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At least 91 records · Page 5

Destructive physical analysis results of Ni/H2 cells cycled in LEO regime

Six 48-Ah individual pressure vessel (IPV) Ni/H2 cells containing 26 and 31 percent KOH electrolyte were life cycle tested in low earth orbit. All three cells containing 31 percent KOH failed (3729, 4165, and 11,355 cycles), while those with 26 percent KOH were cycled over 14,000 times in the continuing test. Destructive physical analysis (DPA) of the failed cells included visual inspections, measurements of electrode thickness, scanning electron microscopy, chemical analysis, and measurements of nickel electrode capacity in an electrolyte flooded cell. The cycling failure was due to a decrease of nickel electrode capacity. As possible causes of the capacity decrease, researchers observed electrode expansion, rupture, and corrosion of the nickel electrode substrate, active material redistribution, and accumulation of electrochemically undischargeable active material with cycling.

Lim, Hong S.↗

Special tests and destructive physical analyses as used by the Aerospace Corporation with nickel-hydrogen cells

The destructive physical analysis (DPA) of electrochemical devices is an important part of the overall test. Specific tests were developed to investigate the degradation mode or the failure mechanism that surfaces during the course of a cell being assembled, acceptance tested, and life-cycle tested. The tests that have been developed are peculiar to the cell chemistry under investigation. Tests are often developed by an individual or group of researchers as a result of their particular interest in an unresolved failure mechanism or degradation mode. A series of production, operational, and storage issues that were addressed by the Electrochemistry Group at The Aerospace Corporation are addressed. As a result of these investigations, as well as associated research studies carried out to develop a clearer understanding of the nickel oxyhydroxide electrode, a series of unique and useful specialized tests were developed. Some of these special tests were assembled to describe the methods that were found to be particularly useful in resolving a wide spectrum of manufacturing, operational, and storage issues related to nickel-hydrogen cells. The general methodology of these tests is given here with references listed to provide the reader with a more detailed understanding of the tests. The tests are classified according to the sequencing, starting with the impregnation of the nickel plaque material and culminating with the storage of completed cells. The details of the wet chemical procedures that were found to be useful because of their accuracy and reproducibility are given. The equations used to make the appropriate calculations are listed.

Zimmerman, A. H.↗

COMSAT's destructive physical analysis of aerospace nickel-cadmium cells for NASA/Goddard Space Flight Center

Over the past 5 years, COMSAT has performed numerous destructive physical analyses (DPA's) on NASA-Goddard-supplied nickel-cadmium (Ni/Cd) cells. The samples included activated but uncycled cells, wet stored cells, cycled cells, and anomalous cells. The DPA's provided visual, morphological, and chemical analyses of the cell components. The DPA data for the analyzed cells are presented. For the cells investigated, the leading cause of poor performance, as determined by DPA, has been poor negative electrode utilization, which resulted in negative-electrode-limiting operation.

Robbins, Kathleen M. B.↗

An x ray scatter approach for non-destructive chemical analysis of low atomic numbered elements

A non-destructive x-ray scatter (XRS) approach has been developed, along with a rapid atomic scatter algorithm for the detection and analysis of low atomic-numbered elements in solids, powders, and liquids. The present method of energy dispersive x-ray fluorescence spectroscopy (EDXRF) makes the analysis of light elements (i.e., less than sodium; less than 11) extremely difficult. Detection and measurement become progressively worse as atomic numbers become smaller, due to a competing process called 'Auger Emission', which reduces fluorescent intensity, coupled with the high mass absorption coefficients exhibited by low energy x-rays, the detection and determination of low atomic-numbered elements by x-ray spectrometry is limited. However, an indirect approach based on the intensity ratio of Compton and Rayleigh scattered has been used to define light element components in alloys, plastics and other materials. This XRS technique provides qualitative and quantitative information about the overall constituents of a variety of samples.

