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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 91 records · Page 5
All sourcesNASA NTRSDOE OSTI
NASA NTRS1977

Thermal environment effects on strength and impact properties of boron-aluminum composites

Thermal effects on fracture strength and impact energy were studied in 50 volume percent unidirectional composites of 143 and 203 micron boron fibers in 6061 and 1100 aluminum matrices. For 6061 matrix composites, strength was maintained to approximately 400 C in the cyclic tests and higher than 400 C in the static tests. For the 1100 matrix composites, strength degradation appeared near 260 C after cycling and higher than 260 C in static heating. This composite strength degradation is explained by a fiber degradation mechanism resulting from a boron-aluminum interface reaction. The impact energy absorption degraded significantly only above 400 C for both matrix alloys. Thus, while impact loss for the 6061 composite correlates with the fiber strength loss, other energy absorption processes appear to extend the impact resistance of the 1100 matrix composites to temperatures beyond where its strength is degraded. Interrupted impact tests on as-received and thermally cycled composites define the range of load over which the fibers break in the impact event.

Grimes, H. H.↗
NASA NTRS1992

Fracture resistance and fatigue crack growth characteristics of two Al-Cu-Mg-Zr alloys

The dependence of strength, fracture resistance, and fatigue crack growth rate on the aging conditions of two alloy compositions based on Al-3.7Cu-1.85Mg-0.2Mn is investigated. Mechanical properties were evaluated in two heat treatment conditions and in two orientations (longitudinal and transverse). Compact tension specimens were used to determine fatigue crack growth characteristics and fracture resistance. The aging response was monitored on coupons using hardness measurements determined with a standard Rockwell hardness tester. Fracture resistance is found to increase with increasing yield strength during artificial aging of age-hardenable 2124-Zr alloys processed by powder metallurgy techniques. Fatigue crack growth rate increases with increasing strength. It is argued that these changes are related to deformation modes of the alloys; a homogeneous deformation mode tends to increase fracture resistance and to decrease the resistance to the fatigue crack propagation rate.

Sarkar, Bhaskar↗
NASA NTRS1987

Flaw imaging and ultrasonic techniques for characterizing sintered silicon carbide

The capabilities were investigated of projection microfocus x-radiography, ultrasonic velocity and attenuation, and reflection scanning acoustic microscopy for characterizing silicon carbide specimens. Silicon carbide batches covered a range of densities and different microstructural characteristics. Room temperature, four point flexural strength tests were conducted. Fractography was used to identify types, sizes, and locations of fracture origins. Fracture toughness values were calculated from fracture strength and flaw characterization data. Detection capabilities of radiography and acoustic microscopy for fracture-causing flaws were evaluated. Applicability of ultrasonics for verifying material strength and toughness was examined.

Baaklini, George Y.↗
NASA NTRS1988

Radiographic and ultrasonic characterization of sintered silicon carbide

The capabilities were investigated of projection microfocus X-radiography, ultrasonic velocity and attenuation, and reflection scanning acoustic microscopy for characterizing silicon carbide specimens. Silicon carbide batches covered a range of densities and different microstructural characteristics. Room temperature, four point flexural strength tests were conducted. Fractography was used to identify types, sizes, and locations of fracture origins. Fracture toughness values were calculated from fracture strength and flaw characterization data. Detection capabilities of radiography and acoustic microscopy for fracture-causing flaws were evaluated. Applicability of ultrasonics for verifying material strength and toughness was examined.

Baaklini, G. Y.↗
NASA NTRS1976

Large-diameter fasteners of CRES alloy

Double-hex bolthead allows bolts of high strength corrosion-resistant steel (CRES) to be made in diameters up to 1-1/4 in. Design allows 12-point tension heads to be cold formed to retain required minimum tensile strength of 220,000 psi and to retain high fracture strength.

Charles, J. F.↗
NASA NTRS1973

An investigation of the plastic fracture of high strength steels

Three generally recognized stages of plastic fracture in high strength steels are considered in detail. These stages consist of void initiation, void growth, and void coalescence. A brief review of the existing literature on plastic fracture is included along with an outline of the experimental approach used in the investigation.

Cox, T. B.↗
NASA NTRS1990

Matrix density effects on the mechanical properties of SiC/RBSN composites

The room temperature mechanical properties were measured for SiC fiber reinforced reaction-bonded silicon nitride composites (SiC/RBSN) of different densities. The composites consisted of approx. 30 vol percent uniaxially aligned 142 micron diameter SiC fibers (Textron SCS-6) in a reaction-bonded Si3N4 matrix. The composite density was varied by changing the consolidation pressure during RBSN processing and by hot isostatically pressing the SiC/RBSN composites. Results indicate that as the consolidation pressure was increased from 27 to 138 MPa, the average pore size of the nitrided composites decreased from 0.04 to 0.02 microns and the composite density increased from 2.07 to 2.45 gm/cc. Nonetheless, these improvements resulted in only small increases in the first matrix cracking stress, primary elastic modulus, and ultimate tensile strength values of the composites. In contrast, HIP consolidation of SiC/RBSN resulted in a fully dense material whose first matrix cracking stress and elastic modulus were approx. 15 and 50 percent higher, respectively, and ultimate tensile strength values were approx. 40 percent lower than those for unHIPed SiC/RBSN composites. The modulus behavior for all specimens can be explained by simple rule-of-mixture theory. Also, the loss in ultimate strength for the HIPed composites appears to be related to a degradation in fiber strength at the HIP temperature. However, the density effect on matrix fracture strength was much less than would be expected based on typical monolithic Si3N4 behavior, suggesting that composite theory is indeed operating. Possible practical implications of these observations are discussed.

