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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 91 records · Page 5
All sourcesNASA NTRSDOE OSTI
NASA NTRS2013

Lap Shear Testing of Candidate Radiator Panel Adhesives

During testing of a subscale radiator section used to develop manufacturing techniques for a full-scale radiator panel, the adhesive bonds between the titanium heat pipes and the aluminum face sheets failed during installation and operation. Analysis revealed that the thermal expansion mismatch between the two metals resulted in relatively large shear stresses being developed even when operating the radiator at moderate temperatures. Lap shear testing of the adhesive used in the original joints demonstrated that the two-part epoxy adhesive fell far short of the strength required. A literature review resulted in several candidate adhesives being selected for lap shear joint testing at room temperature and 398 K, the nominal radiator operating temperature. The results showed that two-part epoxies cured at room and elevated temperatures generally did not perform well. Epoxy film adhesives cured at elevated temperatures, on the other hand, did very well with most being sufficiently strong to cause yielding in the titanium sheet used for the joints. The use of an epoxy primer generally improved the strength of the joint. Based upon these results, a new adhesive was selected for the second subscale radiator section.

Ellis, David↗
NASA NTRS2015

(40)Ar/(39)Ar Age of Hornblende-Bearing R Chondrite LAP 04840

Chondrites have a complex chronology due to several variables affecting and operating on chondritic parent bodies such as radiogenic heating, pressure and temperature variation with depth, aqueous alteration, and shock or impact heating. Unbrecciated chondrites can record ages from 4.56 to 4.4 Ga that represent cooling in small parent bodies. Some brecciated chondrites exhibit younger ages (much less than 4 to 4.4 Ga) that may reflect the age of brecciation, disturbance, or shock and impact events (much less than 4 Ga). A unique R chondrite was recently found in the LaPaz Icefield of Antarctica - LAP 04840. This chondrite contains approximately 15% hornblende and trace amounts of biotite, making it the first of its kind. Studies have revealed an equigranular texture, mineral equilibria yielding equilibration near 650-700 C and 250-500 bars, hornblende that is dominantly OH-bearing (very little Cl or F), and high D/H ratios. To help gain a better understanding of the origin of this unique sample, we have measured the (40)Ar/(39)Ar age (LAP 04840 split 39).

Righter, K.↗
NASA NTRSDate not supplied

Introducing The Lunar Autonomous PNT System(LAPS) Simulator

In this paper we introduce a software simulator that has been used to develop an architecture for a low-cost Lunar Autonomous Position, Navigation and Time (PNT) System, LAPS. LAPS is a conceptual architecture for providing autonomous PNT services on and around the Moon using non-dedicated low-cost orbital and ground assets. The simulation tool has been developed to be flexible and is capable of modeling and analyzing the many different capabilities and configurations that the non-dedicated assets could support. The tool models the creation of an ad hoc swarm, the localization of this swarm and the subsequent provision of PNT services from this swarm. We present results from several studies of select configurations chosen to reflect existing and future real-world needs and capabilities.

Benjamin Hagenau↗
DOE OSTI2019

Fusion joining of thermoplastic composite wind turbine blades: Lap-shear bond characterization

Wind turbine blades are typically manufactured from a small number of components which are bonded together with an adhesive. Over the life span of a wind turbine, the static and fatigue loads in varying environmental conditions can lead to cracking and/or debonding of the adhesive joints, ultimately leading to blade structural collapse. The objective of this work is to investigate fusion joining of wind turbine blades manufactured using thermoplastic resin. Thermoplastic resins for wind turbine blades can reduce cycle times and energy consumption during manufacturing and facilitate end-of-life recycling and on-site manufacturing. Additionally, fusion joining of these materials can replace adhesives, resulting in stronger and more robust blades. This work showed that, compared to typical adhesives used in wind turbine blades, fusion welding resulted in an increase in both the static and fatigue lap-shear strength as compared to bonded thermoplastic composite coupons. This initial coupon-scale research suggests that there is potential for developing fusion welding techniques for full-scale wind turbine blades.

17 WIND ENERGY↗
DOE OSTI2020

Materials Data on LaP by Materials Project

LaP is Halite, Rock Salt structured and crystallizes in the cubic Fm-3m space group. The structure is three-dimensional. La3+ is bonded to six equivalent P3- atoms to form a mixture of corner and edge-sharing LaP6 octahedra. The corner-sharing octahedral tilt angles are 0°. All La–P bond lengths are 3.03 Å. P3- is bonded to six equivalent La3+ atoms to form a mixture of corner and edge-sharing PLa6 octahedra. The corner-sharing octahedral tilt angles are 0°.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Materials Data on LaPS by Materials Project