Ross, H. Richard↗

Non-destructive, ultra-low resistance, thermally stable contacts for use on shallow junction InP solar cells

Contact formation to InP is plagued by violent metal-semiconductor intermixing that takes place during the contact sintering process. Because of this the InP solar cell cannot be sintered after contact deposition. This results in cell contact resistances that are orders of magnitude higher than those that could be achieved if sintering could be performed in a non-destructive manner. We report here on a truly unique contact system involving Au and Ge, which is easily fabricated, which exhibits extremely low values of contact resistivity, and in which there is virtually no metal-semiconductor interdiffusion, even after extended sintering. We present a description of this contact system and suggest possible mechanisms to explain the observed behavior.

Weizer, V. G.↗

Helium destruction and gamma-ray line emission in accreting neutron stars

The prevalent gamma-ray production channel of a neutron star - emission of 2.2-MeV photons from neutron-proton recombination - is reconsidered. The 2.2-MeV gamma-ray line flux and Compton-scattered continuum are calculated. The flux of gravitationally redshifted 2.2-MeV photons from the brightest accreting X-ray source Scorpius X-1 is about 10 exp -6 gamma/sq cm s, a factor of 20 below the sensitivities on the Compton Gamma-Ray Observatory. The destruction of accreted He-4 leads to significant abundances of lighter elements (D, H-3, He-3) in the upper atmosphere, which are determined. The destroyed He-4 is reformed through fusion reactions a few scale heights beneath the photosphere, and thus does not hamper H-ray bursts.

Bildsten, Lars↗

Nasa Records Disposition Handbook: Procedures Governing the Retention, Retirement, and Destruction of Agency Records

This handbook sets forth the disposition of official records of the National Aeronautics and Space Administration. Its provisions are applicable to NASA Headquarters and all field installations. This revised edition has been enlarged in scope and re-titled to provide guidance in all aspects of records retirements, transfers, destruction, and retrievals from Federal Records Centers. New records control schedules have been added and others revised. Also included are procedures for making recommendations for improved coverage of records categories by additions or revisions. The NASA Records Control Schedules are issued under authority of the NASA Records Management Officer in accordance with Section 101-11.406, Federal Property Management Regulations. They were approved for NASA use by the National Archives and Records Service, the General Accounting Office, and by the Joint Committee on the Disposition of Executive Papers, U.S. Congress.

Source record↗

Destruction of problematic airborne contaminants by hydrogen reduction using a Catalytically Active, Regenerable Sorbent (CARS)

Thermally regenerable sorbent beds were demonstrated to be a highly efficient means for removal of toxic airborne trace organic contaminants aboard spacecraft. The utilization of the intrinsic weight savings available through this technology was not realized since many of the contaminants desorbed during thermal regeneration are poisons to the catalytic oxidizer or form highly toxic oxidation by-products in the Trace Contaminant Control System (TCCS). Included in this class of compounds are nitrogen, sulfur, silicon, and halogen containing organics. The catalytic reduction of these problematic contaminants using hydrogen at low temperatures (200-300 C) offers an attractive route for their destruction since the by-products of such reactions, hydrocarbons and inorganic gases, are easily removed by existing technology. In addition, the catalytic oxidizer can be operated more efficiently due to the absence of potential poisons, and any posttreatment beds can be reduced in size. The incorporation of the catalyst within the sorbent bed further improves the system's efficiency. The demonstration of this technology provides the basis for an efficient regenerable TCCS for future NASA missions and can be used in more conventional settings to efficiently remove environmental pollutants.

