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DOE OSTI2025

Physics-informed machine learning analysis for nanoscale grain mapping by synchrotron Laue microdiffraction

Understanding the grain morphology, orientation distribution and crystal structure of nanocrystals is essential for optimizing the mechanical and physical properties of functional materials. Synchrotron X-ray Laue microdiffraction is a powerful technique for characterizing crystal structures and orientation mapping using focused X-rays. However, when the grain sizes are smaller than the beam size, mixed peaks in the Laue pattern from neighboring grains limit the resolution of grain morphology mapping. We propose a physics-informed machine learning (PIML) approach that combines a convolutional neural network feature extractor with a physics-informed filtering algorithm to overcome the spatial resolution limits of X-rays, achieving nanoscale resolution for grain mapping. Our PIML method successfully resolves the grain size, orientation distribution and morphology of Au nanocrystals through synchrotron microdiffraction scans, showing good agreement with electron backscatter diffraction results. This PIML-assisted synchrotron microdiffraction analysis can be generalized to other diffraction-based probes, enabling the characterization of nanosized structures with micrometre-sized probes.

X-ray crystallography↗

NASA NTRS1979

A hydrological analysis of east Australian floods using Nimbus-5 electrically scanning radiometer data

The chronological development and diminution of six floods in eastern Australia during January, February, and March 1974 were mapped for the first time by the Nimbus Electrically Scanning Microwave Radiometer (ESMR). Day and nighttime ESMR (19.35 GHz) coverage was analyzed for the low gradient, flooded Darling River system in New South Wales. Apparent movement of surface water as indicated by low brightness temperatures (less than 250 K, day and less than 240 K, night) was easily followed around the curved runoff basin along the northern shoreline of the flooded Darling River during this 3-month period. This pattern was in good agreement with flood crest data at selected river height gage stations, even under cloudy conditions.

Allison, L. J.↗

NASA NTRS1993

An Application of a New Electromagnetic Sensor to Real-Time Monitoring of Fatigue Crack Growth in Thin Metal Plates

A major part of fracture mechanics is concerned with studying the initiation and propagation of fatigue cracks. This typically requires constant monitoring of crack growth during fatigue cycles which necessitates automation of the whole process. If the rate of crack growth can be determined the experimenter can vary externally controlled parameters such as load level, load cycle frequency and so on. Hence, knowledge of the precise location of the crack tip at any given time is very valuable. One technique currently available for measuring fatigue crack length is the DC potential drop method. The method, however, may be inaccurate if the direction of crack growth deviates considerably from what was assumed initially or the curvature of the crack becomes significant. Another approach is to digitize an optical image of the test specimen surface and then apply a pattern recognition technique to locate the crack tip, but this method is still under development. The present work is an initial study on applying eddy current-type probes to monitoring fatigue crack growth. The performance of two types of electromagnetic probes, a conventional eddy current probe and a newly developed self-nulling probe, was evaluated for the detection characteristics at and near the tips of fatigue cracks. The scan results show that the latter probe provides a very well defined local maximum in its output in the crack tip region suggesting the definite possibility of precisely locating the tip, while the former provides a somewhat ambiguous distribution of the sensor output in the same region. The paper is organized as follows: We start by reviewing the design and performance characteristics of the self-nulling probe and then describe the scan results which demonstrate the basic properties of the self-nulling probe. Next, we provide a brief description of the software developed for tracing a simulated crack and give a brief discussion of the main results of the test. The final section summarizes the major accomplishments of the present work and the elements of the future R&D needs.

