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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 865 records · Page 48
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Nanosecond Laser Drying in Wafer Foundries for Significant Energy Efficiency Improvement

Surface drying is a critical process in microelectronics wafer fabrication. In order to reduce and eliminate watermarks, many surface drying processes have been studied and used. Most of the wafer foundries currently use drying processes based on Isopropyl Alcohol (IPA), which causes serious safety (fire), health, environmental, and energy efficiency issues. The long-term goal of this project is to develop a fast, effective, chemical-free, and extremely energy efficient wafer drying technology that employs nanosecond laser-induced sub-surface evaporation and explosion. The objectives of this project are to 1) experimentally develop and verify the laser surface drying method, explore and identify how and to what extent various physical parameters influence the drying efficiency and effectiveness; and 2) understand and optimize the underlying thermodynamics in the proposed laser surface drying, including micro/nanoscale sub-surface superheating, evaporation, explosion, and photo/thermochemical bond breaking via atomistic modeling and experimental characterization. Toward these objectives, five tasks have been accomplished successfully, including 1) develop in-lab laser surface drying setup and study the effect of varied laser parameters, 2) use multiscale hybrid-modeling to study and understand the physics of water behavior during drying toward process optimization, 3) investigate the effect of drying conditions on the drying effectiveness, 4) develop a large-scale laser drying scanning system with automatic scanning, and 5) conduct large-scale simulation to study the effect of dopant level and develop strategies for system development toward industry deployment.

42 ENGINEERING↗
DOE OSTI2011

On the problem of local tissue hyperthermia control: multiscale modelling of pulsed laser radiation action on a medium with embedded nanoparticles

Methods for solving analytically and numerically the problem of multiscale modelling of the laser hyperthermia processes in a medium with nanoparticles are developed with regard to composite spherical nanoparticles (nanoshells). The features of the laser radiation field localisation on nanoscale inhomogeneities are investigated. Issues related to the control of the tissue hyperthermia processes by choosing the parameters of spatiotemporal localisation of the laser beam and of the absorbing nanoparticles are discussed. (application of lasers and laser-optical methods in life sciences)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2021

Femtosecond Laser Desorption Postionization MS vs ToF-SIMS Imaging for Uncovering Biomarkers Buried in Geological Samples

The study of lipid molecular fossils by traditional biomarker analysis requires bulk sample crushing, followed by solvent extraction, and then the analysis of the extract by gas chromatography-mass spectrometry (GC–MS). This traditional analysis mixes all organic compounds in the sample regardless of their origins, with a loss of information on the spatial distribution of organic molecules within the sample. These shortcomings can be overcome using the chemical mapping of intact samples. Spectroscopic techniques such as UV fluorescence or Raman spectroscopy, laser ablation inductively coupled plasma mass spectrometry, and time-of-flight secondary ion mass spectrometry (ToF-SIMS) are among those elemental and molecular mapping techniques. This study employed femtosecond (fs) laser ablation combined with single-photon ionization, a method called fs-laser desorption postionization mass spectrometry (fs-LDPI-MS). In this work, a pulsed ~75 fs, 800 nm laser was used to ablate the geological sample, which was then photoionized after a few microseconds by a pulsed 7.9 eV vacuum ultraviolet laser. An organic carbon-rich geological sample was used for this study to map hydrocarbon biomarkers in sediments that were previously studied by GC–MS. The petrography of this sample was examined by optical and fluorescence microscopy. It is demonstrated here that fs-LDPI-MS combined with petrography for multimodal imaging can expose buried compounds within the sample via in situ layer removal. When used in conjunction with traditional organic geochemical analysis, this method has the potential to determine the spatial distribution of organic biomarkers in geological material. Finally, fs-LDPI-MS imaging data are compared with ToF-SIMS imaging that is commonly used for such studies.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

Efficient Full-Field Vibration Measurements and Operational Modal Analysis Using Neuromorphic Event-Based Imaging