Thompson, John O.↗

Competition of supermassive black holes and galactic spheroids in the destruction of globular clusters

The globular clusters that we observe in galaxies may be only a fraction of the initial population. Among the evolutionary influences on the population is the destruction of globular clusters by tidal forces as the cluster moves through the field of influence of a disk, a bulge, and/or a putative nuclear component (black hole). We have conducted a series of N-body simulations of globular clusters on bound and marginally bound orbits through poetentials that include black hole and speroidal components. The degree of concentration of the spheroidal component can have a considerable impact on the extent to which a globular cluster is disrupted. If half the mass of a 10(exp 10) solar mass spheroid is concentrated within 800 pc, then only black holes with masses greater than 10(exp 9) solar mass can have a significant tidal influence over that already exerted by the bulge. However, if the matter in the spheroidal component is not so strongly concentrated toward the center of the galaxy, a more modest central black hole (down to 10(exp 8) solar mass) could have a dominant influence on the globular cluster distribution, particularly if many of the clusters were initially on highly radial orbits. Our simulations show that the stars that are stripped from a globular cluster follow orbits with roughly the same eccentricity as the initial cluster orbit, spreading out along the orbit like a 'string of pearls.' Since only clusters on close to radial orbits will suffer substantial disruption, the population of stripped stars will be on orbits of high eccentricity.

Charlton, Jane C.↗

Dust destruction and kinematics in the Galactic Center

We present observations of the 34.815 micron (SiII) line and continuum emission from the inner few parsecs of the Galaxy obtained with the KAO Echelle Grating Spectrograph (KEGS) in June 1993. The SiII emission, which has been spectrally resolved at 64 km/s and spatially resolved at 10 arcsec, in kinematically consistent with the motions of ionized and neutral gas interior to the circumnuclear disk (CND). In addition, the emission in the (SiII) line as well as the continuum extends northward along the 'northern arm' past the inner edge of the CND. A peak in the (SiII) line/continuum ratio is observed at approx. 25 arcsec W and 75 arcsec N of Sgr A* with a large velocity dispersion. This may be an indication of dust destruction via cloud-cloud collisions.

Stolovy, Susan R.↗

Non-destructive evaluation of composites

The composite materials have been used in aerospace industries for quite some time. Several non-destructive evaluation (NDE) methods have been developed to inspect composites in order to detect flaws, matrix cracking, and delamination. These methods include ultrasonics, acoustic emission, shearography, thermography, X-ray, and digital image correlation. The NDE Branch of Marshall Space Flight Center has recently acquired a thermal imaging NDE system. The same system has been used at NASA Langley Research Center for detecting disbonds. In order to compare different NDE methods, three carbon/carbon composite panels were used for experiment using ultrasonic C-scan, shearography, and thermography methods. These panels have teflon inserts to simulate the delamination between plies in a composite panel. All three methods have successfully located the insert. The experiment and results are presented in the following sections.

Chu, Tsuchin Philip↗

A Preliminary Investigation on the Destruction of Solid-Propellant Rocket Motors by Impact from Small Particles

An investigation was conducted to determine whether solid-propellant rocket motors could be ignited and destroyed by small-particle impacts at particle velocities up to a approximately 10,940 feet per second. Spheres ranging from 1/16 to 7/32 inch in diameter were fired into simulated rocket motors containing T-22 propellant over a range of ambient pressures from sea level to 0.12 inch of mercury absolute. Simulated cases of stainless steel, aluminum alloy, and laminated Fiberglas varied in thickness from 1/50 to 1/8 inch. Within the scope of this investigation, it was found that ignition and explosive destruction of simulated steel-case rocket motors could result from impacts by steel spheres at the lowest attainable pressure.

Carter, David J., Jr.↗

Destructive Evaluation of a Xenon Hollow Cathode after a 28,000 Hour Life Test

International Space Station (ISS) plasma contactor system requires a hollow cathode assembly (HCA) with a lifetime of at least 18,000 hours. In order to demonstrate the lifetime capability of the HCA, a series of hollow cathode wear tests was performed which included a life test operated at the maximum current of the HCA. This test sought to verify hollow cathode lifetime capability and contamination control protocols. This hollow cathode accumulated 27,800 hours of operation before it failed during a restart attempt. The cathode was subsequently destructively analyzed in order to determine the failure mechanism. Microscopic examination of the cathode interior determined that relatively small changes in the cathode physical geometry had occurred and barium tungstates, which are known to limit the emission process, had formed over a majority of the electron emitter surface. Because the final state of the insert was consistent with expected impregnate chemistry, the hollow cathode was believed to have reached the end of its usable life under the test conditions.

