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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 91 records · Page 5
All sourcesNASA NTRSDOE OSTI
NASA NTRS1979

Measurement techniques for trace metals in coal-plant effluents: A brief review

The strong features and limitations of techniques for determining trace elements in aerosols emitted from coal plants are discussed. Techniques reviewed include atomic absorption spectroscopy, charged particle scattering and activation, instrumental neutron activation analysis, gas/liquid chromatography, gas chromatographic/mass spectrometric methods, X-ray fluorescence, and charged-particle-induced X-ray emission. The latter two methods are emphasized. They provide simultaneous, sensitive multielement analyses and lend themselves readily to depth profiling. It is recommended that whenever feasible, two or more complementary techniques should be used for analyzing environmental samples.

Singh, J. J.↗
NASA NTRS1994

Igneous inclusions from ordinary chondrites: High temperature cumulates and a shock melt

We report microprobe, instrumental neutron activation analysis, and radiochemical neutron activation analysis data for three large igneous inclusions in the Yamato (Y-)75097, Y-793241, and Y-794046 ordinary chondrites. The inclusions in the first two chondrites are troctolitic cumulates that have undergone appreciable reactions with their hosts either during emplacement and/or cooling. Olivine-spinel Fe-Mg exchange pairs in these two inclusions record equilibration temperatures of about 710 C, and these temperatures are similar to those exhibited by mineral pairs in the Y-75097 and Y-793241 hosts. The inclusion in Y-794046 is texturally unique, consisting of fine-grained, randomly distributed olivines, coarse (approximately 2 mm) fascicular pyroxene laths, and angular pockets of maskelynite/plagioclase feldspar. The phase compositions are readily interpreted as having resulted from extremely rapid, essentially isochemical cooling to temperatures less than 1000 C of a melt with an initial temperature greater than 1670 C. We suggest that this igneous inclusion formed in-situ by shock.

Sack, Richard O.↗
NASA NTRS1973

Evaluation of radioisotope tracer and activation analysis techniques for contamination monitoring in space environment simulation chambers

Radioisotope measurement techniques and neutron activation analysis are evaluated for use in identifying and locating contamination sources in space environment simulation chambers. The alpha range method allows the determination of total contaminant concentration in vapor state and condensate state. A Cf-252 neutron activation analysis system for detecting oils and greases tagged with stable elements is described. While neutron activation analysis of tagged contaminants offers specificity, an on-site system is extremely costly to implement and provides only marginal detection sensitivity under even the most favorable conditions.

Smathers, J. B.↗
NASA NTRS1972

Applications of activation analysis to geochemical, meteoritic and lunar studies.

The application of activation analysis techniques to the analysis of cosmological materials, i.e., terrestrial, tektitic, meteoritic, and lunar matter, is reviewed. Elemental determinations can be made by instrumental fast-neutron and thermal-neutron activation analysis, photonuclear and charged-particle activation analysis, and by radiochemical neutron activation analysis. Partition-coefficient methods, autoradiography studies, gamma-gamma coincidence counting, and age determination by neutron activation are discussed. Attention is given to K-Ar and I-Xe dating of meteorites.

Showalter, D. L.↗
NASA NTRS1989

Relativistic neutrons in active galactic nuclei

The acceleration of protons to relativistic energies in active galactic nuclei leads to the creation of relativistic neutrons which escape from the central engine. The neutrons decay at distances of up to 1-100 pc, depositing their energies and momenta in situ. Energy deposition by decaying neutrons may inhibit spherical accretion and drive a wind, which could be responsible for the velocity fields in emission-line regions and the outflow of broad absorption line systems. Enhanced pressure in the neutron decay region may also help to confine emission line clouds. A fraction of the relativistic proton energy is radiated in gamma-rays with energies which may be as large as about 100,000 GeV.

Sikora, Marek↗
NASA NTRS1974

Chemical studies of Apollo 16 and 17 samples

Instrumental neutron activation analyses were conducted to nine Apollo 16 samples and 23 Apollo 17 samples. Radiochemical neutron activation analyses were carried out in the case of six Apollo 16 boulder-2 rocks, five Apollo 17 soils, and one Apollo 16 soil. The elemental abundances obtained are presented in tables and the significance of the analytical results is discussed. Attention is also given to interelement correlations.