Namkung, M.↗

NASA NTRS2006

Measurement of Model Noise in a Hard-Wall Wind Tunnel

Identification, analysis, and control of fluid-mechanically-generated sound from models of aircraft and automobiles in special low-noise, semi-anechoic wind tunnels are an important research endeavor. Such studies can also be done in aerodynamic wind tunnels that have hard walls if phased microphone arrays are used to focus on the noise-source regions and reject unwanted reflections or background noise. Although it may be difficult to simulate the total flyover or drive-by noise in a closed wind tunnel, individual noise sources can be isolated and analyzed. An acoustic and aerodynamic study was made of a 7-percent-scale aircraft model in a NASA Ames 7-by-10-ft (about 2-by-3-m) wind tunnel for the purpose of identifying and attenuating airframe noise sources. Simulated landing, takeoff, and approach configurations were evaluated at Mach 0.26. Using a phased microphone array mounted in the ceiling over the inverted model, various noise sources in the high-lift system, landing gear, fins, and miscellaneous other components were located and compared for sound level and frequency at one flyover location. Numerous noise-alleviation devices and modifications of the model were evaluated. Simultaneously with acoustic measurements, aerodynamic forces were recorded to document aircraft conditions and any performance changes caused by geometric modifications. Most modern microphone-array systems function in the frequency domain in the sense that spectra of the microphone outputs are computed, then operations are performed on the matrices of microphone-signal cross-spectra. The entire acoustic field at one station in such a system is acquired quickly and interrogated during postprocessing. Beam-forming algorithms are employed to scan a plane near the model surface and locate noise sources while rejecting most background noise and spurious reflections. In the case of the system used in this study, previous studies in the wind tunnel have identified noise sources up to 19 dB below the normal background noise of the wind tunnel. Theoretical predictions of array performance are used to minimize the width and the side lobes of the beam pattern of the microphone array for a given test arrangement. To capture flyover noise of the inverted model, a 104-element microphone array in a 622-mm-diameter cluster was installed in a 19-mm-thick poly(methyl methacrylate) plate in the ceiling of the test section of the wind tunnel above the aircraft model (see Figure 1). The microphones were of the condenser type, and their diaphragms were mounted flush in the array plate, which was recessed 12.7 mm into the ceiling and covered by a porous aromatic polyamide cloth (not shown in the figure) to minimize boundary-layer noise. This design caused the level of flow noise to be much less than that of flush-mount designs. The drawback of this design was that the cloth attenuated sound somewhat and created acoustic resonances that could grow to several dB at a frequency of 10 kHz.

Soderman, Paul T.↗

NASA NTRS2014

Performance Verification of the Gravity and Extreme Magnetism Small Explorer GEMS X-Ray Polarimeter

olarimetry is a powerful tool for astrophysical observations that has yet to be exploited in the X-ray band. For satellite-borne and sounding rocket experiments, we have developed a photoelectric gas polarimeter to measure X-ray polarization in the 2-10 keV range utilizing a time projection chamber (TPC) and advanced micro-pattern gas electron multiplier (GEM) techniques. We carried out performance verification of a flight equivalent unit (1/4 model) which was planned to be launched on the NASA Gravity and Extreme Magnetism Small Explorer (GEMS) satellite. The test was performed at Brookhaven National Laboratory, National Synchrotron Light Source (NSLS) facility in April 2013. The polarimeter was irradiated with linearly-polarized monochromatic X-rays between 2.3 and 10.0 keV and scanned with a collimated beam at 5 different detector positions. After a systematic investigation of the detector response, a modulation factor greater than or equal to 35% above 4 keV was obtained with the expected polarization angle. At energies below 4 keV where the photoelectron track becomes short, diffusion in the region between the GEM and readout strips leaves an asymmetric photoelectron image. A correction method retrieves an expected modulation angle, and the expected modulation factor, approximately 20% at 2.7 keV. Folding the measured values of modulation through an instrument model gives sensitivity, parameterized by minimum detectable polarization (MDP), nearly identical to that assumed at the preliminary design review (PDR).

