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FY19 Report for Instrumentation Development for the Transient Testing Program

This report details the technical activities and accomplishment carried out under funding from the Department of Energy (DOE) Nuclear Technology Research and Development (NTRD) program for in-pile instrumentation supporting the transient testing program in FY19. These activities were performed in support of cross-cutting transient testing experiment objectives. The purpose of this report is to provide a summary of key technical work, of particular interest to nuclear irradiation test experimenters and in-pile instrumentation engineers. During FY19, development activities are focused on deployment of devices to perform online measurement of neutron flux, temperature, and mechanical behaviors in nuclear fuels experiments. Specifically, these R&D activities include in-pile investigations at the Transient Reactor Test (TREAT) facility throughout the year. Other in-pile instrumentation R&D activities are being carried out under other DOE programs, which may be recognized but not the focus of this document. A brief summary of activities and accomplishments is first provided for each major activity. More detailed summaries are presented in appendices.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Neutronics Analysis of TREAT Multi-SERTTA Calibration Test Vehicle (Multi-SERTTA CAL)

Transient testing is a necessary step in the performance evaluation of Accident Tolerant Fuels (ATF) developed as part of the Fuel Cycle Research and Development Advanced Fuels Campaign initiated and supported by the United States Department of Energy (DOE-NE). These advanced fuels are expected to be used in future reactors or replace the current fuel design used in existing power reactors for enhanced performance and safety. Upon completion of a process proscribed by the National Environmental Policy Act, the Transient Reactor Test (TREAT) facility, located at Idaho National Laboratory (INL), was chosen by DOE-NE to provide the desired specialized testing. TREAT has successfully operated from start-up in 1959 to 1994 when it was placed on operational stand-by. Careful preparations are being made for operational readiness and TREAT is projected to resume testing no later than 2018. Past TREAT testing primarily focused on sodium-cooled reactor fuels (SRF). Test vehicle designs varied to accommodate testing needs ranging from separate effects tests to integral tests approaching simulation of actual reactor environment conditions including forced convection cooling. The current focus on light water reactor (LWR) ATF requires design of new experiment vehicles to accommodate the water/steam environment and associated complexities regarding desired energy deposition into the specimen and proper containment. The first set of experiments in TREAT restart is expected to be conducted with the Multi-SERTTA (Static Environment Rodlet Transient Test Apparatuses). Difficult to quantify and calculate integral and time dependent effects inherent in transient testing limit predictive modeling capability; therefore, calibration testing in TREAT prior to the actual experiment is necessary to empirically determine the effectiveness of core-to-specimen power coupling in order to achieve the desired energy deposition into the test specimen during a nuclear power transient. This has been done in the past, in part, by evaluating the difference in energy deposition into dosimeter wires subjected to various TREAT time dependent power conditions. These calibration tests were typically conducted in a test vehicle neutronically similar to the actual test vehicle, but more simplistic in design in order to quickly retrieve and analyze dosimeter wires and minimize containment structure costs due to several trials. Prior calibration testing for SRF experiments could be conducted without coolant as sodium has no notable neutronic effect on the core-to-specimen power coupling factor (PCF). Such is not the case with LWR fuel where water serves as both moderator and coolant. This presents a design challenge as the calibration test vehicle must retain heated, high-pressure water to preserve neutronic equivalence representative of near prototypic reactor conditions while allowing for quick retrieval of dosimeters. The solution to this challenge comes in the form of a thin walled dry well positioned through the center of the basic Multi-SERTTA design. Test vehicle reactivity worth and PCF are two important factors with respect to ascertainment of neutronic equivalence. Similarity in test vehicle reactivity worth is desired to avoid the need to change operational core rod positions in TREAT which could significantly alter neutron flux distribution and consequently power distribution throughout the core and into the test specimen. The geometry and composition of various materials within the experiment containment structure can also significantly alter the quality of neutron signal delivery from the core to the test specimen. Introduction of an Inconel tube, albeit very thin, is expected to impact PCF. Simple modifications to the CAL design may compensate for the anticipated change. Evaluation of these factors and proposed modifications through neutronics analysis serves to inform experiment design and is a valuable tool towards achieving the optimal CAL design.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Embedded I&C for Extreme Environments

