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DOE OSTI2019

Raman Spectroscopy for the On-Line Analysis of Oxidation States of Oxygen Carrier Particles (Final Report)

The need for cleaner energy systems, including CO 2 capture technologies, is driving the current development of chemical looping technologies such as chemical looping combustion (CLC) and chemical looping gasification (CLG). Specific processes that are under development for using solid fuels are in-situ Gasification Chemical-Looping Combustion (iG-CLC) and Chemical Looping with Oxygen Uncoupling (CLOU). Chemical looping is based on using oxygen carriers (e.g., iron oxides, copper oxides, calcium sulfates, etc.) to provide the oxygen for the reaction with the fuel. In order to optimize the overall process performance, it is critical that the properties of the oxygen carriers are well-defined and maintained for their specific purpose during the different stages of the CLC process. One of the critical properties of the oxygen carrier is its oxidation state (e.g., content of Fe 2 O 3 vs. Fe 3 O 4 ) as it affects the fundamental operation of the CLC process. Unfortunately, the ability to make on-line measurements of the oxidation state of oxygen carriers is lacking and new sensors need to be developed. The goal of this project was to evaluate the potential of Raman spectroscopy as a sensor for the on-line analysis of the oxidation state of oxygen carrier particles. Oxygen carrier particles (OCPs) of interest include iron oxides, copper oxides, calcium sulfite, and calcium sulfate, with particle sizes typically less than 0.5 mm diameter. The expected operating conditions of the sensor include OCP temperatures in the range of 800 °C to 1000 °C, and pressures of about 10 atm. We evaluated continuous wave (cw), Quasi cw, pulsed, and time-gated Raman spectroscopy at multiple wavelengths (355 nm, 360 nm, 532 nm, 633 nm, 785 nm). Samples included iron oxides, copper oxides, calcium sulfate, and a custom sample provided by NETL for temperatures beyond 1000 °C. Our findings can be summarized as follows: Calcium sulfate can be detected via cw and pulsed 532 nm Raman spectroscopy at temperatures above 1100 °C.; Hematite (Fe 2 O 3 ) Raman spectra can be detected at temperatures of 700 °C via cw 360 nm, 1089 °C with cw 532 nm, 400 °C with cw 633 and 600 °C with cw 785 nm lasers; Magnetite (Fe 3 O 4 ) can be detected via cw 532 nm Raman spectroscopy up to 600 °C; Mixtures of Fe2O3 and Fe 3 O 4 can be distinguished for temperatures up to 600 °C using 532 nm; Copper oxides did not yield suitable signals at elevated temperatures; The custom NETL samples did not yield suitable signals at elevated temperatures. Raman spectroscopy would be a suitable approach for calcium sulfate as this material provides a very strong Raman signal at high temperatures. Oxygen carrier particles of higher interest such as metal oxides, however, do not yield a strong-enough signal at elevated temperatures. As such, Raman spectroscopy is not suitable to differentiate the oxidation state of these materials at temperatures above 600 °C.

01 COAL, LIGNITE, AND PEAT↗

DOE OSTI2019

Raman Spectroscopy for the On-Line Analysis of Oxidation States of Oxygen Carrier Particles

