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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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NASA NTRS1983

Information contained in protein shapes

The sequence of local conformations at C-alpha atoms of a protein has been considered as an informational message string. The total self-information contents and self-information per letter have been evaluated for 83 globular proteins whose structures are known from X-ray crystallography. The derived information contents provide a method of quantitating structural specificity of proteins. This method of analysis enables repeating, intricate structural features to be recognized. Among the globular proteins whose structures have been solved, high potential iron protein stands out with the largest three-letter dependence.

Sundaram, K.↗
NASA NTRS1983

Bibliography

A bibliography of articles entered into the data base at the Lunar and Planetary Institute Library from November 1982 through January 1983 is presented. An abstract of each article is given. The subjects covered by the articles include: the motion of the moon and dynamics of the earth-moon system: shape and gravity field of the moon; the physical structure of the moon, its thermal and stress history; the morphology of the lunar surface, the origin and stratigraphy of lunar formations, and mapping of the moon; the chemical composition of the moon, lunar petrology, mineralogy, and crystallography; electromagnetic properties of the moon; the planets; and other objects, including asteroids, comets, meteorites, and cosmic dust.

Kopal, Z.↗
NASA NTRS1983

Surface studies with (clean) supported metal particles and clusters

Small particles are ideal for combined studies with surface analytical and electron microscopy/diffraction methods. In this way crystallography, microstructure, morphology, physical stability, and electronic structure can be correlated directly with chemical reactivity. Various integrated experimental approaches for conducting model studies with UHV-evaporated particles have been successfully developed; they entail the use of TPD, AES, XPS, and work function measurements on one hand and standard TEM/TED, in-situ TEM/TED, and in-situ STED/TEM techniques on the other hand. The essential features of four particular experimental approaches are discussed and a selection of representative results is presented to illustrate the potential usefulness of such studies in the field of catalysis.

Poppa, H. R.↗
NASA NTRS1984

High pressure cosmochemistry applied to major planetary interiors: Experimental studies

Progress is reported on a project to determine the properties and boundaries of high pressure phases of the H2-He-H2O-NH3-CH4 system that are needed to constrain theoretical models of the interiors of the major planets. This project is one of the first attempts to measure phase equilibria in binary fluid-solid systems in diamond anvil cells. Vibrational spectroscopy, direct visual observations, and X-ray diffraction crystallography of materials confined in externally heated cells are the primary experimental probes. Adiabats of these materials are also measured in order to constrain models of heat flow in these bodies and to detect phase transitions by thermal anomalies. Initial efforts involve the NH3-H2O binary. This system is especially relevant to models for surface reconstruction of the icy satellites of Jupiter and Saturn. Thermal analysis experiments were completed for the P-X space, p4GPa:0 or = 0.50, near room temperature. The cryostat, sample handling equipment, and optics needed to extend the optical P-T-X work below room temperature was completed.

Nicol, M. F.↗
NASA NTRS1985

High pressure cosmochemistry applied to major planetary interiors: Experimental studies

The measurement of equilibria in binary fluid-solid systems in diamond anvil cells, represents a major advance of the art of high-pressure experimentation. Vibrational spectroscopy, direct visual observations, and X-ray diffraction crystallography of materials confined in externally heated cells are the primary experimental probes being used. Adiabats in these systems are being measured in order to constrain models of heat flow in these bodies and to detect phase transitions by thermal anomalies. Other studies are directed toward interpreting high pressure reactions in these systems that are suggested by shockwave measurements, and developing methods for reaching high temperatures and high pressures of planetary interest in diamond cells. The overall objective of this project is to determine the properties of the H2-He-H2O-HN3-CH4 system and related small-molecule systems that are needed to constrain theoretical models of the interiors of the major planets.

Nicol, M. F.↗
NASA NTRS1983

Modal comparison of Yamato and Allan Hills polymict eucrites

Seven Yamato and six Allan Hills polymict eucrite specimens were compared by modal analysis. The analyses reveal differences of plagioclase and pyroxene content between the two groups. The Yamato suite has more 'pigeonitic' pyroxene and less plagioclase and low-calcium pyroxene than the Allan Hills suite. Variations within each suite are small and three sections of Allan Hills A78040 are more variable than the Allen Hills suite considered as a group. Modal data provides a basis for pairing polymict eucrite specimens when used together with mineralogical and petrographic criteria. Modal data furthermore confirms the presence of several rock types previously identified using pyroxene crystallography and hints at the presence of an augite-rich component.