This project uses embedded instrumentation and control (I&C) technologies to demonstrate potential performance gains of nuclear power plant components in extreme environments. Extreme environments include high temperature, radiation, high pressure, high vibration, and high EMI conditions. For extreme environments, performance gains arise from moment-to-moment sensing of local variables and immediate application of local feedback control. Planning for embedding I&C during early system design phases contrasts with the traditional, serial design approach that incorporates minimal I&C after mechanical and electrical design is complete. The demonstration application involves the development and control of a novel, proof-of-concept motor/pump design. The motor and pump combination operate within the fluid environment, eliminating the need for rotating seals. Actively controlled magnetic bearings also replace failure-prone mechanical contact bearings that typically suspend rotating components. Such as design has the potential to significantly enhance the reliability and life of the pumping system and would not be possible without embedded I&C.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Development of a Research Reactor Protocol for Neutron Multiplication Measurements

Establishing a protocol for measurements on research reactors is the next step in advanced subcritical neutron multiplication inference measurements. Such measurements can help identify deficiencies and quantify uncertainties in nuclear data and validate predictive Monte Carlo radiation transport simulation capabilities related to subcritical neutron multiplication inference techniques. This work expands on previous benchmark-quality efforts performed at the National Criticality Experiments Research Center (NCERC) located in Nevada, including subcritical experiments with a 4.5-kg {alpha}-phase plutonium sphere surrounded by copper, tungsten and nickel. Evaluations of the nickel and tungsten measurements have both been accepted into the International Criticality Safety Benchmark Evaluation Project (ICSBEP) Handbook. The nickel benchmark was the first ICSBEP-accepted evaluation of measurements using the Feynman Variance-to-Mean method based on the Hage-Cifarelli formulism, and was the culmination of many years of subcritical experiment research. To help establish a protocol for research reactor-based subcritical measurements, a series of Critical and Subcritical {Phi}-Power Experiments at Rensselaer (CaSPER) have been designed. This neutron multiplication measurement series will be executed at the Rensselaer Polytechnic Institute Walthousen Reactor Critical Facility (RPI-RCF) in upstate New York. The RPI reactor facility can provide benchmark-quality integral experimental configurations where different reactivity states can be achieved by varying the control rod height/water height in the reactor. The diversity of achievable configurations are also unique in contrast to previous subcritical benchmark measurements in that they are spatially complex, involve different materials (fuel, moderator), and are characterized by system-specific neutron cross section sensitivities (various energy ranges and neutron reaction contributions). It is worth noting that previous proof-of-concept subcritical measurements have been performed on thermal systems at NCERC, at a variety of reactivity states by separation distance, yet it was not possible to know the reactivity of various configurations accurately for benchmarking (there are no control rod worth curves as there are no control rods). (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Overview and Recommendations for Cyber Risk Assessment in Nuclear Power Plants

Digital instrumentation and control (I&C) systems are being deployed in nuclear power plants (NPPs) for both existing and advanced reactor designs. As I&C systems become more digitized to allow features like near autonomous control and remote operation, they introduce greater cyber risk to NPPs. Cyberattacks targeting industrial control systems (ICSs) are growing in both qualities and capabilities, which indicates that cybersecurity needs to be an integral part of risk assessment in the industry. Although there are some risk assessment methods in traditional information technology (IT) cybersecurity, the differences between IT and ICS cybersecurity make it infeasible to apply these risk assessment methods directly to ICSs. Some research has focused on risk assessment methods for ICSs, but few studies focus on applications to NPPs. Ideal risk frameworks for the nuclear industry are dynamic and account for system dependencies; this survey review focuses on such risk assessment methods both in and outside the nuclear field. In this article, the major challenges in cybersecurity risk assessment research are pointed out, and further research suggestions and considerations for cyber risk assessment in I&C systems are identified.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Detailed Analysis of RUS Insertion Experiment and Scoping Studies for Performing Next Experiment using an Enriched Fuel Sample

Microstructure evolution due to irradiation in a nuclear reactor can have a dramatic effect on material properties. A better understanding of this evolution is necessary for developing improved nuclear fuels and materials. The ability to measure such changes in real time is extremely challenging due to high temperatures, high radiation fields, and limited access of the reactor environment. Through carefully designed experiments, measurement of elastic properties can be tied directly to microstructure. We present an instrument that has been developed to monitor in-pile changes in grain microstructure. The measurement approach involves optically exciting and detecting flexural waves in a thin cantilever beam. An instrument capsule based on this technique was fabricated and underwent an irradiation test in the TREAT reactor in May 2019. Analyses of the test results are presented in this report. Scoping studies on the expected impact of radiation on similar tests are also presented.

