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All sourcesNASA NTRSDOE OSTI
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Robust and Mass Efficient Thermal Protection Systems for Future Venus Missions

Several international Venus missions, both orbiter, and in-situ probe are in the works after a prolonged absence. Future missions are expected to be long-duration lander missions and balloon missions to investigate the cloud layer. The entry mass for these in-situ missions will be significantly higher, and the aeroshell will be larger, than previous missions. Two cardinal requirements govern the selection and use of thermal protection systems (TPS), namely, robustness to assure mission safety during entry and mass efficiency so that the useful mass for science is maximized. One cannot trade mission safety for mass when it comes to TPS. The robustness of the TPS is a paramount requirement as it is a single point of system failure. At the same time, TPS mass is carried for the entire mission duration prior to entry, and any excess TPS mass is at the cost of science payload. Future missions will benefit enormously from TPS options with mass and performance benefits far beyond advanced carbon-carbon (ACC) that is currently proposed for the DAVINCI mission. NASA STMD, and SMD jointly invested in the development of 3-D woven thermal protection systems in the last decade, and as a result, the Heat-shield for Extreme Entry Environment Technology (HEEET) TPS has been matured to TRL 6. It is ready for future mission use including Venus. The HEEET project focused on developing a broad technology base, applicable for missions not only to Venus, but also to Saturn, the Ice Giants, and higher speed sample return missions such as Mars Sample Return requiring extreme robustness due to bio-hazards. The dual-layer HEEET (DL-HEEET) is proven to be extremely robust. DL-HEEET performed well in arc jet and laser testing conditions where heritage carbon-phenolic failed. HEEET also proved to be more mass efficient compared to Carbon-Phenolic. Recently, the principal author was invited to present his perspectives to the 2023-2032 Planetary Sciences Decadal Venus subcommittee on the current state of TPS for future Venus missions [1]. In addition to pointing out successful TPS and other developments in the last decade in support of entry systems, the principal author made two findings: 1) importance of and need to sustain TPS capabilities that took nearly a decade to develop and 2) the opportunity to further optimize TPS mass without sacrificing robustness to further enable future in-situ missions. This talk will focus on the above two recommendations and provide the rationale for them. The intent of the talk is to seek advocacy from the VEXAG community for the criticality of TPS sustainment and the benefits of 3D woven TPS optimization. TPS Capability Sustainment: HEEET development was necessitated by the atrophy of heritage carbon-phenolic. Atrophy has impacted other TPS materials as well. Avcoat, the TPS that successfully allowed astronauts to explore the Moon in the 1960s and 70s, took nearly a decade and $10’sM to recover in support of Orion/Artemis. One of the most used TPS materials, SLA 561V, had to be recovered prior to its use on Mars Pathfinder. Phenolic Impregnated Carbon Ablator (PICA), the TPS that replaced SLA 561V on MSL, has undergone multiple replacements and recovery due to constituent rayon changes. Recently, NASA invested in a domestic rayon replacement program and also invested in FMI to consolidate PICA capability for NASA missions, as a result of FMI’s decision to discontinue commercial FiberForm, which is needed for PICA. TPS used for planetary missions are unique and have no other commercial or defense use. In addition, low mission cadence is also a driver for TPS atrophy. Hence, NASA, as the steward, must take steps to ensure and sustain TPS capabilities. In this talk, we outline steps NASA can take to keep abreast of emerging risks and target risk mitigation steps to ensure TPS capability sustainment for Venus and other extreme environment missions. Next Generation of Mass efficient and Robust TPS: NASA invested in an alternate TPS to PICA based on felt-technology called Conformal-PICA which has the potential to save 30% - 50% mass over PICA. The development was discontinued at a Technology Readiness Level (TRL) of ~ 5. 3D Mid-Density Carbon Phenolic (3MDCP) is a single layer variant of HEEET, based on the insulating layer only (SL-HEEET) and currently baselined for the Mars Sample Return Mission Earth Entry System due to its mass efficiency (30% more mass efficient than DL- HEEET). Currently, SL-HEEET is limited to aeroshell diameters of < 1.3m. The SL-HEEET was compared to DL-HEEET in the recent ADVENT flag-ship class mission study in support of the Planetary Science Decadal. SL HEEET was the recommended TPS based on 30% mass savings for both the balloon and lander missions. Given C-PICA and SL-HEEET have superior reliability and mass efficiency, advocacy from VEXAG is sought for completing their further development to TRL 5/6 in this decade so as to enable TPS readiness for future missions.