The need for cleaner energy systems, including CO 2 capture technologies, is driving the current development of chemical looping technologies such as chemical looping combustion (CLC) and chemical looping gasification (CLG). Specific processes that are under development for using solid fuels are in-situ Gasification Chemical-Looping Combustion (iG-CLC) and Chemical Looping with Oxygen Uncoupling (CLOU). Chemical looping is based on using oxygen carriers (e.g., iron oxides, copper oxides, calcium sulfates, etc.) to provide the oxygen for the reaction with the fuel. In order to optimize the overall process performance, it is critical that the properties of the oxygen carriers are well-defined and maintained for their specific purpose during the different stages of the CLC process. One of the critical properties of the oxygen carrier is its oxidation state (e.g., content of Fe 2 O 3 vs. Fe 3 O 4 ) as it affects the fundamental operation of the CLC process. Unfortunately, the ability to make on-line measurements of the oxidation state of oxygen carriers is lacking and new sensors need to be developed. The goal of this project was to evaluate the potential of Raman spectroscopy as a sensor for the on-line analysis of the oxidation state of oxygen carrier particles. Oxygen carrier particles (OCPs) of interest include iron oxides, copper oxides, calcium sulfite, and calcium sulfate, with particle sizes typically less than 0.5 mm diameter. The expected operating conditions of the sensor include OCP temperatures in the range of 800 °C to 1000 °C, and pressures of about 10 atm. We evaluated continuous wave (cw), Quasi cw, pulsed, and time-gated Raman spectroscopy at multiple wavelengths (355 nm, 360 nm, 532 nm, 633 nm, 785 nm). Samples included iron oxides, copper oxides, calcium sulfate, and a custom sample provided by NETL for temperatures beyond 1000 °C. Our findings can be summarized as follows: Calcium sulfate can be detected via cw and pulsed 532 nm Raman spectroscopy at temperatures above 1100 °C. Hematite (Fe 2 O 3 ) Raman spectra can be detected at temperatures of 700 °C via cw 360 nm, 1089 °C with cw 532 nm, 400 °C with cw 633 and 600 °C with cw 785 nm lasers. Magnetite (Fe 3 O 4 ) can be detected via cw 532 nm Raman spectroscopy up to 600 °C. Mixtures of Fe 2 O 3 and Fe 3 O 4 can be distinguished for temperatures up to 600 °C using 532 nm. Copper oxides did not yield suitable signals at elevated temperatures. The custom NETL samples did not yield suitable signals at elevated temperatures. Raman spectroscopy would be a suitable approach for calcium sulfate as this material provides a very strong Raman signal at high temperatures. Oxygen carrier particles of higher interest such as metal oxides, however, do not yield a strong-enough signal at elevated temperatures. As such, Raman spectroscopy is not suitable to differentiate the oxidation state of these materials at temperatures above 600 °C.

01 COAL, LIGNITE, AND PEAT↗

NASA NTRS1974

Data analysis study and performance evaluation of the scanning laser Doppler system

A simulation program which provided information on theoretically expected vortex spectra, evaluations of potential algorithms, and expected location accuracies for given scan patterns is presented. Field tests using an aircraft engine flow field and aircraft vortices during flyby tests were compared to the results of the simulation. From these studies, a vortex location algorithm was developed which provided vortex location for one or two vortices as a function of time. Results of this algorithm used on data from flyby tests were used to study vortex transport, to evaluate system performance, and to provide suggestions for real-time vortex location algorithms. The results of real-time analysis were compared to those which were expected based on theoretical considerations.

Sonnenschein, C. M.↗

DOE OSTI2022

De novo design and Rosetta-based assessment of high-affinity antibody variable regions (Fv) against the SARS-CoV -2 spike receptor binding domain ( RBD )

The continued emergence of new SARS-CoV-2 variants has accentuated the growing need for fast and reliable methods for the design of potentially neutralizing antibodies (Abs) to counter immune evasion by the virus. Here, we report on the de novo computational design of high-affinity Ab variable regions (Fv) through the recombination of VDJ genes targeting the most solvent-exposed hACE2-binding residues of the SARS-CoV-2 spike receptor binding domain (RBD) protein using the software tool OptMAVEn-2.0. Subsequently, we carried out computational affinity maturation of the designed variable regions through amino acid substitutions for improved binding with the target epitope. Immunogenicity of designs was restricted by preferring designs that match sequences from a 9-mer library of “human Abs” based on a human string content score. We generated 106 different antibody designs and reported in detail on the top five that trade-off the greatest computational binding affinity for the RBD with human string content scores. We further describe computational evaluation of the top five designs produced by OptMAVEn-2.0 using a Rosetta-based approach. We used Rosetta SnugDock for local docking of the designs to evaluate their potential to bind the spike RBD and performed “forward folding” with DeepAb to assess their potential to fold into the designed structures. Ultimately, our results identified one designed Ab variable region, P1.D1, as a particularly promising candidate for experimental testing. This effort puts forth a computational workflow for the de novo design and evaluation of Abs that can quickly be adapted to target spike epitopes of emerging SARS-CoV-2 variants or other antigenic targets.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2023

Changes in soil pore structure generated by the root systems of maize , sorghum and switchgrass affect in situ N 2 O emissions and bacterial denitrification