36 MATERIALS SCIENCE↗

THE CALCULATION OF BURNABLE POISON CORRECTION FACTORS FOR PWR FRESH FUEL ACTIVE COLLAR MEASUREMENTS

Verification of commercial low enriched uranium light water reactor fuel takes place at the fuel fabrication facility as part of the overall international nuclear safeguards solution to the civilian use of nuclear technology. The fissile mass per unit length is determined nondestructively by active neutron coincidence counting using a neutron collar. A collar comprises four slabs of high density polyethylene that surround the assembly. Three of the slabs contain {sup 3}He filled proportional counters to detect time correlated fission neutrons induced by an AmLi source placed in the fourth slab. Historically, the response of a particular collar design to a particular fuel assembly type has been established by careful cross-calibration to experimental absolute calibrations. Traceability exists to sources and materials held at Los Alamos National Laboratory for over 35 years. This simple yet powerful approach has ensured consistency of application. Since the 1980's there has been a steady improvement in fuel performance. The trend has been to higher burn up. This requires the use of both higher initial enrichment and greater concentrations of burnable poisons. The original analytical relationships to correct for varying fuel composition are consequently being challenged because the experimental basis for them made use of fuels of lower enrichment and lower poison content than is in use today and is envisioned for use in the near term. Thus a reassessment of the correction factors is needed. Experimental reassessment is expensive and time consuming given the great variation between fuel assemblies in circulation. Fortunately current modeling methods enable relative response functions to be calculated with high accuracy. Hence modeling provides a more convenient and cost effective means to derive correction factors which are fit for purpose with confidence. In this work we use the Monte Carlo code MCNPX with neutron coincidence tallies to calculate the influence of Gd{sub 2}O{sub 3} burnable poison on the measurement of fresh pressurized water reactor fuel. To empirically determine the response function over the range of historical and future use we have considered enrichments up to 5 wt% {sup 235}U/{sup tot}U and Gd weight fractions of up to 10 % Gd/UO{sub 2}. Parameterized correction factors are presented.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Investigation of similarity metrics for simulation based scaling analysis

Scaling analysis is a technique for characterizing degree of similarity between processes to occur in a real prototypic system and those to occur in its reduced scale (experimental) analog. In the context of nuclear reactor thermal-hydraulics and safety, scaling analysis is instrumental in assessing the applicability of data obtained from a scaled test facility for calibration of models and validation of simulation codes. Quantification of scale-related distortions is the key element in scaling analysis. In this work, we examine an approach for scaling analysis using computer simulation codes. Similarity analysis using information-theoretic approach is performed by comparing performance of experiment and application to variation of system conditions. Three different information theoretic measures namely mutual information, Kullback-Leibler divergence and overlap coefficient are selected for their potential use as metric for similarity analysis. We test the metrics by comparing them against physics-based scaling ratios, which are well known in fundamental thermal-hydraulic processes. In this exploratory analysis, a case of pressure drop of a steady-state flow through a channel is employed to test the proposed approach. It was found that in the absence of model uncertainties, mutual information serve as an effective measure of the scale effects present in the experiment. However, model uncertainty can significantly impact the quality of similarity analysis. Our analysis indicates that model uncertainties can have significant impact on the information theoretic metrics used for scaling analysis. Furthermore, if the model uncertainties exceeds beyond a critical value, the scale effect present in the experiment cannot be adequately evaluated. (authors)

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Integrated emergency control board including design extended conditions for Krsko NPP - 297

In the aim of implementing post-Fukushima safety measures, Krsko Nuclear Power Plant is developing a Safety Upgrade Program. Krsko NPP is upgrading the remote shutdown capabilities and implementing ways to prevent and mitigate the consequences of potential Severe Accidents. This modification enhances remote shutdown capabilities of the plant to prevent potential severe accidents and improve the ways to mitigate their consequences. Within the set of plant design modifications, addressed the design, construction, and commissioning, of a new Emergency Control Room (EMCB. Tecnatom is the responsible of the design modification of the plant together with Idom, that participates with Tecnatom in the project as a joint venture, who provides a new set of field instrumentation, including its design and the corresponding wiring. EMCB integrates Human- System Interface throughout centralizing capabilities to safety shutdown and cooldown the plant as well as to control the new Design Extension Systems. The process relies on a Human Factors Engineering (HFE) analysis applying a specific methodology based on NUREG-0711 . Tecnatom has developed a specific HFE Program Management Plan to proceed with the analysis in a documented, traceable and reliable way. HFE activities ends with an Integrated System Validation in the actual full scope simulator involving MCR crews. This paper describes different phases of the project, the integrated schedule between HFE and I and C activities, benefits of upgrading main and emergency control rooms beyond design bases and addresses Tecnatom lessons learned obtained during the project execution. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Developing a Human Factors Engineering Program Plan and End State Vision to Support Full Nuclear Power Plant Modernization