Time Projection↗

NASA NTRS2003

Afferent innervation of the utricular macula in pigeons

Biotinylated dextran amine (BDA) was used to retrogradely label afferents innervating the utricular macula in adult pigeons. The pigeon utriclar macula consists of a large rectangular-shaped neuroepithelium with a dorsally curved anterior edge and an extended medioposterior tail. The macula could be demarcated into several regions based on cytoarchitectural differences. The striola occupied 30% of the macula and contained a large density of type I hair cells with fewer type II hair cells. Medial and lateral extrastriola zones were located outside the striola and contained only type II hair cells. A six- to eight-cell-wide band of type II hair cells existed near the center of the striola. The reversal line marked by the morphological polarization of hair cells coursed throughout the epithelium, near the peripheral margin, and through the center of the type II band. Calyx afferents innervated type I hair cells with calyceal terminals that contained between 2 and 15 receptor cells. Calyx afferents were located only in the striola region, exclusive of the type II band, had small total fiber innervation areas and low innervation densities. Dimorph afferents innervated both type I and type II hair cells with calyceal and bouton terminals and were primarily located in the striola region. Dimorph afferents had smaller calyceal terminals with few type I hair cells, extended fiber branches with bouton terminals and larger innervation areas. Bouton afferents innervated only type II hair cells in the extrastriola and type II band regions. Bouton afferents innervating the type II band had smaller terminal fields with fewer bouton terminals and smaller innervation areas than fibers located in the extrastriolar zones. Bouton afferents had the most bouton terminals on the longest fibers, the largest innervation areas with the highest innervation densities of all afferents. Among all afferents, smaller terminal innervation fields were observed in the striola and large fields were located in the extrastriola. The cellular organization and innervation patterns of the utricular maculae in birds appear to represent an organ in adaptive evolution, different from that observed for amphibians or mammals.

Non-NASA Center↗

DOE OSTI2026

Search for the chiral magnetic effect through beam energy dependence of charge separation using event shape selection

High-energy, heavy-ion collisions can create local domains of chirality-imbalanced quarks, reflecting the topological features of quantum chromodynamics. The chiral magnetic effect (CME) predicts an electric charge separation of quarks in such topological domains along the magnetic field ($\vec{B}$) generated by the passing of two high-Z nuclei. Here, we use a correlation observable Δ⁢𝛾$^{112}$ between charged meson pairs to detect the CME-induced charge separation and a novel event shape selection (ESS) method to mitigate the background effects related to elliptic flow (𝑣 2 ). The ESS method classifies events based on the emission pattern of final-state particles and determines Δ⁢𝛾$^{112}_{ESS}$ from the zero-flow limit. We reconstruct the $\vec{B}$ field direction from the spectator nucleons, which minimizes backgrounds unrelated to the collective motion of the system. In this work, we report the measurements of Δ⁢𝛾$^{112}$ and a background indicator Δ⁢𝛾$^{132}$ in Au+Au collisions from the Brookhaven National Laboratory Relativistic Heavy Ion Collider (RHIC) Beam Energy Scan phase II and at the top RHIC energy. After background suppression, Δ⁢𝛾$^{132}_{ESS}$ aligns with zero, and Δ⁢𝛾$^{112}_{ESS}$ is reduced to no more than 20% of Δ⁢𝛾$^{112}$. We observe a finite residual charge separation with 2.5⁢𝜎, 3⁢𝜎, and 3.2⁢𝜎 significance in the 20–50% centrality range of Au + Au collisions at 11.5, 14.6, and 19.6 GeV. The results at 17.3 and 27 GeV also show positive values but with a lower significance of 1.3⁢𝜎 and 1.1⁢𝜎, respectively. The corresponding Δ⁢𝛾$^{112}_{ESS}$ values at 7.7, 9.2, and 200 GeV are consistent with zero within uncertainties.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

NASA NTRS1981

Passive optical and infrared meteorology

Applications of passive visible and infrared techniques to the study of meteorological parameters are presented. For the remote sensing of temperature and humidity profiles, infrared sounder improvements have proceeded with the narrow band-pass channels approach, and the partially scanned interferogram approach. Current and planned infrared and microwave sea-surface temperature sounders have an expected accuracy of approximately 2 K, and this can be improved by using three super window channels from the 3.7 micron window region, with narrow band passes away from principal water vapor absorption lines. Cloud data remote sensing is currently performed from satellites, and these visible and infrared images have been used to track weather patterns. In addition, a passive infrared correlation-spectroscopy technique has been proposed for wind measurements. Finally, these techniques have also been applied to monitor such parameters as the Solar Constant, aerosols, and minor gas constituents.