Due to the heterogeneous nature of soil pore structure, processes such as nitrification and denitrification can occur simultaneously at microscopic levels, making prediction of small-scale nitrous oxide (N 2 O) emissions in the field notoriously difficult. We assessed N 2 O+N 2 emissions from soils under maize (Zea mays L.), switchgrass (Panicum virgatum L.), and energy sorghum (Sorghum bicolor L.), three potential bioenergy crops in order to identify the importance of different N 2 O sources to microsite production, and relate N 2 O source differences to crop-associated differences in pore structure formation. The combination of isotopic surveys of N 2 O in the field during one growing season and X-ray computed tomography (CT) enabled us to link results from isotopic mappings to soil structural properties. Further, our methodology allowed us to evaluate the potential for in situ N 2 O suppression by biological nitrification inhibition (BNI) in energy sorghum. Our results demonstrated that the fraction of N 2 O originating from bacterial denitrification and reduction of N 2 O to N 2 is largely determined by the volume of particulate organic matter occluded within the soil matrix and the anaerobic soil volume. Bacterial denitrification was greater in switchgrass than in the annual crops, related to changes in pore structure caused by the coarse root system. This led to high N-loses through N 2 emissions in the switchgrass system throughout the season a novel finding given the lack of data in the literature for total denitrification. Isotopic mapping indicated no differences in N 2 O-fluxes or their source processes between maize and energy sorghum that could be associated with the release of BNI by the investigated sorghum variety. The results of this research show how differences in soil pore structures among cropping systems can determine both N 2 O production via denitrification and total denitrification N losses in situ.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2017

Substance P enhances proliferation and paracrine potential of adipose-derived stem cells in vitro

Stem cells have tremendous promise to treat intractable diseases. Notably, adipose-derived stem cells (ADSCs) are actively being investigated because of ease of sampling and high repopulation capacity in vitro. ADSCs can exert a therapeutic effect through differentiation and paracrine potential, and these actions have been proven in many diseases, including cutaneous and inflammatory diseases. Transplantation of ADSCs necessitates therapeutic quantities and thus, long term ex vivo culture of ADSCs. However, this procedure can impair the activity of ADSCs and provoke cellular senescence, leading to low efficacy in vivo. Accordingly, strategies to restore cellular activity and inhibit senescence of stem cells during ex vivo culture are needed for stem cell-based therapies. This study evaluated a potential supplementary role of Substance P (SP) in ADSC ex vivo culture. After confirming that the ADSC cell cycle was damaged by passage 6 (p6), ADSCs at p6 were cultured with SP, and their proliferation rates, cumulative cell numbers, cytokine profiles, and impact on T/endothelial cells were assessed. Long-term culture weakened proliferation ability and secretion of the cytokines, transforming growth factor-beta 1 (TGF-beta1), vascular endothelial growth factor (VEGF), and stromal cell derived factor-1 alpha (SDF-1alpha) in ADSCs. However, SP treatment reduced the population doubling time (PDT), enabling gain of a sufficient number of ADSCs at early passages. In addition, SP restored cytokine secretion, enhancing the ADSC-mediated paracrine effect on T cell and human umbilical vein endothelial cells (HUVECs). Taken together, these results suggest that SP can retain the therapeutic effect of ADSCs by elevating their proliferative and paracrine potential in ex vivo culture. - Highlights: • Long-term culture of ADSCs leads to cell senescence. • Paracrine potential of ADSC decreases as passage number increases. • SP enhances the weakened proliferation capacity of ADSCs. • SP stimulates cytokine secretion from ADSC with impaired paracrine potential.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2026

Task Sharing of Proton Incorporation in Vertically Aligned Nanocomposite Triple Conductors: Growth, Structure, and Surface Exchange Kinetics