The Light Water Reactor Sustainability (LWRS) Program, which is sponsored by the United States (U.S.) Department of Energy (DOE), conducts research and development (R&D) to establish the technical bases to sustain U.S. nuclear assets. One area in the LWRS program is the Plant Modernization pathway, which includes human factors R&D, human factors engineering (HFE), and ergonomics. LWRS program researchers in this pathway conduct targeted R&D to address aging and reliability concerns with the legacy instrumentation and control (I&C) and related information systems in commercial nuclear power plants (NPPs). One key aspect of this pathway is to develop a strategy for full nuclear plant modernization, which previous LWRS plant modernization milestone reports have begun to describe. To further support this comprehensive plan and vision for full plant modernization, additional details need to be further developed. In particular, a core aspect of a strategy for full nuclear plant modernization is an HFE program plan and an end state vision for plant modernization that is well-integrated with both 1) a technically defensible approach to migrating the existing, mostly analog I&C infrastructure to a digital I&C infrastructure, and 2) a valid business case methodology to cost-justify the modernization activity. Thus, the purpose of this LWRS R&D activity and milestone report is threefold. First, the report provides guidance for operating commercial NPPs to support their development and evaluation of an HFE program management plan (HFE PMP) and an end state vision for plant modernization. The report presents best practices and lessons learned related to HFE PMPs based on MCR modifications in which analog systems were replaced by digital I&C systems. Second, the report summarizes the rationale for full digital I&C integration, highlights a number of factors that are critical to consider, and describes how HFE should merge with full digital I&C integration. Finally, the report summarizes and integrates the economic factors that must be considered to cost-justify HFE involvement in plant modernization.

99 GENERAL AND MISCELLANEOUS↗

A qualitative assessment of current CCF guidance based on a review of safety system digital implementation changes with evolving technology - 148

This paper is a summary of a study performed in support of the US Nuclear Regulatory Commission (NRC) to evaluate current policy on software common-cause failure (CCF). The study reported in this paper is one of several that contributed to the technical basis to inform NRC staff. The study first reviewed policies and assessment guidance as discussed in the Staff Requirements Memorandum to the Secretary of the Commission, Office of the NRC (SECY) 93-087, Policy, Technical, and Licensing Issues Pertaining to Evolutionary and Advanced Light Water Reactor (ALWR) Designs, and Branch Technical Position (BTP) 7-19, Guidance on Evaluation of Defense-in-Depth and Diversity in Digital Computer-Based Instrumentation and Control Systems, as well as Chapter 7, 'Instrumentation and Controls', in NUREG-0800, Standard Review Plan for Review of Safety Analysis Reports for Nuclear Power Plants. The study then examined instrumentation and controls (I and C) technology implementations in nuclear power plants in the light of current CCF guidance. The intent was to assess whether the current position on CCF remains appropriate given the evolutions in digital safety system implementations and, if gaps in the guidance were found, to provide recommendations as to how these gaps could be closed. The methodology adopted was to review the vendors' technology and software implementation processes for digital safety systems as technology evolved. The following three representative safety systems were selected to provide illustrative examples: - Eagle 21 was selected to represent vintage microprocessor-based technology used from the 1980's to mid-1990's, - TELEPERM XS (TXS) was selected to represent second generation microprocessor-based technology used from the mid-1990's to the 2000's, and - The advanced logic system (ALS) was selected to represent the latest trend of using technology based on field programmable gate arrays (FPGAs). Technology implementations were reviewed in light of the basic premise of the NRC in BTP 7-19 (Revision 6), that software-based or software-logic-based digital system development errors are a credible source of CCF and therefore are susceptible to CCF because identical copies of the software-based logic and architecture are present in redundant divisions of safety-related systems. BTP 7-19 categorizes firmware and logic developed from software-based development systems all under software. (authors)