Thermal Protection Systems↗
DOE OSTI2022

Continuous Additive Manufacturing using Olefin Metathesis

Abstract The development of chemistry is reported to implement selective dual‐wavelength olefin metathesis polymerization for continuous additive manufacturing (AM). A resin formulation based on dicyclopentadiene is produced using a latent olefin metathesis catalyst, various photosensitizers (PSs) and photobase generators (PBGs) to achieve efficient initiation at one wavelength (e.g., blue light) and fast catalyst decomposition and polymerization deactivation at a second (e.g., UV‐light). This process enables 2D stereolithographic (SLA) printing, either using photomasks or patterned, collimated light. Importantly, the same process is readily adapted for 3D continuous AM, with printing rates of 36 mm h –1 for patterned light and up to 180 mm h –1 using un‐patterned, high intensity light.

36 MATERIALS SCIENCE↗
DOE OSTI2021

3D printing of lignin: Challenges, opportunities and roads onward

Abstract As the second most abundant biopolymer on earth, and as a resource recently becoming more available in separated and purified form on an industrial scale due to the development of new isolation technologies, lignin has a key role to play in transitioning our material industry towards sustainability. Additive manufacturing (AM), the most efficient‐material processing technology to date, has likewise made great strides to promote sustainable industrial solutions to our needs in engineered products. Bringing lignin research to AM has prompted the emergence of the nascent “lignin 3D printing” field. This review presents the recent state of art of this promising field and highlights its challenges and opportunities. Following a review of the industrial availability, molecular attributes, and associated properties of technical lignins, we review R&D efforts at implementing lignin systems in extrusion‐based and stereolithography (SLA) printing technologies. Doing so underlines the adage of lignin research that “all lignins are not created equal,” and stresses the opportunity nested in this chemical diversity created mostly by differences in isolation conditions to molecularly select and tune the attributes of technical lignin systems towards desirable properties, be it by modification or polymer blending. Considering the AM design process in its entirety, we finally propose onward routes to bring the full potential to this emerging field. We hope that this review can help promote the unique value and overdue industrial role of lignin in sustainable engineered materials and products.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Does the leaf economic spectrum hold within plant functional types? A Bayesian multivariate trait meta-analysis

The leaf economic spectrum is a widely-studied axis of plant trait variability that defines a trade-off between leaf longevity and productivity. While this has been investigated at the global scale, where it is robust, and at local scales, where deviations from it are common, it has received less attention at the intermediate scale of PFTs. We investigated whether global leaf economic relationships are also present within the scale of plant functional types (PFTs) commonly used by Earth System models, and the extent to which this global-PFT hierarchy can be used to constrain trait estimates. We developed a hierarchical multivariate Bayesian model that assumes separate means and covariance structures within and across PFTs and fit this model to seven leaf traits from the TRY database related to leaf longevity, morphology, biochemistry, and photosynthetic metabolism. Although patterns of trait covariation were generally consistent with the leaf economic spectrum, we found three approximate tiers to this consistency. Relationships among morphological and biochemical traits (SLA, N, P) were the most robust within and across PFTs, suggesting that covariation in these traits is driven by universal leaf construction trade-offs and stoichiometry. Relationships among metabolic traits (R_d, V_{c,max}, J_max) were slightly less consistent, reflecting in part their much sparser sampling (especially for high-latitude PFTs), but also pointing to more flexible plasticity in plant metabolistm. Finally, relationships involving leaf lifespan were the least consistent, indicating that leaf economic relationships related to leaf lifespan are dominated by across-PFT differences and that within-PFT variation in leaf lifespan is more complex and idiosyncratic. Across all traits, these covariance were an important source of information, as evidenced by the improved imputation accuracy and reduced predictive uncertainty in multivariate models compared to univariate models. Ultimately, our study reaffirms the value of studying not just individual traits but the multivariate trait space and the utility of hierarchical modeling for studying the scale dependence of trait relationships.