As protonic ceramic electrolysis cells emerge for efficient H 2 production, there is a need to develop air electrode materials enabling fast, durable steam splitting and proton incorporation. Single-phase triple conductors may fail to satisfy the myriad performance/stability requirements, and their critical charge-carriers (holes, oxygen vacancies, and protons) are in competition, limiting their concentrations. Instead, we propose task-sharing, vertically aligned nanocomposites (VANs), comprising a proton conductor (BaZr 0.9 Y 0.1 O 3-δ ) and a redox-active mixed ionic electronic conductor (Ce 0.9 Pr 0.1 O 2-δ ), that may enable rapid proton surface exchange at the solid–gas interface and transport along the solid–solid heterointerfaces. We grew VANs by pulsed laser deposition and investigated the interplay between their processing conditions, structure, and proton and oxygen surface exchange kinetics. We varied the substrate temperature, laser repetition rate, laser fluence, and processing oxygen pressure. The crystallinity and phases were characterized by grazing-incidence X-ray diffraction, and the strain and structural order as a function of depth were evaluated by angle-dependent synchrotron X-ray pair distribution function analysis. To evaluate the potential for interdiffusion, the formation energies of substitutional defects were simulated with density functional theory. Corresponding structural analysis and elemental mapping were performed by scanning/transmission electron microscopy, energy-dispersive X-ray spectroscopy, and electron energy-loss spectroscopy, indicating distinct nanoscale compositional regions with a hierarchical structure embedded in individual VANs columns and minimal interdiffusion across a bilayer film. Proton and oxygen surface exchange coefficients (k H , k O ) and polarization resistances were evaluated by electrical and optical relaxations and impedance spectroscopy of VAN-incorporated protonic ceramic electrochemical cells, respectively, at 400–500 °C, demonstrating values comparable to some of the best-known triple and mixed conductors.

36 MATERIALS SCIENCE↗

NASA NTRS1979

Physical/chemical modeling for photovoltaic module life prediction

The paper presents a generalized methodology for identification and evaluation of potential degradation and failure of terrestrial photovoltaic encapsulation. Failure progression modeling and an interaction matrix are utilized to complement the conventional approach to failure degradation mode identification. Comparison of the predicted performance based on these models can produce: (1) constraints on system or component design, materials or operating conditions, (2) qualification (predicted satisfactory function), and (3) uncertainty. The approach has been applied to an investigation of an unexpected delamination failure; it is being used to evaluate thermomechanical interactions in photovoltaic modules and to study corrosion of contacts and interconnects.

Moacanin, J.↗

DOE OSTI2018

Multi-Faceted Approach to Evaluate Discharge Locations at a FUSRAP Site - 18421

Following the completion of a Soil and Groundwater Remedial Investigation by USACE at a FUSRAP site located in Nassau County, New York, groundwater data indicated the presence of contaminant source(s) that had not been identified. As a result, a targeted investigation was undertaken to understand how materials were handled and disposed of at a site located in Nassau County, Long Island, New York. The FUSRAP site is a 4.3-hectare (10.5-acre) site encompassing three parcels which had historically been utilized as a nuclear materials manufacturing facility (e.g., cores, slug, and fuel elements) for reactors used in both research and electric power generation in early 1950's until late 1960's; however, the targeted investigation was on the southern-most parcel known as the '70 Property' (the Site). The 70 Property contained a building that was used for atomic fuel-element manufacturing from 1958 until 1966 under license to the Atomic Energy Commission (AEC), and involved the use of natural, enriched, and depleted uranium as well as lesser amounts of thorium. The major contaminants of concern are tetrachloroethene, nickel, uranium and thorium. During the RI, significant sources of contamination were not found in Site soils despite records indicating that chemicals and radionuclides had been disposed of on the property. In addition, downgradient groundwater data indicated a source(s) on the 70 Property that could not be identified by known sources on other the other FUSRAP parcels or from adjacent sites. This conclusion was further supported following development of groundwater contaminant transport and flow models. The main objective of the targeted investigation was to evaluate the potential discharge points on the 70 Property that may have been utilized for liquids waste disposal. However, several challenges existed including 1) lack of building construction details; 2) historical changes to Site building and property; 3) the use of the Site by various tenants; and 4) the commingling of Site contaminants with impacts from multiple sources. To overcome these challenges, historic documents/reports with information about the handling and disposal of liquid wastes were reviewed to evaluate quantities, contents and locations of waste disposal. Thereafter, an investigation was undertaken that included geophysical surveys; pipe tracing and video inspection; in-situ smoke and water testing; installation of test trenches and soil borings; and, sampling sludge residuals, soils and water within the various drainage structures that were located. This paper describes the multi-faceted investigation approach that was utilized to overcome the challenges faced during the investigation as well as insights into the waste disposal practices of the time period and the findings of the investigation. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2023