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Sensitive Resources Assessment and Forest Analysis for the Proposed Versatile Test Reactor, Oak Ridge, Tennessee

The US Department of Energy’s (DOE’s) Oak Ridge National Laboratory (ORNL) is a leading institution in advanced materials, supercomputing, neutrons, and nuclear science. As a research laboratory managed by UT-Battelle, LLC for DOE, ORNL has national priorities in energy, security, and scientific discovery that necessitate facility improvements and expansions. DOE is also committed to environmental stewardship. The laboratory is located on the ~32,000-acre (~13,000-ha) Oak Ridge Reservation (ORR), much of which is categorized as a National Environmental Research Park (NERP) and a state Wildlife Management Area. DOE works with the Tennessee Wildlife Resources Agency (TWRA), Tennessee Department of Environment and Conservation (TDEC), US Fish and Wildlife Service (USFWS), US Department of Agriculture, and other agencies to serve as an effective steward of the ORR. Accordingly, project managers must conform to environmental regulations, agreements, and policies at the federal, state, and institutional levels. Per 40 CFR (Code of Federal Regulations) 1508.14, potential effects on research and science education also represent potential effects of federal actions on the NERP, and impacts on, e.g., deer harvest, must be considered on the Oak Ridge Wildlife Management Area when other aspects of the human environment are affected. The United States currently has no fast neutron testing capability to support advanced nuclear research and development. The proposed Versatile Test Reactor (VTR) will take advantage of current investments by the US government and private industry in nuclear reactors to expedite the design and construction process, using proven technology to create a world-class scientific infrastructure. The VTR will take advantage of fast neutrons provided by this proven technology, along with a capability to rapidly insert, conduct, and remove state-of-the-art experiments. An advantage of the VTR is that it can support future innovations in experimental capabilities without modifying the facility. The VTR will support progress in a variety of science and technology areas, including testing and qualification of advanced reactor fuels; testing and qualification of innovative structural materials; testing of innovative components and instruments; validation of advanced modeling and simulation tools; and versatility for future technical missions. Through proven technology, the VTR can take advantage of existing reactor designs and operating experience to reduce the risk, cost, and time for design and construction. The top available resources of DOE laboratories, industry, and universities will be used to expedite reactor design and construction toward developing the scientific infrastructure that affords a strong testing capability that can be sustained over many years. This report summarizes current knowledge of natural and cultural resources primarily within the VTR construction area. At the time of this report, the proposed VTR site design includes a construction area of ~150.4 acres (~69.9 ha), which contains an ~51.3-acre (~20.8-ha) operations area, located within forested natural areas of the ORR. The primary goal of the work presented here was to evaluate potential effects on sensitive resources that might result from development and construction activities associated with VTR. In addition to on-the-ground surveys during spring and summer 2020 by the ORNL Natural Resources Management Program and Aquatic Ecology Group staff, this report makes use of historical (pre-1995) and contemporary (1995 to present) data from additional confirmed sources (e.g., TDEC). Likewise, forest conditions were compiled from a 2011 forest inventory and supplemented with limited ground observations in 2020. The individuals who obtained and compiled the data presented here are familiar with and routinely assess sensitive resources on the ORR. Anyone who references this report must consider that the timing of surveys did not permit a complete delineation of the resources that will be affected. If the VTR project proceeds, additional surveys will be required to account for the seasonal patterns of various threatened and endangered species. Data deficiencies and potential resources that likely went undetected are indicated where possible. Accordingly, this report should facilitate more environmentally sound decisions during planning and 2 development of the VTR site, provide a foundation for further assessment of sensitive and cultural resources, and help project managers better address regulatory guidance and DOE policies on sustainable development in compliance with, for example, the US Endangered Species Act (ESA), Migratory Bird Treaty Act (MBTA), Tennessee Rare Plant Protection and Conservation Act of 1985, Tennessee Nongame and Endangered or Threatened Wildlife Species Conservation Act of 1974, several federal and state regulations regarding aquatic resource protection, and site-specific policies as outlined in various ORR management plans developed by ORNL and TWRA for DOE.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