biodiversity, ecological modeling, ecology, leaf b↗
DOE OSTI2022

Physical Models from Physical Templates Using Biocompatible Liquid Crystal Elastomers as Morphologically Programmable Inks For 3D Printing

Advanced manufacturing has received considerable attention as a tool for the fabrication of cell scaffolds however, finding ideal biocompatible and biodegradable materials that fit the correct parameters for 3D printing and guide cells to align remain a challenge. Herein, a photocrosslinkable smectic-A (Sm-A) liquid crystal elastomer (LCE) designed for 3D printing is presented, that promotes cell proliferation but most importantly induces cell anisotropy. The LCE-based bio-ink allows the 3D duplication of a highly complex brain structure generated from an animal model. Vascular tissue models are generated from fluorescently stained mouse tissue spatially imaged using confocal microscopy and subsequently processed to create a digital 3D model suitable for printing. The 3D structure is reproduced using a Digital Light Processing (DLP) stereolithography (SLA) desktop 3D printer. Synchrotron Small-Angle X-ray Diffraction (SAXD) data reveal a strong alignment of the LCE layering within the struts of the printed 3D scaffold. The resultant anisotropy of the LCE struts is then shown to direct cell growth. This study offers a simple approach to produce model tissues built within hours that promote cellular alignment.

3D cell culture↗
DOE OSTI2020

3D-printing methacrylate/chitin nanowhiskers composites via stereolithography: Mechanical and thermal properties

We report on the mechanical and thermal properties of stereolithography (SLA) 3D-printed methacrylate (MA) resin reinforced by chitin nanowhiskers (CNWs). CNWs were synthesized by acid hydrolysis of crab shell chitin and nanocomposites with 0 wt%, 0.5 wt%, 1.0 wt%, and 1.5 wt% CNWs loading were prepared by slurry compounding method. The obtained CNWs (diameter = 23 ± 5 nm, length = 253 ± 100 nm, and aspect ratio = 11 ± 3) are well dispersed within the bulk of MA at 1.0 wt% loading, implying good interfacial adhesion between the nanofiller and the resin matrix possibly due to hydrogen bonding interactions. The addition of up to 1.0 wt% CNWs to neat MA enhances the tensile strength, strain at break, modulus, and maximum thermal degradation temperatures of the nanocomposites. Moreover, the incorporation of CNWs not only improves the mechanical and thermal properties, but also preserves the excellent resolution and accuracy of 3D-printed MA/CNWs nanocomposites.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Cyber-Physical Smart Light Control System Integration with Smart Grid using Zigbee

This paper presents a hardware-in-the-loop cyber-physical system architecture design to monitor and control smart lights connected to the active distribution grid. The architecture uses Zigbee-based (IEEE 802.15.4) wireless sensor networks and publish-subscribe architecture to exchange monitoring and control signals between smart-light actuators (SLAs) and a smart-light central controller (SLCC). Each SLA integrated into a smart light consists of a Zigbee-based endpoint module to send and receive signals to and from the SLCC. The SLCC consists of a Zigbee-based coordinator module, which further exchanges the monitoring and control signals with the active distribution management system over the TCP/IP communication network. The monitoring signals from the SLAs include light status, brightness level, voltage, current, and power data, whereas, the control signals to the SLAs include light intensity, turn ON, turn OFF, standby, and default settings. We have used our existing hardware-in-the-loop (HIL) cyber-physical system (CPS) security SCADA testbed to process signals received from the SLCC and respond suitable control signals based on the smart light schedule requirements, system operation, and active distribution grid dynamic characteristics. We have integrated the proposed cyber-physical smart light control system (CPSLCS) testbed to our existing HIL CPS SCADA testbed. We use the integrated testbed to demonstrate the efficacy of the proposed algorithm by real-time performance and latency between the SLCC and SLAs. The experiments demonstrated significant results by 100% realtime performance and low latency while exchanging data between the SLCC and SLAs.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2020