Thermopile Energy Harvesting for Subsurface Wellbore Sensors (Final Report)

Robust in situ power harvesting underlies all efforts to enable downhole autonomous sensors for real-time and long-term monitoring of CO 2 plume movement and permeance, wellbore health, and induced seismicity. This project evaluated the potential use of downhole thermopile arrays, known as thermoelectric generators (TEGs), as power sources to charge sensors for in situ real-time, long-term data capture and transmission. Real-time downhole monitoring will enable “Big Data” techniques and machine learning, using massive amounts of continuous data from embedded sensors, to quantify short- and long-term stability and safety of enhanced oil recovery and/or commercial-scale geologic CO 2 storage. This project evaluated possible placement of the TEGs at two different wellbore locations: on the outside of the casing; or on the production tubing. TEGs convert heat flux to electrical power, and in the borehole environment, would convert heat flux into or out of the borehole into power for downhole sensors. Such heat flux would be driven by pumping of cold or hot fluids into the borehole—for instance, injecting supercritical CO 2 —creating a thermal pulse that could power the downhole sensors. Hence, wireless power generation could be accomplished with in situ TEG energy harvesting. This final report summarizes the project’s efforts that accomplished the creation of a fully operational thermopile field unit, including selection of materials, laboratory benchtop experiments and thermal-hydrologic modeling for design and optimization of the field-scale power generation test unit. Finally, the report describes the field unit that has been built and presents results of performance and survivability testing. The performance and survivability testing evaluated the following: 1) downhole power generation in response to a thermal gradient produced by pumping a heated fluid down a borehole and through the field unit; and 2) component survivability and operation at elevated temperature and pressure conditions representative of field conditions. The performance and survivability testing show that TEG arrays are viable for generating ample energy to power downhole sensors, although it is important to note that developing or connecting to sensors was beyond the scope of this project. This project’s accomplishments thus traversed from a low Technical Readiness Level (TRL) on fundamental concepts of the application and modeling to TRL-5 via testing of the fully integrated field unit for power generation in relevant environments. A fully issued United States Patent covers the wellbore power harvesting technology and applications developed by this project.

47 OTHER INSTRUMENTATION↗

DOE OSTI2020

Real-World Evaluation of National Energy Efficiency Potential of Cold Storage Evaporator Technology in the Context of Engine Start-Stop Systems

National concerns over energy consumption and emissions from the transportation sector have prompted regulatory agencies to implement aggressive fuel economy targets for light-duty vehicles through the U.S. National Highway Traffic Safety Administration/Environmental Protection Agency (EPA) Corporate Average Fuel Economy (CAFE) program. Automotive manufacturers have responded by bringing competitive technologies to market that maximize efficiency while meeting or exceeding consumer performance and comfort expectations. In a collaborative effort among Toyota Motor Corporation, Argonne National Laboratory (ANL), and the National Renewable Energy Laboratory (NREL), the real-world savings of one such technology is evaluated. A commercially available Toyota Highlander equipped with two-phase cold storage technology was tested at ANL’s chassis dynamometer testing facility. The cold storage technology maintains the thermal state of air-conditioning evaporators to enable longer and more frequent engine-off operation in vehicles equipped with start-stop functionality. Test results were analyzed and provided to NREL where a novel simulation framework was developed and calibrated to the test data. The vehicle model was then exercised over a large set of real-world drive cycle and ambient condition data to estimate national-level fuel economy benefits. Results indicate that the cold storage evaporator provided national fuel consumption reductions of 0.113% relative to a conventional evaporator in the same vehicle. In addition, when the cold storage evaporator engine stop/start was enabled for any temperature and the baseline was limited to the EPA menu, Start and Stop credit assumption of 27°C, a national fuel savings of 0.497% was found. Fuel savings resulted from a combination of extended engine-off duration during idle events and increased frequency of deceleration fuel cutoff, both enabled by the ability of the cold storage evaporator to maintain thermal state in situations where air conditioning is active.