PARTITIONING AND TRANSMUTATION OF USED NUCLEAR FUEL IN SUPPORT OF GEOLOGICAL WASTE DISPOSAL

Nuclear energy is a low-carbon technology that generates bulk baseload electricity and supports long-lasting eco-friendly sustainability goals. However, it still faces challenges, such as the securing and managing of long-lived nuclear actinides and fission products—most notably the used fuel, which is considered high-level waste (HLW). Direct geological waste disposal would be the most economical option for HLW but requires highly qualified sites whose geophysical behavior will remain stable for 10,000 years. Partitioning and transmutation (P&T) of used fuel reduces radioactivity and decay heat generation, enabling efficient geological waste disposal. P&T research and development, along with the prospects of P&T techniques such as wet/dry separation and accelerator-driven systems, were reviewed to identify critical needs that must be met to foster their successful implementation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

TRANSPORTATION CONSIDERATIONS FOR USED FUEL AND ADVANCED NUCLEAR ENERGY TECHNOLOGIES

This study focuses on requirements and challenges pertaining to advanced transportable nuclear energy systems, which are currently in development and feature varying degrees of mobility. These reactors mostly use high-assay low-enriched uranium (HALEU) fuel, and only limited refueling is required during their lifecycles. Due to the smaller source terms, higher burnup fuel, and potentially higher thermal efficiency involved, the waste inventory will be less than that generated by conventional light-water reactors. However, the relevant regulatory requirements must be met when transporting HALEU fuel (whether fresh or used) inside the reactor vessel—mainly the fuel material transportation, siting, and physical protection requirements outlined in US Nuclear Regulatory Commission (NRC) regulations 10 CFR 71 and 73. Spent nuclear fuel (SNF), as well as irradiated fuel (used during any interval of reactor operation), contains highly radioactive materials that generate heat and necessitate special precautions during transportation. This study addresses the challenges that this incurs, and outlines potential solutions.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Instrument development continues in Oak Ridge

Peer review panels composed of 80 external scientists recently visited Oak Ridge National Laboratory (ORNL) to review almost 700 proposals for experiments on 23 instruments at the Spallation Neutron Source (SNS) and High Flux Isotope Reactor (HFIR). These were proposed for the time period from January-June 2012. About 40% of the proposals were approved for beam time and 20% were placed on an alternate list if time becomes available. The Hybrid Spectrometer HYSPEC at SNS began its commissioning in September 2011. HYSPEC is otpimized for studying low energy dynamics in single-crystal samples using a broad variety of sample environments, and is equipped with a polarization analysis capability. It is expected to be available for users on a limited basis in the second half of 2012. The detector tank of CORELLI has been installed on beamline 9 at SNS. Now that the tank is in place, banks of neutron detectors and boron carbide shielding will be installed around the interior. CORELLI is optimized to probe complex disorder in crystalline materials through diffuse scattering from single-crystal samples. It will begin commissioning in 2014. CORELLI is one of four instruments being developed under the SING II (SNS Instruments Next Generation II) project. The others are the Macromolecular Neutron Diffractometer (MANDI), the Vibrational Spectrometer (VISION, scheduled to begin commissioning in 2012), and the Time of Flight Ultra Small Angle Neutron Scattering Instrument (TOF-USANS). The single crystal neutron diffractometer IMAGINE, was deliverd to HFIR in October 2011. Preliminary testing has been carried out. IMAGINE will provide atomic resolution information on chemical, organic, metallo-organic and protein single crystals that will enable their chemical, physical and biological structure and function to be understood. This instrument will benefit scientists with interests in pharmaceuticals, minerals and other inorganic crystals, small molecules, molecular organo-metallic crystals and metal-organic frameworks (MOFs) molecular crystal structures. The quasi-Laue geometry, combined with a large solid angle detector, will enable rapid data collection from crystals with volume < 1mm{sup 1} and unit cell < 100 {angstrom}. Construction and installation of the optical system is in progress. Commissioning is expected to start in April 2012.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Irradiation of electronic components and circuits at the Portuguese Research Reactor: Lessons learned