Experimental Investigation of Sweeping Jet Film Cooling in a Transonic Turbine Cascade

Abstract The sweeping jet (SJ) film cooling hole has shown promising cooling performance compared to the standard shaped hole in low-speed conditions. The present work demonstrates the first attempt of SJ film cooling at an engine relevant Mach number. An experimental investigation was conducted to study the SJ film cooling on a nozzle guide vane suction surface. A well-established additive manufacturing technique commonly known as stereolithography (SLA) was utilized to design a transonic, engine representative vane geometry in which a row of SJ holes was used on the vane suction surface. Experiments were performed in a linear transonic cascade at an exit Mach number of 0.8 and blowing ratios of BR = 0.25–2.23. The measurement of heat transfer was conducted with the transient IR method, and the convective heat transfer coefficient (HTC) and adiabatic film cooling effectiveness were estimated using a dual linear regression technique (DLRT). Aerodynamic loss measurements were also performed with a total pressure Kiel probe at 0.25Cax downstream of the exit plane of the vane cascade. Experiments were also conducted for a baseline-shaped hole (777-hole) for a direct comparison. Results showed that the SJ hole has a wider coolant spreading in the lateral direction near the hole exit due to its sweeping motion that improves the overall cooling performance particularly at high blowing ratios (BR > 1). Aerodynamic loss measurement suggested that the SJ hole has a comparable total pressure loss to the 777-shaped hole.

Engineering↗
DOE OSTI2020

Data from: "Growth strategies and threshold responses to water deficit modulate effects of warming on tree seedlings from forest to alpine"

This data package contains data that were used to support conclusions drawn in “Growth strategies and threshold responses to water deficit modulate effects of warming on tree seedlings from forest to alpine”, by Lazarus, Castanha et al. 2017. Data were collected at field sites within the Alpine Treeline Warming Experiment (ATWE) on Niwot Ridge, Colorado, USA, and at the U.S. Geological Survey laboratory located in Boise, Idaho. This archive contains comma-separated-values (.csv) files, as well as the same files in Microsoft Excel (.xlsx) format, which can be opened by either Microsoft Excel, R, or any simple text editor program. There are two types of geospatial data files: .kml and ESRI shapefiles (.shp). The kml files contain placemarks, which can be opened by Google Earth, or Google Maps. The ESRI shapefiles can be opened by any geographic information system application that can read shapefiles, including ESRI's entire ArcGIS suite, and QGIS. We asked whether and how tree species differences in response to water deficit relates to their establishment along the gradient from forest to alpine. To do this, we compared growth and moisture stress responses in first-year seedlings of three species planted in common gardens subject to a factorial of heating and watering treatments below, at, and above tree line. This combination of an elevation gradient alongside warming and watering treatments enabled us to observe species differences in seedling responses to a broad set of climatic conditions.Entire seedlings were harvested at c. 3- and again at 9 weeks of age following germination/emergence in the experimental plots, and we then measured dry mass (DM) of above and belowground parts, root length, root mass fraction (RMF), relative growth rates (RGRs) from seed to 3 weeks and from 3 to 9 weeks, turgor-loss point (TLP), and photosynthetic WUE (as δ13C). Also included in this dataset (but not described in the manuscript) are measures of specific leaf area (SLA) and other variables generated by pressure-volume curves (saturated water content, osmotic potential at full turgor, elastic modulus).

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2024

Analytical Assessment of Impurities Found in Process Gases using the InfiTOF, a High Resolution, Low Mass, Variable Time-of-Flight Mass Spectrometer

The JEOL InfiToF is a high-resolution, low mass (HRLM) mass spectrometer (MS) with the application potential to meet analytical needs for tritium handling systems, such as those at the Savannah River Tritium Facilities (SRTE) and those used in fusion research. The Service Level Agreement (SLA) #144 line 27 “InfiTOF R&D” has concluded its first year of efforts under Tritium Recycle and Renewal. The project goals for FY22 were: (1) Production of a finalized modification list for tritium hardened components in the InfiTOF, (2) perform an assessment on impurity gases commonly found in process gases from Tritium Facilities and (3) begin developing a set of standardized work instructions that will be used as a basis for operations on the InfiTOF.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2021