DIRECT ENERGY CONVERSION↗

DOE OSTI2017

R1234yf and R1234ze(E) as low-GWP refrigerants for residential heat pump water heaters; Le R1234yf et le R1234ze(E) comme frigorigènes à faible GWP pour des chauffe-eau domestiques à pompe à chaleur

Owing to the growing concerns about the relatively high global warming potential (GWP) of current refrigerants, a serious effort is currently in progress to find lower-GWP substitutes. The hydrofluoroolefin (HFO)-based refrigerants R1234yf and R1234ze(E) are being considered for use in multiple heating, ventilation, air conditioning, and refrigeration applications because of their very low GWP. A study was conducted to model a residential heat pump water heater using these HFOs. A system model was calibrated using experimental data and the calibrated model was used to evaluate the potential of HFOs to replace R134a. A series of parametric analyses were used to investigate the impacts of condenser wrap pattern, condenser tube size, evaporator size, and heat loss factor from the storage tank. It has been shown that both R1234yf and R1234ze(E) can be substituted for R134a with comparable performance and no substantial modifications to the original system. Finally, this study presents a detailed feasibility analysis for successful replacement of high-GWP refrigerants with low-GWP refrigerants with acceptable performance.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

NASA NTRS1996

Independent Verification and Validation of Complex User Interfaces: A Human Factors Approach

The Usability Testing and Analysis Facility (UTAF) at the NASA Johnson Space Center has identified and evaluated a potential automated software interface inspection tool capable of assessing the degree to which space-related critical and high-risk software system user interfaces meet objective human factors standards across each NASA program and project. Testing consisted of two distinct phases. Phase 1 compared analysis times and similarity of results for the automated tool and for human-computer interface (HCI) experts. In Phase 2, HCI experts critiqued the prototype tool's user interface. Based on this evaluation, it appears that a more fully developed version of the tool will be a promising complement to a human factors-oriented independent verification and validation (IV&V) process.

Whitmore, Mihriban↗

DOE OSTI2019

Environmental and Operational Performance of CO2-EOR as a CCUS Technology: A Cranfield Example with Dynamic LCA Considerations

This study evaluates the potential of carbon dioxide-enhanced oil recovery (CO2-EOR) to reduce greenhouse gas emissions without compromising oil production goals. A novel, dynamic carbon lifecycle analysis (d-LCA) was developed and used to understand the evolution of the environmental impact (CO2 emissions) and mitigation (geologic CO2 storage) associated with an expanded carbon capture, utilization and storage (CCUS) system, from start to closure of operations. EOR operational performance was assessed through CO2 utilization rates, which relate usage of CO2 to oil production. Because field operational strategies have a significant impact on reservoir engineering parameters that affect both CO2 storage and oil production (e.g., sweep efficiency, flood conformance, fluid saturation distribution), we conducted a scenario analysis that assessed the operational and environmental performance of four common and novel CO2-EOR field development strategies. Each scenario was evaluated with and without stacked saline carbon storage, an EOR/storage combination strategy where excess CO2 from the recycling facility is injected into an underlying saline aquifer for long-term carbon storage. The dynamic interplay between operational and environmental performance formed the basis of our CCUS technology analysis. The results showed that all CO2-EOR evaluated scenarios start operating with a negative carbon footprint and, years into the project, transitioned into operating with a positive carbon footprint. The transition points were significantly different in each scenario. Water-alternating-gas (WAG) was identified as the CO2 injection strategy with the highest potential to co-optimize EOR and carbon storage goals. The results provide an understanding of the evolution of the system’s net carbon balance in all four field development strategies studied. The environmental performance can be significantly improved with stacked storage, where a negative carbon footprint can be maintained throughout the life of the operation in most of the injection scenarios modelled. This information will be useful to CO2-EOR operators seeking value in storing more CO2 through a carbon credit program (e.g., the 45Q carbon credit program in the USA). Most importantly, this study serves as confirmation that CO2-EOR can be operationally designed to both enhance oil production and reduce greenhouse gas emissions into the atmosphere.

