groups of vents along the ridge axis of the East Pacific Rise near 21 deg N latitude are investigated. Solid samples of mixed sulfides and sulfates from mounds, chimneys and the surrounding sediment as well as fresh basaltic glass were examined with a portable X-ray fluorescence spectrometer and by scanning electron microscopy, X-ray diffractometry, and electron microprobe analysis. For the three vents of exit temperature close to 350 C, the chimneys are found to be rich in copper sulfides, while for those of temperatures around 300 C, zinc sulfide is found to predominate. The major sulfides found in the chimneys include wurtzite, chalcopyrite, pyrite and cubanite, with anhydrite the dominant sulfate. Significant mineralogical differences are found between active and inactive vents. The isotopic composition of sulfur in anhydrites from active vents is observed to be close to that of sea water and consistent with a derivation from sea water sulfate. The isotopic composition of sulfur in the sulfide minerals is explained in terms of precipitation from solutions with reduced sulfur derived from basalts or basaltic magmas, and sea water sulfate. Finally, the deposits are interpreted as the results of the mixing of H2S-dominated hydrothermal fluids with cold sea water near the sea floor.

Styrt, M. M.↗
NASA NTRS1982

Surface chemistry, microstructure and friction properties of some ferrous-base metallic glasses at temperatures to 750 C

X-ray photoelectron spectroscopy analysis, transmission electron microscopy, diffraction studies, and sliding friction experiments were conducted with ferrous-base metallic glasses in sliding contact with aluminum oxide at temperatures from room to 750 C in a vacuum of 30 nPa. The results indicate that there is a significant temperature influence on the friction properties, surface chemistry, and microstructure of metallic glasses. The relative concentrations of the various constituents at the surface of the sputtered specimens were very different from the normal bulk compositions. Contaminants can come from the bulk of the material to the surface upon heating and impart boric oxide and silicon oxide at 350 C and boron nitride above 500 C. The coefficient of friction increased with increasing temperature to 350 C. Above 500 C the coefficient of friction decreased rapidly. The segregation of contaminants may be responsible for the friction behavior.

Miyoshi, K.↗
NASA NTRS1982

Deposit formation in hydrocarbon rocket fuels with an evaluation of a propane heat transfer correlation

A high pressure fuel coking testing apparatus was designed and developed and was used to evaluate thermal decomposition limits and carbon decomposition rates in heated copper tubes for hydrocarbon fuels. A commercial propane (90% grade) and chemically pure (CP) propane were tested. Heat transfer to supercritical propane was evaluated at 136 atm, bulk fluid velocities of 6 to 30 m/s, and tube wall temperatures in the range of 422 to 811 K. A forced convection heat transfer correlation developed in a previous test effort verified a prediction of most of the experimental data within a + or - 30% range, with good agreement for the CP propane data. No significant differences were apparent in the predictions derived from the correlation when the carbon resistance was included with the film resistance. A post-test scanning electron microprobe analysis indicated occurrences of migration and interdiffusion of copper into the carbon deposit.

Masters, P. A.↗
NASA NTRS1980

Petrography of lunar soil 15601

Lunar soil 15601 has been studied petrographically using grain size analysis, modal analysis, and electron probe microanalysis of monomineralic fragments in the 90-150-micron size fraction. The soil is immature; the grain size distribution is unimodal and very symmetrical, indicating that the soil is a homogeneous product of a single set of processes. It is concluded that 15601 is mostly a simple Apollo 15 mare basalt soil, and its properties can be used to approximate an end product of the array of complex soils that the lunar sample missions have returned.

Basu, A.↗
NASA NTRS1982

An incursion of dust in the southwestern United States from April 1980 eruptions of Mount St. Helens

An intrusion of volcanic dust occurred over the northern Mojave Desert, one month before the explosive eruption of 18 May 1980. Visibility was reduced to 15 to 30 miles during meteorological conditions that should have yielded a visibility in excess of 100 miles. This intrusion was documented by particle size distributions, scanning electron microscope analysis of Nuclepore filter samples, insolation measurements, observations by Navy and NASA aircraft, and meteorological data. No further incidents have been observed to date because of a lack of simultaneous volcanic activity with the particular wind patterns that existed in April. Therefore, under certain meteorological conditions, the desert of the southwestern United States could be significantly affected by volcanic ash from an eruption of Mount St. Helens.