Chahine, M. T.↗

NASA NTRS1986

Mesoscale and synoptic scale features of North Pacific weather systems observed with the scanning multichannel microwave radiometer on Nimbus 7

Employing data on integrated atmospheric water vapor, total cloud liquid water and rain rate obtainable from the Nimbus 7 Scanning Multichannel Microwave Radiometer (SMMR), the frontal structure of several mid-latitude cyclones over the North Pacific Ocean as they approach the West Coast of North America in the winter of 1979. The fronts, analyzed with all available independent data, are consistently located at the leading edge of the strongest gradient in integrated water vapor. The cloud liquid water content, which unfortunately has received very little in situ verification, has patterns which are consistent with the structure seen in visible and infrared imagery. The rain distribution is also a good indicator of frontal location and rain amounts are generally within a factor of two of what is observed with rain gauges on the coast. Furthermore, the onset of rain on the coast can often be accurately forecast by simple advection of the SMMR observed rain areas.

Katsaros, K. B.↗

NASA NTRS2024

A Specialized Ultrasound Protocol for NASA's Renal Stone Surveillance and Clinical Practice

INTRODUCTION Ample evidence exists on the effectiveness of ultrasound in the diagnosis of kidney stones. However, terrestrial practice is mostly concerned with diagnosis of clinically significant urolithiasis. Adapting this non-irradiating, low-cost imaging modality for the asymptomatic astronaut population offers high-sensitivity screening and limits their career radiation dose. METHODS NASA developed a novel ultrasound-based detection and surveillance protocol to identify, categorize, and monitor mineralized renal material (MRM) in astronauts. The term MRM was developed to denote abnormal, presumably calcified, focal material of unknown clinical significance in the kidneys. Sonographic criteria for MRMs include measurable echogenic foci, their detectability in multiple, designated imaging plains, posterior shadowing, and “twinkle” pattern visualized in Color Doppler and/or demonstrated in Spectral Doppler modes. The mere discovery of an MRM does not trigger further imaging or intervention, unless the affected crewmember is mission-assigned, or the MRM meets actionable criteria based on size, location, and sonographic characteristics. If the threshold is met, the crew surgeon is notified, and additional diagnostic imaging and urology consultation are considered. RESULTS In total, 73 individuals have been scanned using our specialized methods, 60 have had more than one study done. As of April 2023, 282 total studies have been performed. So far, over 30 pairs of pre-and postflight studies have been obtained, and the findings are presented elsewhere in this panel. DISCUSSION A surveillance program was initiated nine years ago to screen asymptomatic members of the astronaut corps for renal calcifications, from their initial hiring, through their mission timeframes, and throughout their career. The goal is to reduce the probability that an astronaut will fly with a renal stone that may become symptomatic. This also gives NASA the information it needs to improve screening criteria for future long-duration crewed missions.

H Lyons↗

DOE OSTI2019

Nanoscale mosaicity revealed in peptide microcrystals by scanning electron nanodiffraction

Abstract Changes in lattice structure across sub-regions of protein crystals are challenging to assess when relying on whole crystal measurements. Because of this difficulty, macromolecular structure determination from protein micro and nanocrystals requires assumptions of bulk crystallinity and domain block substructure. Here we map lattice structure across micron size areas of cryogenically preserved three−dimensional peptide crystals using a nano-focused electron beam. This approach produces diffraction from as few as 1500 molecules in a crystal, is sensitive to crystal thickness and three−dimensional lattice orientation. Real-space maps reconstructed from unsupervised classification of diffraction patterns across a crystal reveal regions of crystal order/disorder and three−dimensional lattice tilts on the sub-100nm scale. The nanoscale lattice reorientation observed in the micron-sized peptide crystal lattices studied here provides a direct view of their plasticity. Knowledge of these features facilitates an improved understanding of peptide assemblies that could aid in the determination of structures from nano- and microcrystals by single or serial crystal electron diffraction.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Tracer-Guided Characterization of Dominant Pore Networks and Implications for Permeability and Wettability in Shale