Laul, J. C.↗
NASA NTRS1973

Analytical and Radio-Histo-Chemical Experiments of Plants and Tissue Culture Cells Treated with Lunar and Terrestrial Materials

The nature and mechanisms of the apparent simulation of growth originally observed in plants growing in contact with lunar soil during the Apollo project quarantine are examined. Preliminary experiments employing neutron activated lunar soil indicate uptake of a few elements by plants. It was found that while the preliminary neutron activation technique allowed demonstration of uptake of minerals it presented numerous disadvantages for use in critical experiments directed at elucidating possible mechanisms of stimulation.

Halliwell, R. S.↗
NASA NTRS1974

Breccia 66055 and related clastic materials from the Descartes region, Apollo 16

Trace and major element contents obtained by instrumental neutron activation are reported for a number of Apollo 16 soil samples and miscellaneous breccia fragments. In addition, data obtained by instrumental neutron activation and electron microprobe techniques along with petrographic descriptions are presented for selected subsamples of breccia 66055. The compositions of our soil samples can be modeled by mixtures of various amounts of anorthosite, anorthositic gabbro and low-K Fra Mauro basalt components. These mixtures are typical of those found in a number of petrographic surveys of the fines. Breccia 66055 is a complex regolith breccia which consists of at least four distinct types of microbreccias. No systematic relation with respect to stratigraphic age among the various microbreccia types was observed. Compositionally and texturally, the clasts which compose breccia 66055 are similar to a number of previously reported rock types from the Apollo 16 area. The entire breccia appears to have undergone a complex history of thermal metamorphism. We conclude from the study of these samples that the Cayley Formation is probably homogeneous in its gross compositional and petrographic aspects.

Fruchter, J. S.↗
NASA NTRS1974

Major and trace element concentrations in samples from 72275 and 72255

Analytical data have been obtained for Co, Sc, Hf, Zn, Cr, Ga, Rb, Cs, Ni, major elements, and rare earth elements in eight samples from boulder 1. The data for trace elements were obtained by radiochemical neutron activation analysis. Major elements, except Na and Mn, were obtained by atomic absorption spectral photometry. Values for Na and Mn were obtained by neutron activation analysis of the same powder that was later dissolved to provide the atomic absorption analyses.

Haskin, L. A.↗
NASA NTRS1975

Extinct superheavy element in the Allende meteorite

Radiochemical neutron activation analysis of seven Allende samples for 26 trace elements were conducted. In addition, Cr and Fe were studied with the aid of instrumental neutron activation analysis. The investigation had the objective to identify the extinct superheavy element which was present in meteorites and decayed to Xe isotopes by spontaneous fission. The superheavy element was found to reside mainly in a rare mineral (probably a Fe, Ni, Cr, Al-sulfide), comprising only 0.04% of the meteorite. It is pointed out that of the nine volatile superheavy elements 111 to 119, only 115, 114, and 113 are expected to condense as sulfides in the temperature interval between 400 and 500 K corresponding to mineral formation conditions in the solar nebula.

Anders, E.↗
NASA NTRS1989

Lunar meteorites - Siderophile element contents, and implications for the composition and origin of the moon

Data for 10 siderophile elements in all of the known lunar meteorites except for Y793274 are reported. Bulk compositional data for Ni, Ge, Cd, Re, Os, Ir, and Au were obtained from radiochemical neutron activation analysis (Warren et al., 1986). Data for Fe, Co, and Zn, and additional data for Ni, Ir, and Au were obtained by instrumental neutron activation analysis (Kallemeyn et al., 1988). Except for the case of Au in Y791197, there was good agreement between the results obtained by the two methods. The differences observed between the lunar-meteoritic regolith samples and central nearside highlands regolith samples are discussed.