Traditional vibration measurement typically requires physically attached sensors, such as accelerometers and strain gauges. However, these discrete-point sensors provide only low spatial resolution vibration measurements, potentially foregoing valuable structural information such as localized damage. Noncontact optical measurement methods such as laser vibrometers can achieve high spatial resolution vibration measurements but only through time-consuming sequential measurements and are not cost-effective. As an alternative to traditional vibration measurement methods, digital video cameras are relatively low-cost, agile, and offer noncontact, simultaneous high spatial resolution measurements where every pixel on the structure becomes a measurement point. However, regular digital video cameras are frame-based where each pixel simultaneously performs temporally uniform (synchronous) measurements containing large amounts of redundant (background) data, which consumes considerable resources for video data measurement, management, and processing. To alleviate such a challenge, this work explores the use of event-based neuromorphic imagers, specifically silicon retinas, an efficient alternative to traditional frame-based video cameras, to perform full-field vibration measurements and operational modal analysis. By imitating biological vision, each silicon retina pixel independently and asynchronously records only intensity change events that contain structural motion information while excluding redundant (background) information. Such an asynchronous event-based data measurement mechanism allows for structural motion to be captured on the microsecond scale in an extremely data-efficient manner, which could benefit real-time vibration measurement and control applications. This study takes the first step toward these applications by formulating an existing video frame-based full-field operational modal analysis technique in the event-based, asynchronous silicon retina measurement framework. Specifically, local phase-based motion extraction and blind source separation are used to automatically and efficiently extract full-field vibration and dynamics parameters from silicon retina measurements. The developed method is validated by laboratory experiments on a bench-scale cantilever beam.

42 ENGINEERING↗
NASA NTRS1987

A method of atmospheric density measurements during Shuttle entry using UV laser Rayleigh scattering

A detailed study is described of the performance capabilities and the hardware requirements for a method in which ambient density is measured along the Space Shuttle flight path using on-board optical instrumentation. The technique relies on Rayleigh scattering of light from a pulsed, ultraviolet, ArF excimer laser operating at a wavelength of 193 nm. The method is shown to be capable of providing direct measurements of ambient density with an uncertainty of less than 1 percent and with a spatial resolution of 1 km, over an altitude range from 50 to 90 km. In addition, extensions of this concept are discussed that allow measurements of the shock wave location and the density profile within the shock layer. Two approaches are identified that appear to be feasible, in which the same laser system is used for the extended measurements as that required for the ambient density measurements.

Mckenzie, Robert L.↗
NASA NTRS1975

Flow tracing fidelity of scattering aerosol in laser Doppler velocimetry

An experimental method for the determination of the flow-tracing fidelity of a scattering aerosol used in laser Doppler velocimeters was developed with particular reference to the subsonic turbulence measurements. The method employs the measurement of the dynamic response of a flow-seeding aerosol excited by acoustic waves. The amplitude and frequency of excitation were controlled in order to simulate the corresponding values of fluid turbulence components. Experimental results are presented on the dynamic response of aerosols over the size range from 0.1 to 2.0 microns in diam and over the frequency range 100 Hz to 100 kHz. It was observed that unit-density spherical scatterers with diameters of 0.2 micron followed subsonic air turbulence frequency components up to 100 kHz with 98% fidelity.

Mazumder, M. K.↗
DOE OSTI2017

Increasing the Sensitivity of Lidar Systems Based on the LF/LIF Method

The results of studies on the development of laser sources in the UV and IR spectral ranges for the lidar systems operating on the basis of a method of laser fragmentation with subsequent laser-induced fluorescence (LF/LIF) are presented. It is shown that LF/LIF is an effective method for the remote detection of harmful and dangerous substances including nitrogen oxides in the atmosphere. The formation of a high-quality sounding UV radiation in excimer lasers and its transportation along the atmospheric path is studied. The causes are revealed that lead to the formation of noise arising in the atmosphere and limiting the sensitivity of the applied method.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
NASA NTRS1978

Rapid laser induced energy transfer in atomic systems

Analytical and experimental studies of the rapid transfer of stored populations from metastable states to selected target states of a different species are reported. Both laser-induced or laser-switched collision and laser-induced two-photon spontaneous emission are described. It is shown that the laser-induced collision method is particularly useful in the visible and UV spectral regions. It has applications in photochemistry, gas-phase kinetics, and in high-power, high-energy gas-phase lasers. The anti-Stokes source is useful in the VUV and soft X-ray spectral regions.