Bhatt, Ramakrishna T.↗
NASA NTRS1989

Improving the low temperature ductility of NiAl

As part of a study aimed at developing a ductile NiAl-based alloy, ingots of Ni-Fe-Al alloys were cast and hot extruded to rods. The purpose of the iron additions was two-fold viz; to produce a change in the slip vector from 001 to 111 line and, in one alloy, to add a L1(2)-structured ductile second phase. Extruded Ni-20Al-30Fe was two-phase, containing a pro-eutectic B2 phase in a fine lamellar structure of B2+L1(2) phases. Room temperature tensile testing of both single extruded and double extruded alloys resulted in 8-percent and 22-percent plastic elongation and yield stresses of 850 and 760 MPa, respectively. Fracture in both cases occurred by ductile tearing of the eutectic and transgranular cleavage of the proeutectic phase at 1350 MPa. The ductility in double extruded condition is higher than that reported earlier in rapidly solidified wires by Inoue et al. (1984). By comparison, extruded single-phase B2-structured Ni-30Al-20Fe exhibited a fracture strength of 780 MPa, no plasticity, and a mixture of intergranular fracture and transgranular cleavage. This is contrast to earlier work by Inoue et al. where a yield stress of 400 MPa, 5 percent plastic strain, and a mixture of dimple and intergranular fracture was reported.

Guha, Sumit↗
NASA NTRS1990

Matrix density effects on the mechanical properties of SiC fiber-reinforced silicon nitride matrix properties

The room temperature mechanical properties were measured for SiC fiber reinforced reaction-bonded silicon nitride composites (SiC/RBSN) of different densities. The composites consisted of approx. 30 vol percent uniaxially aligned 142 micron diameter SiC fibers (Textron SCS-6) in a reaction-bonded Si3N4 matrix. The composite density was varied by changing the consolidation pressure during RBSN processing and by hot isostatically pressing the SiC/RBSN composites. Results indicate that as the consolidation pressure was increased from 27 to 138 MPa, the average pore size of the nitrided composites decreased from 0.04 to 0.02 microns and the composite density increased from 2.07 to 2.45 gm/cc. Nonetheless, these improvements resulted in only small increases in the first matrix cracking stress, primary elastic modulus, and ultimate tensile strength values of the composites. In contrast, HIP consolidation of SiC/RBSN resulted in a fully dense material whose first matrix cracking stress and elastic modulus were approx. 15 and 50 percent higher, respectively, and ultimate tensile strength values were approx. 40 percent lower than those for unHIPed SiC/RBSN composites. The modulus behavior for all specimens can be explained by simple rule-of-mixture theory. Also, the loss in ultimate strength for the HIPed composites appears to be related to a degradation in fiber strength at the HIP temperature. However, the density effect on matrix fracture strength was much less than would be expected based on typical monolithic Si3N4 behavior, suggesting that composite theory is indeed operating. Possible practical implications of these observations are discussed.

Bhatt, Ramakrishna T.↗
NASA NTRS1972

Investigation of the plastic fracture of high strength steels

An investigation of the plastic fracture process to improve tensile strength in high strength steels is presented. Two generic types of steels are considered: a quenched and tempered grade and a maraging grade, in order to compare two different matrix microstructures. Each type of steel was studied in commercial grade purity and in special melted high purity form, low in residual and impurity elements. The specific alloys dealt with include AISI 4340 and 18 Ni, 200 grade maraging steel, both heat treated to the same yield strength level of approximately 200 ksi.

Cox, T. B.↗
NASA NTRS2015

Mechanical Properties of a High Lead Glass Used in the Mars Organic Molecule Analyzer

The elastic constants, strength, fracture toughness, slow crack growth parameters, and mirror constant of a high lead glass supplied as tubes and funnels were measured using ASTM International (formerly ASTM, American Society for Testing and Materials) methods and modifications thereof. The material exhibits lower Young's modulus and slow crack growth exponent as compared to soda-lime silica glass. Highly modified glasses exhibit lower fracture toughness and slow crack growth exponent than high purity glasses such as fused silica.

lead↗
NASA NTRS1972

Investigation of the plastic fracture of high strength steels

This investigation deals in detail with the three recognized stages of plastic fracture in high strength steels, namely, void initiation, void growth, and void coalescence. The particular steels under investigation include plates from both commercial purity and high purity heats of AISI 4340 and 18 Ni, 200 grade maraging steels. A scanning electron microscope equipped with an X-ray energy dispersive analyzer, together with observations made using light microscopy, revealed methods of improving the resistance of high strength steels to plastic fracture.