Delaney, J. S.↗
NASA NTRS1986

Intact capture of hypervelocity particles

Knowledge of the phase, structure, and crystallography of cosmic particles, as well as their elemental and isotopic compositions, would be very valuable information toward understanding the nature of our solar system. This information can be obtained from the intact capture of large mineral grains of cosmic particles from hypervelocity impacts. Hypervelocity experiments of intact capture in underdense media have indicated realistic potential in this endeaver. The recovery of the thermal blankets and louvers from the Solar Max spacecraft have independently verified this potential in the unintended capture of cosmic materials from hypervelocity impacts. Passive underdense media will permit relatively simple and inexpensive missions to capture cosmic particles intact, either by going to a planetary body or by waiting for the particles to come to the Shuttle or the Space Station. Experiments to explore the potential of using various underdense media for an intact comet sample capture up to 6.7 km/s were performed at NASA Ames Research Center Vertical Gun Range. Explorative hypervelocity experiments up to 7.9 km/s were also made at the Ernst Mach Institute. These experiments have proven that capturing intact particles at hypervelocity impacts is definitely possible. Further research is being conducted to achieve higher capture ratios at even higher hypervelocities for even smaller projectiles.

Tsou, P.↗
NASA NTRS1986

High pressure cosmochemistry applied to major planetary interiors: Experimental studies

The overall goal of this project is to determine properties of the H-He-C-N-O system, as represented by small molecules composed of these elements, that are needed to constrain theoretical models of the interiors of the major planets. Much of our work now concerns the H2O-NH3 system. This project is the first major effort to measure phase equilibria in binary fluid-solid systems in diamond anvil cells. Vibrational spectroscopy, direct visual observations, and X-ray crystallography of materials confined in externally heated cells are our primary experimental probes. We also are collaborating with the shockwave physics group at Lawrence Livermore Laboratory in studies of the equation of state of a synthetic Uranus fluid and molecular composition of this and other H-C-N-O materials under planetary conditions.

Nicol, M. F.↗
NASA NTRS1988

High-Resolution Detector For X-Ray Diffraction

Proposed x-ray-sensitive imaging detector offers superior spatial resolution, counting-rate capacity, and dynamic range. Instrument based on laser-stimulated luminescence and reusable x-ray-sensitive film. Detector scans x-ray film line by line. Extracts latent image in film and simultaneously erases film for reuse. Used primarily for protein crystallography. Principle adapted to imaging detectors for electron microscopy and fluorescence spectroscopy and general use in astronomy, engineering, and medicine.

Carter, Daniel C.↗
NASA NTRS1988

Improved Charge-Coupled Imager For X Rays

Device proposed to improve imaging of x rays. Features thin layer of oxide in virtual phase to increase quantum efficiency and depletion layer nearly as thick as epitaxial silicon layer to increase resolution. Applications include imaging spectrometers for x-ray astronomy, investigations of plasmas, and x-ray crystallography.

Wadsworth, Mark↗
NASA NTRS1988

Protein crystal growth in a microgravity environment

Protein crystal growth is a major experimental problem and is the bottleneck in widespread applications of protein crystallography. Research efforts now being pursued and sponsored by NASA are making fundamental contributions to the understanding of the science of protein crystal growth. Microgravity environments offer the possibility of performing new types of experiments that may produce a better understanding of protein crystal growth processes and may permit growth environments that are more favorable for obtaining high quality protein crystals. A series of protein crystal growth experiments using the space shuttle was initiated. The first phase of these experiments was focused on the development of micro-methods for protein crystal growth by vapor diffusion techniques, using a space version of the hanging drop method. The preliminary space experiments were used to evolve prototype hardware that will form the basis for a more advanced system that can be used to evaluate effects of gravity on protein crystal growth.

Bugg, Charles E.↗
NASA NTRS1989

Protein crystal growth in microgravity

Major advances have been made in several of the experimental aspects of protein crystallography, leaving protein crystallization as one of the few remaining bottlenecks. As a result, it has become important that the science of protein crystal growth is better understood and that improved methods for protein crystallization are developed. Preliminary experiments with both small molecules and proteins indicate that microgravity may beneficially affect crystal growth. For this reason, a series of protein crystal growth experiments using the Space Shuttle was initiated. The preliminary space experiments were used to evolve prototype hardware that will form the basis for a more advanced system that can be used to evaluate effects of gravity on protein crystal growth. Various optical techniques are being utilized to monitor the crystal growth process from the incipient or nucleation stage and throughout the growth phase. The eventual goal of these studies is to develop a system which utilizes optical monitoring for dynamic control of the crystallization process.