Harris, S. E.↗
NASA NTRS1987

Measurements of temperature, density, pressure, and their fluctuations in supersonic turbulence using laser-induced fluorescence

A laser-induced fluorescence method has been developed that provides simultaneous measurements of temperature, density, and their fluctuations owing to turbulence in unheated compressible flows. Pressure and its fluctuations are also deduced using the equation of state. Fluorescence is induced in nitric oxide that has been seeded into a nitrogen flow in concentrations of 100 ppm. Measurements are obtained from each laser pulse, with a spatial resolution of 1 mm and a temporal resolution of 125 ns. The method was applied to a supersonic, turbulent, boundary-layer flow with a free-stream Mach number of 2. For stream conditions in the range from 150-300 K and 0.3-1 atm, temperature is measured with an uncertainty of approximately 1 percent rms, while density and pressure uncertainties are approximately 2 percent rms.

Gross, K. P.↗
DOE OSTI2020

Uncovering Uranium Isotopic Heterogeneity of Fuel Pellets from the Fifth Collaborative Materials Exercise of the Nuclear Forensics International Technical Working Group

In 2017, the Nuclear Forensics International Technical Working Group (ITWG) organized their fifth 37 Collaborative Materials Exercise (CMX-5). The exercise samples were two uranium dioxide fuel pellets 38 manufactured from the same starting materials by different processes to have similar bulk isotopic 39 composition, but different spatial uranium isotopic distributions. Sets of identical materials were sent to 40 all participating laboratories, who then utilized their existing nuclear forensic capabilities to 41 independently analyse fuel pellets and identify similarities and differences of the materials’ 42 characteristics. The analytical methods used to probe the fuel pellets included ex situ, such as sectioning 43 or breaking up the pellets and analyzing dissolved pieces using inductively coupled plasma mass 44 spectrometry (ICP-MS), analyzing particles collected from intact or fragmented pellets by secondary ion 45 mass spectrometry (SIMS), as well as in situ methods, such as laser ablation coupled with ICP-MS, 46 autoradiography and nanoSIMS. In this paper we present the results of these independent analyses and 47 compare the capabilities of those nuclear forensic analytical methods to uncover details of the isotopic 48 heterogeneity of uranium fuel pellets.

Nuclear Forensic Analysis of Uranium Fuel Pellets,↗
NASA NTRS2012

Characterization of 4H <000-1> Silicon Carbide Films Grown by Solvent-Laser Heated Floating Zone

Commercially available bulk silicon carbide (SiC) has a high number (>2000/sq cm) of screw dislocations (SD) that have been linked to degradation of high-field power device electrical performance properties. Researchers at the NASA Glenn Research Center have proposed a method to mass-produce significantly higher quality bulk SiC. In order for this bulk growth method to become reality, growth of long single crystal SiC fibers must first be achieved. Therefore, a new growth method, Solvent-Laser Heated Floating Zone (Solvent-LHFZ), has been implemented. While some of the initial Solvent-LHFZ results have recently been reported, this paper focuses on further characterization of grown crystals and their growth fronts. To this end, secondary ion mass spectroscopy (SIMS) depth profiles, cross section analysis by focused ion beam (FIB) milling and mechanical polishing, and orientation and structural characterization by x-ray transmission Laue diffraction patterns and x-ray topography were used. Results paint a picture of a chaotic growth front, with Fe incorporation dependant on C concentration.