LaPS crystallizes in the orthorhombic Pnma space group. The structure is three-dimensional. there are two inequivalent La3+ sites. In the first La3+ site, La3+ is bonded in a 9-coordinate geometry to four equivalent P1- and five S2- atoms. There are two shorter (3.28 Å) and two longer (3.35 Å) La–P bond lengths. There are a spread of La–S bond distances ranging from 2.90–3.00 Å. In the second La3+ site, La3+ is bonded in a 9-coordinate geometry to four equivalent P1- and five S2- atoms. There are two shorter (3.01 Å) and two longer (3.26 Å) La–P bond lengths. There are a spread of La–S bond distances ranging from 2.89–2.96 Å. P1- is bonded in a 6-coordinate geometry to four La3+ and two equivalent P1- atoms. There are one shorter (2.24 Å) and one longer (2.27 Å) P–P bond lengths. There are two inequivalent S2- sites. In the first S2- site, S2- is bonded to five La3+ atoms to form a mixture of distorted corner and edge-sharing SLa5 trigonal bipyramids. In the second S2- site, S2- is bonded to five La3+ atoms to form a mixture of distorted corner and edge-sharing SLa5 trigonal bipyramids.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Determination of Total, Organic, and Inorganic Carbon and Total Nitrogen in Biological Cultures and Liquid Fraction Process Samples: Laboratory Analytical Procedure (LAP)

This Laboratory Analytical Procedure (LAP) describes the quantitative determination of total organic carbon, inorganic carbon in whole suspended biological samples and in the cell-free supernatant, by combustion and CO 2 detection with a non-dispersive infrared (NDIR) detector. This allows for distinct reporting of soluble and insoluble organic and inorganic carbon. In addition, this procedure covers the quantitative determination of soluble nitrogen in the cell-free supernatant.

09 BIOMASS FUELS↗
DOE OSTI2013

Determination of Total Lipids as Fatty Acid Methyl Esters: Laboratory Analytical Procedure (LAP)

This Laboratory Analytical Procedure (LAP) covers the determination of total lipids expressed as fatty acid methyl esters (FAME). Results are reported as the percent FAME content based on the dry weight of the sample. The procedure is based on a whole biomass transesterification procedure of lipids to FAME, which eliminates the need for extraction and therefore is able to access all fatty acids in the biomass and represent an accurate reflection of the biofuels potential.

09 BIOMASS FUELS↗
DOE OSTI2015

Fracture mechanics approach to estimate fatigue lives of welded lap-shear specimens

A full range of stress intensity factor solutions for a kinked crack with finite length is developed as a function of weld width and the sheet thickness. When used with the main crack solutions (global stress intensity factors) in terms of the applied load and the specimen geometric parameters, the fatigue lived of the kinked crack can be estimated for the laser-welded lap-shear specimens. The predicted curve for the load range-fatigue life passes through the cluster of experimental data and is in good agreement. A classical solution associated with an infinitesimal kink is also employed. Furthermore, its life prediction tends to overestimate the actual fatigue life. In addition, the traditional fatigue life estimation based on structural stress is performed for completeness. As a result, this non-fracture mechanics approach only agrees well with the experimental data under high cyclic load conditions.

42 ENGINEERING↗
DOE OSTI2014

FRACTURE MECHANICS APPROACH TO ESTIMATE FATIGUE LIVES OF WELDED LAP-SHEAR SPECIMENS

A full range of stress intensity factor solutions for a kinked crack is developed as a function of weld width and the sheet thickness. When used with the associated main crack solutions (global stress intensity factors) in terms of the applied load and specimen geometry, the fatigue lives can be estimated for the laser-welded lap-shear specimens. The estimations are in good agreement with the experimental data. A classical solution for an infinitesimal kink is also employed in the approach. However, the life predictions tend to overestimate the actual fatigue lives. The traditional life estimations with the structural stress along with the experimental stress-fatigue life data (S-N curve) are also provided. In this case, the estimations only agree with the experimental data under higher load conditions.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Empirical Characterization and Modeling of Cohesive – to – Adhesive Shear Fracture Mode Transition due to Increased Adhesive Layer Thicknesses of Fiber Reinforced Composite Single – Lap Joints

Here, to ensure a strong adhesive bond, most standards and adhesive manufacturers specify a maximum adhesive gap of 1 mm when bonding fiber reinforced composite structures. In manufacturing large components, such as joining two halves of wind turbine blades, meeting this gap tolerance specification is impractical; gaps larger than 10 mm are common in large adhesively bonded composite structures using state-of-the-art manufacturing techniques. Currently, there is a lack of fundamental understanding of the failure mechanics of adhesive gaps larger than 3 mm. To create such understanding, glass fiber - acrylic thermoplastic composite panels bonded using different epoxy adhesives within single-lap joint samples with adhesive thicknesses of 0.1 mm, 0.3 mm, 1 mm, 3 mm, 5 mm, and 10 mm were sheared to failure. A transition from cohesive to adhesive failure was observed to occur about 1 mm to 3 mm joint thicknesses. Plotting the shear stress normalized by the ratio of the joint width to thickness as a function of the joint thickness normalized by the joint length is shown to result in the ability to fit simple empirically derived models of the cohesive-to-adhesive failure transition, regardless of the adhesive. Furthermore, using these normalized variables, all the observed cohesively failed specimens collapse to a single master curve, as do the adhesively failed specimens.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Analysis on the Fracture of Al-Cu Dissimilar Materials Friction Stir Welding Lap Joint