Pore network characterization is an important aspect in unconventional reservoir evaluation. While application of the technique of scanning electron microscope (SEM) brings substantial advances in pore characterization in shale, understanding the connected pore network that dominates flow in shale samples is limited by using SEM alone because of small fields of view and lack of views of connectivity in 3D. In this research, a technique integrating tracer imbibition, micro-computed tomography (CT) imaging, and SEM imaging was developed to provide a solution for multiscale imaging in shale. Tracer imbibition indicates pore connectivity; micro-CT imaging after tracer imbibition thus provides an overview of the connected pore network at the millimeter scale. With guidance from micro-CT images after tracer imbibition, a more accurate and detailed characterization of pore systems and related mineralogy can be conducted using higher-resolution SEM. The method was applied to five samples from Wolfcamp and Eagle Ford Formations. Results reveal the effectiveness of the integrated method by showing different patterns of distribution of the dominant pore network and different controlling mineralogy. Dominant porosity, estimated from grayscale analyses, displays a good correlation with permeability. This result indicates that dominant porosity is more relevant to permeability than is total porosity. Results from imbibition tests are also compared with that from contact angle measurement, and important implications on wettability can be obtained. The integrated method thus has the capacity to link the dominant pore network and wettability with microscale to submicroscale mineralogy, which can help better understand the pore systems and fluid flow in shale. Plain Language Summary Pore network characterization and wettability are two important aspects in unconventional reservoir evaluation and are crucial to understanding the nature of shale oil or gas storage and production. Here, a new technique integrating tracer imbibition, micro-computed tomography imaging, and scanning electron microscope imaging was developed for a more representative and effective pore characterization in shale. This integrated technique can provide a direct visualization of the dominant pore network in a millimeter-scale sample and, at the same time, can provide a guided pore network characterization under nanoscale resolution. This method thus can generate results that are more representative and more accurate in a more efficient way compared with the traditional scanning electron microscope method. The new technique can also reveal the local wettability in microscale. High-resolution analysis on the tracer imbibition or fluid displacement and mineralogy can shed light on the local wettability and the controlling mineralogy in shale.

58 GEOSCIENCES↗

DOE OSTI2022

A wide-field micro-computed tomography detector: micron resolution at half-centimetre scale

Ideal three-dimensional imaging of complex samples made up of micron-scale structures extending over mm to cm, such as biological tissues, requires both wide field of view and high resolution. For existing optics and detectors used for micro-CT (computed tomography) imaging, sub-micron pixel resolution can only be achieved for fields of view of <2 mm. This article presents a unique detector system with a 6 mm field-of-view image circle and 0.5 µm pixel size that can be used in micro-CT units utilizing both synchrotron and commercial X-ray sources. A resolution-test pattern with linear microstructures and whole adult Daphnia magna were imaged at beamline 8.3.2 of the Berkeley Advanced Light Source. Volumes of 10000 × 10000 × 7096 isotropic 0.5 µm voxels were reconstructed over a 5.0 mm × 3.5 mm field of view. Measurements in the projection domain confirmed a 0.90 µm measured spatial resolution that is largely Nyquist-limited. This unprecedented combination of field of view and resolution dramatically reduces the need for sectional scans and computational stitching for large samples, ultimately offering the means to elucidate changes in tissue and cellular morphology in the context of larger, whole, intact model organisms and specimens. This system is also anticipated to benefit micro-CT imaging in materials science, microelectronics, agricultural science and biomedical engineering.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2018

Elemental and topographical imaging of microscopic variations in deposition on NSTX-U and DIII-D samples

Tokamak plasma facing components have surface roughness that can cause microscopic spatial variations in erosion and deposition and hence influence material migration, erosion lifetime, dust and tritium accumulation, and plasma contamination. However high spatial resolution measurements of deposition on the scale of the surface roughness have been lacking to date. We will present elemental images of graphite samples from NSTX-U and DIII-D DiMES experiments performed with a Scanning Auger Microprobe at sub-micron resolution that show strong microscopic variations in deposition and correlate this with 3D topographical maps of surface irregularities. The NSTX-U samples were boronized and exposed to deuterium plasmas and the DiMES samples had localized Al and W films and were exposed to dedicated helium plasmas. Topographical maps of the samples were performed with a 3D confocal optical microscope and compared to the elemental deposition pattern. The results revealed localized deposition concentrated in areas shadowed from the ion flux, incident in a direction calculated (for the DiMES case) by taking account of the magnetic pre-sheath.