Cutting out the middleman: calibrating and validating a dynamic vegetation model (ED2-PROSPECT5) using remotely sensed surface reflectance

Canopy radiative transfer is the primary mechanism by which models relate vegetation composition and state to the surface energy balance, which is important to light- and temperature-sensitive plant processes as well as understanding land–atmosphere feedbacks. In addition, certain parameters (e.g., specific leaf area, SLA) that have an outsized influence on vegetation model behavior can be constrained by observations of shortwave reflectance, thus reducing model predictive uncertainty. Importantly, calibrating against radiative transfer outputs allows models to directly use remote sensing reflectance products without relying on highly derived products (such as MODIS leaf area index) whose assumptions may be incompatible with the target vegetation model and whose uncertainties are usually not well quantified. Here, we created the EDR model by coupling the two-stream representation of canopy radiative transfer in the Ecosystem Demography model version 2 (ED2) with a leaf radiative transfer model (PROSPECT-5) and a simple soil reflectance model to predict full-range, high-spectral-resolution surface reflectance that is dependent on the underlying ED2 model state. We then calibrated this model against estimates of hemispherical reflectance (corrected for directional effects) from the NASA Airborne Visible/Infrared Imaging Spectrometer (AVIRIS) and survey data from 54 temperate forest plots in the northeastern United States. The calibration significantly reduced uncertainty in model parameters related to leaf biochemistry and morphology and canopy structure for five plant functional types.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2021

Vegetation Warming Experiment: 15N Uptake Experiment Arctagrostis latifolia Canopy Traits, Utqiagvik (Barrow), Alaska, 2018

This dataset consists of measured Arctagrostis latifolia canopy traits harvested from vegetation warming experiment enclosures and paired control plots located on the BEO, Utqiavik, Alaska. Harvest types include both natural abundance and enriched A. latifolia. Canopy traits measured include leaf area index (LAI), specific leaf area (SLA) and maximum height. Vegetation warming chambers (Zero Power) were deployed on the Barrow Environmental Observatory (BEO), Utqiavik, Alaska. These chambers (Figure 1) consistently elevated air temperatures by approximately 4°C using a self-venting system described by Lewin et al (2017). Five chambers were deployed from June 17, 2018 to September 24, 2018 on the BEO within a 1 km2 area centered on 71.275N, -156.641W. Each chamber was co-located with an ambient plot where temperatures were not manipulated on patches of tundra containing the target species Arctagrostis latifolia. An intensive field campaign in late July investigated the impact of warming had on A. latifolia biomass, chemistry, and uptake of 15N labeled ammonia that was injected into the surface soils for one week. Initial measurements were taken on July 21, 2018. Harvest occurred on July 27, 2018. Water-extractable nutrients in soils were measured in July following harvests of A. latifolia plants and underlying soils. Availability of ammonia, nitrate, and phosphate throughout the growing season was measured by extracting nutrients bound to anion and cation binding resins deployed from July through September. Environmental variables (thaw depth, surface soil temperatures, surface soil moisture) were measured. Leaf traits and root traits of A. latifolia were also measured. This dataset includes one csv file and one pdf file. The Next-Generation Ecosystem Experiments: Arctic (NGEE Arctic), was a research effort to reduce uncertainty in Earth System Models by developing a predictive understanding of carbon-rich Arctic ecosystems and feedbacks to climate. NGEE Arctic was supported by the Department of Energy's Office of Biological and Environmental Research. The NGEE Arctic project had two field research sites: 1) located within the Arctic polygonal tundra coastal region on the Barrow Environmental Observatory (BEO) and the North Slope near Utqiagvik (Barrow), Alaska and 2) multiple areas on the discontinuous permafrost region of the Seward Peninsula north of Nome, Alaska. Through observations, experiments, and synthesis with existing datasets, NGEE Arctic provided an enhanced knowledge base for multi-scale modeling and contributed to improved process representation at global pan-Arctic scales within the Department of Energy's Earth system Model (the Energy Exascale Earth System Model, or E3SM), and specifically within the E3SM Land Model component (ELM).