Sarver-Verhey, Timothy R.↗

Destructive Physical Analysis of Flight- and Ground-Tested Sodium-Sulfur Cells

Destructive physical analysis (DPA) was used to study the effects of microgravity on the sulfur electrode in sodium-sulfur cells. The cells examined in this work were provided by the Air Force Research Laboratory (AFRL) from their program on sodium-sulfur technology. The Naval Research Laboratory (NRL) provided electrical characterization of the flight-tested and ground-tested cells.

Wasz, Margot L.↗

The Evolution of Dust in the Multiphase ISM: Grain Destruction Processes

This proposal covered year one of a long term project in which we acquired the necessary hardware and softwaxe needed to calculate grain destruction processes in the interstellar medium (ISM). The long term goal of this research is to develop a model for the dust evolution in the ISM capable of explaining observations of elemental depletions, the grain size distribution, and the emission characteristics of the ISM from the X-ray through the FIR. We purchased a SUN Ultra 10 workstation and peripheral devices including an Exabyte Tape drive, HP Laser Printer, and Seagate External Hard Disk. The PI installed the hardware and Solaris operating system on the workstation and integrated the hardware into the network. Software was also purchased to enable connections to the workstation from a PC (Hummingbird Exceed). Additional freeware required to carry out the proposed program was installed on the system including compilers (g77, gcc, g++), editors (emacs), a markup language (LaTeX), and display programs (WIP, XV, SAOtng). We have also successfully modified the required plot files to work with our system which display the results of grain processing.

Wolfire, Mark↗

Non-Destructive Evaluation Method and Apparatus for Measuring Acoustic Material Nonlinearity

An acoustic non-linearity parameter (beta) measurement method and system for Non-Destructive Evaluation (NDE) of materials and structural members obviates the need for electronic calibration of the measuring equipment. Unlike known substitutional measuring techniques requiring elaborate calibration procedures, the electrical outputs of the capacitive detector of a sample with known beta and the test sample of unknown beta are compared to determine the unknown beta. In order to provide the necessary stability of the present-inventive reference-based approach, the bandpass filters of the measurement system are maintained in a temperature-controlled environment, and the line voltage supplied to said amplifiers is well-regulated.

William T Yost↗

Non-Destructive Testing Scanner

Bio-Imaging Research's technology that originated in an aerospace program has come full circle with a new aerospace adaptation called the Advanced Computed Tomography Inspection System, or ACTIS. The medical version of CT scans the human body for tumors or other abnormalities, the ACTIS system finds imperfections in aerospace structures and components, such as castings, assemblies, rocket motors and nozzles. ACTIS is described by its developer as the most versatile CT scanner available for non-destructive testing applications. ACTIS is a variable geometry system. ACTIS source and detectors can be moved closer together or farther apart to optimize the geometry for different sizes of test objects. The combination of variable geometry, three sources, and focusing detectors makes ACTIS cost effective for a broad range of applications. System can scan anything from very small turbine blades to large rocket assemblies.

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Sensitivity and Calibration of Non-Destructive Evaluation Method That Uses Neural-Net Processing of Characteristic Fringe Patterns

This paper answers some performance and calibration questions about a non-destructive-evaluation (NDE) procedure that uses artificial neural networks to detect structural damage or other changes from sub-sampled characteristic patterns. The method shows increasing sensitivity as the number of sub-samples increases from 108 to 6912. The sensitivity of this robust NDE method is not affected by noisy excitations of the first vibration mode. A calibration procedure is proposed and demonstrated where the output of a trained net can be correlated with the outputs of the point sensors used for vibration testing. The calibration procedure is based on controlled changes of fastener torques. A heterodyne interferometer is used as a displacement sensor for a demonstration of the challenges to be handled in using standard point sensors for calibration.

Decker, Arthur J.↗