Rosenblum, William M.↗
NASA NTRS1991

Ultra-High-Spectral-Resolution X-Ray/EUV Monochromator

Ultra-high-spectral-resolution X-Ray/EUV monochromator depends on Bragg reflection from multilayer coats and diffraction by mutlilayer-coated grating to select narrow wavelength band from input beam. Its monochromatic output beam of accurately known wavelength very useful in testing and calibration of x-ray telescopes, x-ray microscopes, photographic films, and photodetectors; in research in biological and biomedical disciplines, x-ray crystallography, properties and processing of materials, and x-ray lasers; and in x-ray lithography.

Hoover, Richard B.↗
NASA NTRS1991

Adhesion and abrasion of surface materials in the Venusian aeolian environment

In laboratory simulations of the Venusian environment, rock and mineral 'target' surfaces struck by aeolian particles develop a thin layer of accretionary material derived from the particles' attrition debris. Accretion may be (in part) a manifestation of 'cold welding', a process well known in engineering, where bonding occurs between metals at a tribological interface. Accretion on geological materials was found to occur at all Venusian surface temperatures and for all types of materials tested. First-order variations in the amount deposited by particles are related to relative attrition susceptibilities. Second-order variations relate to properties of the particle-target interface. Variations in accretion volume are apparently independent of mineral chemistry and are only weakly dependent on crystallography. The results suggest that accretion should be a fairly universal phenomenon in areas of Venus subject to aeolian activity.

Marshall, John R.↗
NASA NTRS1992

Phosphor Scanner For Imaging X-Ray Diffraction

Improved optoelectronic scanning apparatus generates digitized image of x-ray image recorded in phosphor. Scanning fiber-optic probe supplies laser light stimulating luminescence in areas of phosphor exposed to x rays. Luminescence passes through probe and fiber to integrating sphere and photomultiplier. Sensitivity and resolution exceed previously available scanners. Intended for use in x-ray crystallography, medical radiography, and molecular biology.

Carter, Daniel C.↗
NASA NTRS1992

Multilayer Monochromator For Hard X Rays And Gamma Rays

Compact monochromator for hard x rays and gamma rays provides high spectral resolution with high throughput. Resembles instruments in "Compact X-Ray and Extreme-Ultraviolet Monochromator" (MFS-28499), "Scanning X-Ray or Extreme-Ultraviolet Monochromator" (MFS-28492), "Ultra-High-Spectral-Resolution X-Ray/EUV Monochromator" (MFS-28500), and "Four-Mirror X-Ray and Extreme-Ultraviolet Monochromator" (MFS-28498). Operates on principle of multilayer Bragg reflector. Used in nuclear, astronomical, and biomedical research, x-ray crystallography, research on processing materials, research in x-ray lasers, and x-ray lithography.

Hoover, Richard B.↗
NASA NTRS1991

Proceedings of the Second Annual Symposium on Industrial Involvement and Successes in Commercial Space

The proceedings of the conference are presented. It is proposed that commercial development in space is an important element in the future competitive posture of the industrial nations of the world. The resources and characteristics of space will play a major role in opening a new economic frontier for all the spacefaring nations of the world. Some topics of discussion are as follow: NASA's mission and the role of CCD's; A balanced commercial access to space; Systems for COMET; SPACEHAB; Space Station Freedom; The center for macromolecular crystallography; Center for space power and advanced electronics; and The center for mapping.

Source record↗
NASA NTRS1991

Statistics of contractive cracking patterns

The statistics of convective soil patterns are analyzed using statistical crystallography. An underlying hierarchy of order is found to span four orders of magnitude in characteristic pattern length. Strict mathematical requirements determine the two-dimensional (2D) topology, such that random partitioning of space yields a predictable statistical geometry for polygons. For all lengths, Aboav's and Lewis's laws are verified; this result is consistent both with the need to fill 2D space and most significantly with energy carried not by the patterns' interior, but by the boundaries. Together, this suggests a common mechanism of formation for both micro- and macro-freezing patterns.

Noever, David A.↗