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1971

The Smithsonian Earth Physics Satellite (SEPS) definition study, volumes 1 through 4

A limited Phase B study was undertaken to determine the merit and feasibility of launching a proposed earth physics satellite with Apollo-type hardware. The study revealed that it would be feasible to launch this satellite using a S-IB stage, a S-IVB with restart capability, an instrument unit, a SLA for the satellite shroud, and a nose cone (AS-204 configuration). A definition of the proposed satellite is provided, which is specifically designed to satisfy the fundamental requirement of providing an orbiting benchmark of maximum accuracy. The satellite is a completely passive, solid 3628-kg sphere of 38.1-cm radius and very high mass-to-area ratio (7980 kg sq mi). In the suggested orbit of 55 degrees inclination, 3720 km altitude, and low eccentricity, the orbital lifetime is extremely long, so many decades of operation can be expected.

Source record↗
NASA NTRS1977

The far-infrared spectrum of the core of Sagittarius B2

A Michelson interferometer aboard NASA's Kuiper Airborne Observatory has been used to measure the spectrum of Sgr B2 from 40 to 200 kaysers with 5-kayser resolution in a 1.4-arcmin beam. The measured spectrum is smooth and featureless with a broad maximum at about 85 kaysers. The data can be fitted analytically with a model corresponding to thermal emission by a uniform sla of dust filling the beam, with an average temperature of approximately 32 K, an optical depth at 100 microns of about 1.6, and a spectral index of the dust emissivity about 1.5. The absence of features implies either that the source is optically thick or that the emission spectrum of the individual grains is smooth in the passband. The possible physical significance of this model is discussed.

Erickson, E. F.↗
NASA NTRS1981

Thermal design of the Space Shuttle External Tank

The history of the engineering and manufacturing requirements leading to the final Thermal Protection System (TPS) for the External Tank (ET) is presented. The thermal design for the ET must be optimized, based on considerations of cost, weight, and application of the TPS. The significant thermal requirements include the structural and component temperature limits, the propellant quality, the minimization of ice and frost, no air liquefaction, and no film boiling. The TPS materials selected to meet the requirements are a low density closed cell foam (CPR-488) and two light-weight ablators (SLA-56 and MA-25s). The first four flights of the Space Shuttle (1981) will measure and evaluate external environmental, structural, propulsion, electrical, and engine performance data. The ET will be instrumented to measure acoustics, pressures, heat transfer, vibration, temperatures, and structural strains. TPS weight reductions are planned for future ETs through the use of a comprehensive thermal instrumentation system.

Warmbrod, J. D.↗
NASA NTRS1985

Thermal design of the space shuttle external tank

The shuttle external tank thermal design presents many challenges in meeting the stringent requirements established by the structures, main propulsion systems, and Orbiter elements. The selected thermal protection design had to meet these requirements, and ease of application, suitability for mass production considering low weight, cost, and high reliability. This development led to a spray-on-foam (SOFI) which covers the entire tank. The need and design for a SOFI material with a dual role of cryogenic insulation and ablator, and the development of the SOFI over SLA concept for high heating areas are discussed. Further issuses of minimum surface ice/frost, no debris, and the development of the TPS spray process considering the required quality and process control are examined.

Bachrtel, F. D.↗
NASA NTRS1994

Preparation And Analysis Of Specimens Of Ablative Materials

Procedure for chemical analysis of specimens of silicone-based ablative thermal-insulation materials SLA-561 and MA25 involves acid digestion of specimens to prepare them for analysis by inductively-coupled-plasma/atomic-emission spectroscopy (ICP/AES). In comparison with atomic-absorption spectroscopy (AAS), ICP/AES is faster and more accurate than AAS. Results of analyses stored in data base, used to trace variations in concentrations of chemical elements in materials during long-term storage, and used in timely manner in investigations of failures. Acid-digestion portion of procedure applied to other thermal-insulation materials containing room-temperature-vulcanizing silicones and enables instrumental analysis of these materials.

Solomon, William C.↗