58 GEOSCIENCES↗

DOE OSTI2025

The Dynamic Networks Experiments: Virtual Experiments to Quantify Gains in Nuclear Explosion Monitoring

We describe an ongoing series of virtual experiments conducted collaboratively by four United States National Laboratories: Sandia National Laboratories, Los Alamos National Laboratory, Lawrence Livermore National Laboratory, and Pacific Northwest National Laboratory. These Dynamic Network Experiments (DNEs) provide an experimental framework to evaluate the potential impact of new research tools on nuclear explosion monitoring. The second DNE (DNE2), completed in 2024, exploited waveform data (seismic, infrasound, and electromagnetic) that was recorded by multi-modal sensors within and near the Nevada National Security Site and synthetic radionuclide signatures over multiple time periods. During the execution of DNE2, we processed and analyzed data through a multi-stage event processing pipeline that ingested raw data, performed quality control, detected signals, built events from these signals, located these events, and characterized the events’ source types and sizes. For each stage and over the entire event processing pipeline, we evaluated performance changes by comparing the performance of new data processing methods, models, and algorithms against a baseline. We also performed an additional execution phase to assess event processing pipeline function, speed, and efficiency against that of an expert analyst, including computational and manual efforts. Finally, we assessed the impact and effort of modern computing infrastructure on the monitoring pipeline. This paper describes key elements of the DNEs, from formulation through execution, as demonstrated in DNE2. The DNEs introduce several novel concepts to quantitatively measure the potential impact of new methods on explosion monitoring, including the collaborative design of multi-modal datasets, performance and logistical metrics, and integrated analyses.

42 ENGINEERING↗

NASA NTRS2018

Multi-Operator Multi-UAV (MOMU) Control: Exploring the Influence of Sensor Tools and Playbook Task Delegation

New concepts of operations for Unmanned Aerial Vehicles (UAVs) will require a change from the current 2:1 operator to vehicle crew configuration. One particular control paradigm, largely driven by logistics, manpower, and training burdens, as well as the desire to force multiply, involves a single operator simultaneously managing multiple UAVs. This mode of operations has shown to significantly increase cognitive workload and decrease situation awareness, as operators are required to simultaneously attend to multiple sources of information. One potential way to mitigate potential drawbacks of multi-vehicle control by a single operator is to migrate to a multi-operator multi-UAV (MOMU) crew configuration, whereby M operators control N (> M) vehicles. This type of crew configuration can be organized in several ways to dynamically manage cognitive workload, match operator qualifications and skills to mission requirements, increase utilization of available assets, and thereby achieve maximum force multiplication. The present experiment examined task performance in a simulated MOMU environment and evaluated the potential benefits of sensor management aids ("Tools") as well as integrated sensor and flight automation ("Plays") compared to a fully manual condition ("Manual"). Tools support the operator by facilitating rapid understanding and management of sensor information, while the Plays support the operator by offloading/automating subtasks. Six pairs of participants were recruited for this study and tasked with sharing a pool of UAVs in order to conduct reconnaissance, surveillance, and target acquisition (RSTA) missions in adjacent Areas of Operation (AOs). Participants were given four tasks to accomplish, in order of priority: 1) prosecute High Value Targets (HVTs); 2) identify / track targets (military vehicles); 3) identify / mark civilian vehicles; and 4) respond to chat messages. Performance on the mission tasks was measured in terms of accuracy and reaction time. A composite mission score was also calculated using a payoff matrix that weighted each task according to priority. The results indicate that Playbook demonstrated better performance overall with higher accuracy rates and the highest composite score compared to Tools and Manual. The implications of these results to supporting future MOMU concepts of operations is discussed.

Playbook↗

NASA NTRS2020

Investigation of a Helicopter Individual Blade Control (IBC) System in Two Full-Scale Wind Tunnel Tests: Volume I