Mathews, L. A.↗
NASA NTRS1983

Friction and wear of some ferrous-base metallic glasses

Sliding friction experiments, X-ray photoelectron spectroscopy (XPS) analysis, and electron microscopy and diffraction studies were conducted with ferrous base metallic glasses (amorphous alloys) in contact with aluminum oxide at temperatures to 750 C in a vacuum. Sliding friction experiments were also conducted in argon and air atmospheres. The results of the investigation indicate that the coefficient of friction increases with increasing temperature to 350 C in vacuum. The increase in friction is due to an increase in adhesion resulting from surface segregation of boric oxide and/or silicon oxide to the surface of the foil. Above 500 C the coefficient of friction decreased rapidly. The decrease correlates with the segregation of boron nitride to the surface. Contaminants can come from the bulk of the material to the surface upon heating and impart boric oxide and/or silicon oxide at 350 C and boron nitride above 500 C. The segregation of contaminants is responsible for the friction behavior. The amorphous alloys have superior wear resistance to crystalline 304 stainless steel. The relative concentrations of the various constituents at the surfaces of the amorphous alloys are very different from the nominal bulk compositions.

Miyoshi, K.↗
NASA NTRS1982

Surface chemistry, friction and wear of Ni-Zn and Mn-Zn ferrites in contact with metals

X-ray photoelectron and Auger electron spectroscopy analysis were used in sliding friction experiments. These experiments were conducted with hot-pressed polycrystalline Ni-Zn and Mn-Zn ferrites, and single-crystal Mn-Zn ferrite in contact with various transition metals at room temperature in both vacuum and argon. The results indicate that Ni2O3 and Fe3O4 were present on the Ni-Zn ferrite surface in addition to the nominal bulk constituents, while MnO2 and Fe3O4 were present on the Mn-Zn ferrite surface in addition to the nominal bulk constituents. The coefficients of friction for the ferrites in contact with metals were related to the relative chemical activity of these metals. The more active the metal, the higher is the coefficient of friction. The coefficients of friction for the ferrites were correlated with the free energy of formation of the lowest metal oxide. The interfacial bond can be regarded as a chemical bond between the metal atoms and the oxygen anions in the ferrite surfaces. The adsorption of oxygen on clean metal and ferrite does strengthen the metal-ferrite contact and increase the friction. The ferrites exhibit local cracking and fracture with sliding under adhesive conditions. All the metals transferred to he surfaces of the ferrites in sliding.

Miyoshi, K.↗
NASA NTRS1983

Ultrastructure of meristem and root cap of pea seedlings under spaceflight conditions

Data of electron microscopic analysis of meristem and root cap of pea seedlings grown aboard the Salyut-6 orbital research station in the Oazis apparatus and in the laboratory are presented. The main morphological and anatomical characteristics of the test and control plants are shown to be similar. At the same time, some differences are found in the structural and functional organization of the experimental cells as compared to the controls. They concern first of all the plastic apparatus, mitochondria and Golgi apparatus. It is assumed that cell function for certain periods of weightlessness on the whole ensures execution of the cytodifferentiation programs genetically determined on the Earth. Biochemical and physiological processes vary rather markedly due to lack of initially rigorous determination.

Sytnyk, K. M.↗
NASA NTRS1982

Trichite growth during oxidation of titanium and TA6V4 alloy by water vapor at high temperatures

Analysis by electron scanning microscope detected the formation of rutile trichites on the surface of specimens of titanium and titanium alloy TA6V4 oxidized in water vapor in the temperature range 650 to 950 C and the water vapor pressure range from 0.5 to 18 torr. In all specimens, two sublayers of rutile were formed: an external layer of basalt-like appearance, and a microcrystalline inner layer. Morphology of the trichites depends on temperature and the material (whether metal or alloy), but not on vapor pressure.

Coddet, C.↗