Surface analysis↗

DOE OSTI2019

Elemental and topographical imaging of microscopic variations in deposition on NSTX-U and DIII-D samples2

Abstract: Tokamak plasma facing components have surface roughness that can cause microscopic spatial variations in erosion and deposition and hence influence material migration, erosion lifetime, dust and tritium accumulation, and plasma contamination. However high spatial resolution measurements of deposition on the scale of the surface roughness have been lacking to date. We will present elemental images of graphite samples from NSTX-U and DIII-D DiMES experiments performed with a Scanning Auger Microprobe at sub-micron resolution that show strong microscopic variations in deposition and correlate this with 3D topographical maps of surface irregularities. The NSTX-U samples were boronized and exposed to deuterium plasmas and the DiMES samples had localized Al and W films and were exposed to dedicated helium plasmas. Topographical maps of the samples were performed with a 3D confocal optical microscope and compared to the elemental deposition pattern. The results revealed localized deposition concentrated in areas shadowed from the ion flux, incident in a direction calculated (for the DiMES case) by taking account of the magnetic pre-sheath.

Erosion, Deposition, NSTX-U, DIMES, Plasma-Materia↗

NASA NTRS1975

Cross correlation anomaly detection system

This invention provides a method for automatically inspecting the surface of an object, such as an integrated circuit chip, whereby the data obtained by the light reflected from the surface, caused by a scanning light beam, is automatically compared with data representing acceptable values for each unique surface. A signal output provided indicated of acceptance or rejection of the chip. Acceptance is based on predetermined statistical confidence intervals calculated from known good regions of the object being tested, or their representative values. The method can utilize a known good chip, a photographic mask from which the I.C. was fabricated, or a computer stored replica of each pattern being tested.

Micka, E. Z.↗

NASA NTRS1980

The Seasat scanning multichannel microwave radiometer /SMMR/ - Instrument description and performance

The scanning multichannel microwave radiometer (SMMR) is an imaging 5-frequency radiometer flown on the Seasat and Nimbus-7 earth satellites launched in 1978. It measures dual-polarized microwave radiances from the earth's atmosphere and surface, primarily for the purpose of deriving global and nearly all-weather measurements of sea surface temperature, wind speed, and atmospheric liquid water and water vapor. This paper describes the SMMR instrument and its calibration, antenna pattern measurements, and data processing procedures. Analysis of early data from the Seasat SMMR shows that the expected engineering performance in flight was achieved, and the measurement of sea surface temperature and wind speed with accuracies of 1.5 K and 2 m/s, respectively, may be achievable once the geophysical data processing algorithms and analysis have been completed.

Njoku, E. G.↗

NASA NTRS1984

Observing atmospheric water in storms with the Nimbus 7 scanning multichannel microwave radiometer

Employing data on integrated atmospheric water vapor, total cloud liquid water and rain rate obtainable from the Nimbus 7 Scanning Multichannel Microwave Radiometer (SMMR), we study the frontal structure of several mid-latitude cyclones over the North Pacific Ocean as they approach the West Coast of North America in the winter of 1979. The fronts, analyzed with all available independent data, are consistently located at the leading edge of the strongest gradient in integrated water vapor. The cloud liquid water content, which unfortunately has received very little in situ verification, has patterns which are consistent with the structure seen in visible and infrared imagery. The rain distribution is also a good indicator of frontal location and rain amounts are generally within a factor of two of what is observed with rain gauges on the coast. Furthermore, the onset of rain on the coast can often be accurately forecast by simple advection of the SMMR observed rain areas.

Katsaros, K. B.↗