Woodworth, Andrew, A↗
DOE OSTI2017

Pulsed Laser Beam Welding of Pd 43 Cu 27 Ni 10 P 20 Bulk Metallic Glass

We used pulsed laser beam welding method to join Pd 43 Cu 27 Ni 10 P 20 (at.%) bulk metallic glass and characterized the properties of the joint. Fusion zone and heat-affected zone in the weld joint can be maintained completely amorphous as confirmed by X-ray diffraction and differential scanning calorimetry. No visible defects were observed in the weld joint. Nanoindentation and bend tests were carried out to determine the mechanical properties of the weld joint. Fusion zone and heat-affected zone exhibit very similar elastic moduli and hardness when compared to the base material, and the weld joint shows high ductility in bending which is accomplished through the operation of multiple shear bands. Furthermore, our results reveal that pulsed laser beam welding under appropriate processing parameters provides a practical viable method to join bulk metallic glasses.

36 MATERIALS SCIENCE↗
NASA NTRS2005

Diagnostics Adapted for Heat-Treating Furnace Environment

Diagnostics developed for the in situ monitoring of rocket combustion environments were adapted for use in heat-treating furnaces. Simultaneous, in situ monitoring of the carbon monoxide, carbon dioxide, methane, water, and hydrogen concentrations in the endothermic gas of a heat-treating furnace were demonstrated under a Space Act Agreement between the NASA Lewis Research Center, the Heat Treating Network, and Akron Steel Treating Company. This endothermic gas, or "endogas," is produced in a catalytic process, where natural gas is "cracked" in the presence of air. Variations in the composition of the natural gas supplied lead to variations in the composition of the endothermic gas. These variations could lead to an unacceptable quality of steel products that are hardened through the carborization process that uses this gas. Conventional methods of monitoring the endogas include measuring the dew point of the gas and the oxygen concentration. From these data, the carbon monoxide content of the gas can be calculated. This carbon monoxide concentration creates the carbon potential needed for carburization. Several weak links are present in this approach. The oxygen monitor deteriorates over time, and the measurement might be inaccurate by 50 percent. Also, the chemistry equations, which are based on several assumptions, such as secondary species concentrations, provide only an approximate estimate of the carbon monoxide concentration. To address these weaknesses, we investigated a new method based on ordinary Raman spectroscopy, in which the carbon monoxide concentration is measured directly and in situ. This method measures the laser light scattered from the molecules. Each species interacts with the light and scatters the light at a different frequency. Spectral monitoring of the scattered light intensity at each molecular frequency of interest provides the species concentrations. One advantage over the conventional method is that several species can be monitored simultaneously. A second advantage is that the measurement is direct; there is no need to make assumptions, to filter the gas, or to calibrate the instrument. An instrument was designed consisting of a laser and a detection system within an enclosure, connected to an optical probe by fibers. For determining carbon monoxide concentration, the probe is mounted on the endothermic gas line, close to the generator. Optical fibers with a length of 150 ft have been used to transmit laser light from the instrument to the probe. There, the light is focused into the gas, and the scattered light is collected and transmitted back to the instrument where it is analyzed with a photomultiplier and lock-in amplifier. Laboratory tests have shown that with the current system the concentration of carbon monoxide, water, nitrogen, oxygen, and hydrogen in the air can be monitored with an accuracy of 1 percent. The concentration of carbon dioxide in the air can be monitored with an accuracy of 0.5 percent, and the concentration of methane with an accuracy of 0.2 percent. This instrument was taken to the Akron Steel Treating Plant, where field tests are in progress to verify the system capabilities. Planned developments are improving the accuracy, monitoring multiple locations, and reducing instrument size and cost.