Warren, Paul H.↗
NASA NTRS1981

Composition of the earth's upper mantle. I - Siderophile trace elements in ultramafic nodules

The considered investigation is concerned with a reexamination of the question of the distribution of siderophile elements in the earth's upper mantle, taking into account a more unified data base which is now available. A comprehensive suite of ultramafic inclusions was collected as part of the Basaltic Volcanism Study Project and has been analyzed by instrument neutron activation analysis for major, minor, and some lithophile trace elements. In addition, 18 of these rocks and the important sheared garnet lherzolite PHN 1611 have been analyzed by means of radiochemical neutron activation analysis for 7 siderophile elements (Au, Ge, Ir, Ni, Os, Pd, and Re) and 9 volatile elements (Ag, Bi, Cd, In, Sb, Se, Te, Tl, and Zn). The siderophile element data reveal interesting inter-element correlations, which were not apparent from the compiled abundance tables of Ringwood and Kesson (1976) and Chou (1978).

Morgan, J. W.↗
NASA NTRS1993

Trace-element composition of Chicxulub crater melt rock, K/T tektites and Yucatan basement

The Cretaceous/Tertiary (K/T) boundary Chicxulub impact is the best preserved large impact in the geologic record. The Chicxulub crater has been buried with no apparent erosion of its intracrater deposits, and its ejecta blanket is known and is well preserved at hundreds of localities globally. Although most of the molten material ejected from the crater has been largely altered, a few localities still preserve tektite glass. Availability of intra- and extracrater impact products as well as plausible matches to the targeted rocks allows the comparison of compositions of the different classes of impact products to those of the impacted lithologies. Determination of trace-element compositions of the K/T tektites, Chicxulub melt rock, and the targeted Yucatan silicate basement and carbonate/evaporite lithologies have been made using instrumental neutron activation analysis (INAA) and inductively coupled plasma mass spectrometry (ICP-MS). Some sample splits were studied with both techniques to ensure that inter-laboratory variation was not significant or could be corrected. The concentration of a few major and minor elements was also checked against microprobe results. Radiochemical neutron activation analysis (RNAA) was used to determine Ir abundances in some samples.

Hildebrand, A. R.↗
NASA NTRS1971

The measurement of radiation exposure of astronauts by radiochemical techniques

Gamma analyses of the neutron-activated fecal samples from the Apollo 12 and 13 missions were completed, and the data are being evaluated. Samples of the exposed Apollo 12 solar wind composition foil and blank foils were obtained for analysis of the Po-2/0 (Pb-210, Rn-222) content. It is expected that the determination of the Po-210 content of these foils will yield the concentration of radon atoms incident on the foil while exposed to the lunar atmosphere, and this indirectly will permit an estimate of the average uranium concentration of the lunar surface. Proposals to measure the cosmic-ray intensity and energy spectra inside and outside of late Apollo and Project Skylab spacecraft by exposing and subsequently analyzing pure metal foils, and to measure the elemental mass balance in Project Skylab astronauts by instrumental neutron activation analysis of the intake and excreta are summarized.

Brodzinski, R. L.↗
NASA NTRS2002

Cosmochemical Studies: Meteorites, Asteroidal Processes, Chondrules

Our research mainly concerned the asteroidal processes involved in the formation of meteorites and meteoritic chondrules. We continued to generate large amounts of instrumental-neutron-activation analysis (INAA) data, both for irons, chondrites and primitive achondrites. Major themes of our chondrule research were: (1) the temperature and crystallization history of individual chondrules, and (2) the evolution of the solar nebula during the period within which chondrule formation occurred. Much of our chondrule research was focused on the highly primitive CO3 chondrites. We initiated a study of the cooling history of high-FeO chondrules by characterizing the overgrowth layers on relict grains.. We also continued our studies of the composition and the formation of iron meteorites and the evolution of their parent planets. The large data sets that we have generated at UCLA allows systematic comparisons of the large magmatic groups both in terms of fractional crystallization (including rough estimates of non-metal contents of the parental melts) and in terms of the effects of variable contents of trapped melt. We have completed a preliminary study of group IIIAB in which we developed a trapped-melt model and more detailed studies of group IVA and the main-group pallasites. By comparing these large groups and modeling them by a combination of crystallization and melt trapping, we are able to better define both the formation processes and the nature of the solid/liquid elemental partitioning. We helped maintain the excellent neutron-activation facilities at UCLA, a major resource for the cosmochemical community.

Wasson, John T.↗