Friction stir welding (FWS) is regarded as a more plausible alternative to other welding methods for Al-Cu dissimilar joining. However, the structure of an FSW joint is different from others. In this study, lap joints of 6061 aluminum alloy and commercially pure copper were produced by FSW, and the effects of rotation rate on macromorphology, microstructure and mechanical properties were investigated. In addition, a fracture J integral model was used to analyze the effect of microstructure on the mechanical properties. The results revealed that the macrodefect-free joints were obtained at a feed rate of 150 mm/min and 1100 rpm and that the failure load of the joint reached as high as 4.57 kN and only reached 2.91 kN for the 900 rpm, where tunnel defects were identified. Particle-rich zones composed of Cu particles dispersed in an Al matrix, and “Flow tracks” were observed by the EDS. The J integral results showed that the microdefects on the advancing side cause serious stress concentration compared with the microdefects located on the Al-Cu interface, resulting in the fracture of the joints.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Experimental Investigation and Finite Element Analysis on Fatigue Behavior of Aluminum Alloy 7050 Single-Lap Joints

The fatigue behavior of single-lap four-riveted aluminum alloy 7050 joints was investigated by using high-frequency fatigue test and scanning electron microscope (SEM). Stress distributions obtained by finite element (FE) analysis help explain the fatigue performance. The fatigue test results showed that the fatigue lives of the joints depend on cold expansion and applied cyclic loads. FE analysis and fractography indicated that the improved fatigue lives can be attributed to the reduction in maximum stress and evolution of fatigue damage at the critical location. The beneficial effects of strengthening techniques result in tearing ridges or lamellar structure on fracture surface, decrease in fatigue striations spacing, delay of fatigue crack initiation, crack deflection in fatigue crack propagation and plasticity-induced crack closure.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Growth kinetics of Al–Fe intermetallic compounds during annealing treatment of friction stir lap welds

In this study, we explored the growth kinetics of the Al–Fe intermetallic (IM) layer at the joint interface of the St-12/Al-5083 friction stir lap welds during post-weld annealing treatment at 350, 400 and 450 °C for 30 to 180 min. Optical microscope (OM), field emission gun scanning electron microscope (FEG-SEM) and transmission electron microscope (TEM) were employed to investigate the structure of the weld zone. The thickness and composition of the IM layers were evaluated using image analysis system and electron back-scatter diffraction (EBSD), respectively. Moreover, kernel average misorientation (KAM) analysis was performed to evaluate the level of stored energy in the as-welded state. The results showed that the growth kinetics of the IM layer was not governed by a parabolic diffusion law. Presence of the IM compounds as well as high stored energy near the joint interface of the as-welded sample was recognized to be the origin of the observed deviation from the parabolic diffusion law. - Highlights: • This work provided a new insight into growth kinetics of Al–Fe IM thickness. • The growth kinetics of IM layer was not governed by a parabolic diffusion law. • IM near the joint interface was the origin of deviation from the parabolic law. • High stored energy at joint interface was origin of deviation from parabolic law.

36 MATERIALS SCIENCE↗
DOE OSTI2013

A feasibility study for experimentally determining dynamic force distribution in a lap joint

Developing constitutive models of the physics in mechanical joints is currently stymied by inability to measure forces and displacements within the joint. The current state of the art estimates whole joint stiffness and energy loss per cycle from external measured force input and one or two acceleration responses. To validate constitutive models beyond this state requires a measurement of the distributed forces and displacements at the joint interface. Unfortunately, introducing measurement devices at the interface completely disrupts the desired physics. A feasibility study is presented for a non-intrusive method of solving for the interface dynamic forces from an inverse problem using full field measured responses. The responses come from the viewable surface of a beam. The noise levels associated with digital image correlation and continuous scanning laser Doppler velocimetry are evaluated from typical beam experiments. Two inverse problems are simulated. One utilizes the extended Sum of Weighted Accelerations Technique (SWAT). The second is a new approach dubbed the method of truncated orthogonal forces. These methods are much more robust if the contact patch geometry is well identified. Various approaches to identifying the contact patch are investigated, including ion marker tracking, Prussian blue and ultrasonic measurements. A typical experiment is conceived for a beam which has a lap joint at one end with a single bolt connecting it to another identical beam. In a virtual test using the beam finite element analysis, it appears that the SWAT inverse method requires evaluation of too many coefficients to adequately identify the force distribution to be viable. However, the method of truncated orthogonal forces appears viable with current digital image correlation (and probably other) imaging techniques.

47 OTHER INSTRUMENTATION↗