Source record↗
NASA NTRS1982

Scanning afocal laser velocimeter projection lens system

A method and apparatus for projecting and focusing parallel laser light beams from a laser doppler velocimeter on a target area are described. The system includes three lenses. Two lenses work together as a fixed afocal lens combination. The third lens is a movable scanning lens. Parallel laser beams travel from the velocimeter through the scanning lens and through the afocal lens combination and converge, i.e., are focused, somewhere beyond. Moving the scanning lens relative to the fixed afocal combination results in a scanning of the focus area along the afocal combination's optical axis.

Rhodes, D. B.↗
NASA NTRS1983

Pulsed laser photolysis study of the reaction between O(3P) and HO2

It is pointed out that bimolecular reactions involving two free radicals are of great interest because both reactants have unpaired electrons and hence could interact at distances longer than those typical of radical-molecule encounters. A method based on laser photolysis is being developed to produce selectively free radicals in the homogeneous gas phase. This is to be done in such a way as to isolate the reaction of interest and subsequently follow the course of the reaction using spectroscopic techniques. The present investigation is concerned with a study in which the rate coefficient for the reaction of O(3P) with HO2, has been measured at N2 pressures ranging from 10 to 500 torr, taking into account the reaction O(3P)+HO2 yields OH-O2. In the described study, O(3P) and HO2 were produced by cophotolysis of O3 and H2O2 in N2 at 248.5 nm using a KrF excimer laser.

Ravishankara, A. R.↗
DOE OSTI2012

V-shaped resonators for addition of broad-area laser diode arrays

A system and method for addition of broad-area semiconductor laser diode arrays are described. The system can include an array of laser diodes, a V-shaped external cavity, and grating systems to provide feedback for phase-locking of the laser diode array. A V-shaped mirror used to couple the laser diode emissions along two optical paths can be a V-shaped prism mirror, a V-shaped stepped mirror or include multiple V-shaped micro-mirrors. The V-shaped external cavity can be a ring cavity. The system can include an external injection laser to further improve coherence and phase-locking.

47 OTHER INSTRUMENTATION↗
DOE OSTI2024

Microfluidic film evaporation with femtosecond laser-patterned surface

Systems, apparatuses, and methods for microfluidic fluid evaporation using femtosecond laser-patterned surfaces are disclosed. A microfluidic device may comprise a femtosecond laser-patterned substrate having at least one input path and at least one output path. The femtosecond laser-patterned substrate may comprise both superhydrophobic and superhydrophilic sections. Fluid deposited at an input path may be wicked to an output path due to the surface pattern. A heating device may be provided to heat the fluid to evaporate volatiles therefrom. Vacuums and gas streams may be used to aid in volatile removal. Gas streams may add gas to the microfluidic device to react with the fluid.

Pearson, Connor Daniel↗
DOE OSTI2012

Evolution of metastable state molecules N{sub 2}(A{sup 3}{Sigma}{sub u}{sup +}) in a nanosecond pulsed discharge: A particle-in-cell/Monte Carlo collisions simulation

A particle-in-cell plus Monte Carlo collisions method has been employed to investigate the nitrogen discharge driven by a nanosecond pulse power source. To assess whether the production of the metastable state N{sub 2}(A{sup 3}{Sigma}{sub u}{sup +}) can be efficiently enhanced in a nanosecond pulsed discharge, the evolutions of metastable state N{sub 2}(A{sup 3}{Sigma}{sub u}{sup +}) density and electron energy distribution function have been examined in detail. The simulation results indicate that the ultra short pulse can modulate the electron energy effectively: during the early pulse-on time, high energy electrons give rise to quick electron avalanche and rapid growth of the metastable state N{sub 2}(A{sup 3}{Sigma}{sub u}{sup +}) density. It is estimated that for a single pulse with amplitude of -9 kV and pulse width 30 ns, the metastable state N{sub 2}(A{sup 3}{Sigma}{sub u}{sup +}) density can achieve a value in the order of 10{sup 9} cm{sup -3}. The N{sub 2}(A{sup 3}{Sigma}{sub u}{sup +}) density at such a value could be easily detected by laser-based experimental methods.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