Cox, T. B.↗
NASA NTRS1978

Thermal environment effects on strength and impact properties of boron-aluminum composites

A systematic study was conducted regarding the degradation of fracture strength and impact energy in commercial B-Al composites in both static and cyclic thermal environments. The composites used in the study contained approximately 50 vol % boron fibers, unidirectionally aligned in either a 6061 Al or 1100 Al matrix. The tensile strengths of the composites after 3000 thermal cycles as a function of upper cycle temperature are presented in graphs. The temperature at which the strengths of 6061 Al matrix, B-Al composites were significantly degraded after 3000 cycles was noticeably higher than that for the 1100 Al matrix composites. Static heating at 420 C resulted in no significant strength degradation for the 6061 Al matrix composites. In the case of 1100 matrix composites, some degradation was observed at 420 C but markedly less than in the composites cycled to 420 C.

Grimes, H. H.↗
NASA NTRS2019

Through-Thickness Tensile Properties of Triaxial Braided Composites

The through-thickness strength of triaxial braided composites was measured using thin specimens bonded to metallic tabs. Despite providing reasonable engineering estimates of the bulk properties, some test specimen limitations were noted: For strong epoxies, significant shear and tensile stresses occur and induce failure between the first layer and bond-line; the strains over much of the exterior are ~10% lower than interior strains, which are representative of the nominal state; and failure often occurred near or along the adhesive bond line. These interference were partially overcome by adding a large radius to the gage section. Based on the finite element analysis and experimental measurements, the nominal elastic modulus and Poisson's ratio are E(sub 33) = 10.7 GPa and v(sub 31) = 0.08 for the three triaxial braided composites tested. Strengths vary from 14 to 40 MPa depending on the resin. Relative to the in-plane properties, the through thickness modulus, fracture strength, failure strain, and Poisson's ratio are 1/5th, 1/30th, 1/6th, and 1/4th. Interlaminar failure occurred with varying degrees of fiber tear out along with little damage to axial tows, resulting is a smooth undulating fracture surface. Post cure temperature excursions to 177 deg C (350 deg F) had little effect on elastic constants but reduced the strength E862 based composites severely. The strength of PR520 and 5208 based composites increased.

composite↗
NASA NTRS2004

Eccentric loading of microtensile specimens

Ceramic materials have a lower density than most metals and are capable of performing at extremely high temperatures. The utility of these materials is obvious; however, the fracture strength of brittle materials is not easily predicted and often varies greatly. Characteristically, brittle materials lack ductility and do not yield as other materials. Ceramics materials are naturally populated with microscopic cracks due to fabrication techniques. Upon application of a load, stress concentration occurs at the root of these cracks and fracture will eventually occur at some not easily predicted strength. In order to use ceramics in any application some design methodology must exist from which a component can be placed into service. This design methodology is CARES/LIFE (Ceramics Analysis and Reliability Evaluation of Structures) which has been developed and refined at NASA over the last several decades. The CARES/LIFE computer program predicts the probability of failure of a ceramic component over its service life. CARES combines finite element results from a commercial FE (finite element) package such as ANSYS and experimental results to compute the abovementioned probability of failure. Over the course of several tests CARES has had great success in predicting the life of various ceramic components and has been used throughout industry. The latest challenge is to verify that CARES is valid for MEMS (Micro-Electro Mechanical Systems). To investigate a series of microtensile specimens were fractured in the laboratory. From this data, material parameters were determined and used to predict a distribution of strength for other specimens that exhibit a known stress concentration. If the prediction matches the experimental results then these parameters can be applied to a desired component outside of the laboratory. During testing nearly half of the tensile Specimens fractured at a location that was not expected and hence not captured in the FE model. It has been my duty to investigate the nature of this phenomenon in hopes of finding a better correlation between theory and empirical results. To investigate I built complete FE models of all of the tensile specimens using ANSYS. It is suspected that some misalignment naturally occurs during testing and thus additional bending stresses are present in the specimens. I modeled this eccentric loading and ran several FE trials using ANSYS/PDS (a probabilistic design system in ANSYS). My objective this summer has been familiarize myself with the CARES/LIFE program in hopes of using it in conjunction with ANSYS to help verify that CARES is applicable to MEMS-scale (greater that 1 micron, less than 1 millimeter) components.

Trapp, Mark A.↗
NASA NTRS1990

Properties of RBSN and RBSN-SiC composites

Strengths, fracture toughnesses, hardnesses, and dimensional changes have been measured for RBSN and RBSN/SiC composites. Samples were made from mixtures of Si and either Si- or C-rich SiC powders. For pure, 75 pct dense RBSN dispersed with octanol, strengths up to 858 MPa have been achieved. Improved strengths result from a combination of microstructural perfection and increased fracture toughness. The mechanical properties of the composites were approximately equal to those of methanol processed RBSN but not quite equal to those of the octanol-processed RBSN. Results are discussed in terms of observed microstructural features.

Lightfoot, A.↗