This report presents the data acquired during the testing of an individual blade control (IBC) system on a full-scale helicopter rotor in two test entries in the NASA Ames 40- by 80-Foot Wind Tunnel. The objective of these investigations was to evaluate the potential benefits of using IBC to improve rotor performance, reduce blade vortex interaction (BVI) noise, and alleviate helicopter vibrations. The wind tunnel tests were an international, collaborative effort between NASA, the U.S. Army Aeroflightdynamics Directorate, ZF Luftfahrttechnik GmbH, Eurocopter Deutschland GmbH, and the German Aerospace Laboratory (DLR). They were conducted as a task of the U.S./German Memorandum of Understanding (MOU) on Helicopter Aeromechanics. The IBC tests were performed using a full-scale BO-105 helicopter rotor mounted to the NASA/U.S. Army Rotor Test Apparatus (RTA). The first test, performed in 1993, was the first full-scale wind tunnel test to explore the effects of an IBC system on rotor vibration, noise, and performance. In this test, the pitch links of the rotor were replaced by servo-actuators. The servo-actuators and IBC control system were designed and manufactured by ZF Luftfahrttechnik GmbH. This control system allowed the pitch of each rotor blade to be changed independently of the other blades. The IBC inputs had large effects on the hub vibrations and BVI noise. However, the rotor hub moments were not retrimmed with each new IBC input. This resulted in an out-of-trim rotor configuration. The same IBC system was used in the second IBC test performed in 1994. This test more carefully investigated the potential of IBC to simultaneously reduce noise and vibration and also investigated the effect of IBC on rotor performance in high-speed-cruise flight. In the 1994 test, the hub moment and rotor thrust were readjusted to maintain rotor trim as the IBC inputs were applied. For this reason, the data taken from the second test are considered to be more accurate, except for some unique IBC input combinations not repeated in the second test. IBC controls that were evaluated were single-frequency inputs from 2/rev to 6/rev and multi-harmonic combinations of these frequencies to form pulses, wavelets, and doublets. Extensive data were acquired for each IBC data point. These data included rotor performance, average and time-varying hub loads, rotor blade bending loads, control system loads, inboard and outboard blade pitch motions, and BVI noise data. The rotor balance hub force and moment data included the mean values, half-peak-to-peak values, and sine/cosine harmonics up to the 20th rotor harmonic. The time history and averaged Fourier spectrum for each measurement are available electronically from NASA Ames Research Center. The data indicate that significant reduction in both BVI noise and hub vibration can be obtained using IBC. The 2/rev input produced the best single-frequency results. At a typical descent flight condition, 2/rev IBC combined with other IBC harmonics reduced the BVI noise up to 12 dB (85 percent) at some microphone locations. At the same time, this input could also reduce the dominant 4/rev vibratory hub loads by up to 75 percent. The data also show that performance improvements of up to 7 percent were obtained using 2/rev IBC at high-speed forward flight conditions. An analysis of the hydraulic power requirements for BVI noise suppression, vibration reduction, and rotor performance improvement is included in this report. This analysis shows that the power required by the IBC system is negligible at low-speed flight conditions, and that a net gain of 3 percent of rotor horsepower can be achieved at high-speed flight conditions.

Investigation↗

DOE OSTI2017

Floodplain and Wetland Assessment for the Mortandad Wetland Enhancement and the DP Dissipater Projects at Los Alamos National Laboratory

This floodplain and wetland assessment was prepared in accordance with 10 Code of Federal Regulations (CFR) 1022 Compliance with Floodplain and Wetland Environmental Review Requirements, which was promulgated to implement the U.S. Department of Energy (DOE) requirements under Executive Order 11988 Floodplain Management and Executive Order 11990 Wetlands Protection. According to 10 CFR 1022, a 100-year floodplain is defined as “the lowlands adjoining inland and coastal waters and relatively flat areas and flood prone areas of offshore islands” and a wetland is defined as “an area that is inundated or saturated by surface or groundwater at a frequency and duration sufficient to support, and that under normal circumstances does support, a prevalence of vegetation typically adapted for life in saturated soil conditions, including swamps, marshes, bogs, and similar areas.” In this action, DOE is proposing two projects to improve wetland and floodplain function at Los Alamos National Laboratory (LANL). The proposed work will comply with corrective action requirements under the Settlement Agreement and Stipulated Final Compliance Order (Settlement Agreement)1 Number HWB-14-20. The first project is located in Technical Areas (TA)-03 in upper Mortandad Canyon. The upper Mortandad wetlands have existing stormwater controls that need to be rehabilitated. Head-cut formation is occurring at the downstream portion of the wetland. This project will repair damages to the wetland and reduce the future erosion potential. The second project is located in TA-21 in Delta Prime (DP) Canyon. The intent of the DP Dissipater Project in DP Canyon is to install stormwater control structures in DP Canyon to retain low channel flows and reduce downstream sediment transport as well as peak flows during low and moderate storm events. Due to increased erosion, the stream bank in this area has unstable vertical walls within the stream channel. The DOE prepared this floodplain and wetland assessment to evaluate the potential impacts of implementing the proposed actions within the wetland and floodplain, as required by 10 CFR 1022.

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