The behavior of electronic components and circuits under radiation is a concern shared by the nuclear industry, the space community and the high-energy physics community. Standard commercial components are used as much as possible instead of radiation hard components, since they are easier to obtain and allow a significant reduction of costs. However, these standard components need to be tested in order to determine their radiation tolerance. The Portuguese Research Reactor (RPI) is a 1 MW pool-type reactor, operating since 1961. The irradiation of electronic components and circuits is one area where a 1 MW reactor can be competitive, since the fast neutron fluences required for testing are in most cases well below 10{sup 16} n/cm{sup 2}. A program was started in 1999 to test electronics components and circuits for the LHC facility at CERN, initially using a dedicated in-pool irradiation device and later a beam line with tailored neutron and gamma filters. Neutron filters are essential to reduce the intensity of the thermal neutron flux, which does not produce significant defects in electronic components but produces unwanted radiation from activation of contacts and packages of integrated circuits and also of the printed circuit boards. In irradiations performed within the line-of-sight of the core of a fission reactor there is simultaneous gamma radiation which complicates testing in some cases. Filters can be used to reduce its importance and separate testing with a pure gamma radiation source can contribute to clarify some irradiation results. Practice has shown the need to introduce several improvements to the procedures and facilities over the years. We will review improvements done in the following areas: - Optimization of neutron and gamma filters; - Dosimetry procedures in mixed neutron / gamma fields; - Determination of hardness parameter and 1 MeV-equivalent neutron fluence; - Temperature measurement and control during irradiation; - Follow-up of reactor power operational fluctuations; - Study of gamma radiation effects only. The fission neutron spectrum can be limitative for some of the tests, as most neutrons are in the 1-2 MeV energy range. Significant progress has been made lately in compact neutron generators using D-D and D-T fusion reactions, achieving higher neutron fluxes and longer lifetime than previously available. The advantages of using compact neutron generators for testing of electronic components and circuits will be also discussed. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Development of Bismuth and Platinum Bi-Metallic Nanoparticles to Enhance Melt Wire Temperature Resolution

Advanced manufacturing (AM) based on direct-write (DW) technologies has emerged as the predominant enabler for the fabrication of active and passive sensors to be deployed in harsh operating environments seen in a nuclear reactor. Recently, Idaho National Laboratory and Boise State University have recently established capabilities to incorporate advanced manufacturing (AM) methods to accelerate, modernize and enhance functionality of nuclear sensors and instrumentation to achieve the goal of enhancing the safety and efficiency of nuclear reactors. A significant thrust of this work includes the development of nuclear relevant feedstock materials compatible with a variety of direct-write processes for the development, fabrication and testing of AM sensors for peak temperature detection and neutron flux monitoring. For this report, bismuth and bismuth/platinum (BiPt) bi-metallic nanoparticles were synthesized using wet chemical approaches to develop bi-metallic feedstock materials to enhance the sensitivity of melt wires for peak temperature detection. Nanoparticle characterization was performed with Transmission Electron Microscopy (TEM) for nanoparticle composition and size, Transmission X-Ray Diffraction Fluorescence (TXRF) for nanoparticle composition, and Differential Scanning Calorimetry to elucidate the melting point of BiPt bi-metallic nanoparticles. Preliminary results indicate bi-metallic BiPt nanoparticles as a viable pathway for fabricating high resolution AM melt wires.

36 MATERIALS SCIENCE↗

Plant Modernization Pathway: FY 2019 External Review Summary Report

This report describes an external review conducted by the Light Water Reactor Sustainability Program Plant Modernization Pathway (referred to as Pathway) to solicit feedback on the topics and results of the ongoing Instrumentation and Control (I&C) research program. This review was held in conjunction with the Nuclear Energy Institute (NEI) Digital I&C Working Group meeting that was held at Idaho National Laboratory on October 16–17, 2018. Members of the Nuclear Regulatory Commission (NRC) staff working on digital I&C issues through their Integrated Action Plan also attended. The NEI and NRC agreed that the meeting participants would serve as an external review panel for the purpose of obtaining expert input on the value and timing of the research projects. Five major research areas were presented, along with demonstrations of new technologies in the Human Systems Simulation Laboratory and the Computer-Assisted Virtual Environment. Following the presentations, the external review was conducted by referring to a set of summary slides of the five research areas, and allowing each participant to enter ratings and comments on a survey form as each area was addressed. Fourteen forms were returned. These feedback forms were analyzed by the Pathway who compiled and responded to the data and comments, which are documented in this report. The participants also had opportunity to provide comments on the LWRS Program as a whole and to suggest additional research topics of value. The feedback provided by the external review participants is taken to be a strong endorsement of the types of projects being conducted by the Pathway, the value they hold for the operating nuclear plants, and the general timing of need. The feedback aligns well with the priorities, levels of efforts allocated for the research projects, and project schedules of the current Pathway research program. The feedback also provides realistic observations on the practicality of some aspects of implementing these technologies. The Pathway will consider all of the feedback and address the recommended research topics that have been identified by the external review participants. Pathway research plans will be adjusted as warranted.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