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At least 91 records · Page 5

Spectroscopic analysis of radiation-generated changes in tensile properties of a polyetherimide film

The effects of electron radiation on Ultem, a polyetherimide were studied for doses from 2 x 10 to the 9th power to 6 x 10 to the 9th power rad. Specimens were studied for tensile property testing and for electron paramagnetic resonance and infrared spectroscopic measurements of molecular structure. A Faraday cup design and a method for remote temperature measurement were developed. The spectroscopic data show that radiation caused dehydrogenation of methyl groups, rupture of main-chain ether linkage, and opening of imide rings, all to form radicals and indicate that the so-formed atomic hydrogen attached to phenyl radicals, but not to phenoxyl radicals, which would have formed hydroxyls. The observed decays of the radiation-generated phenoxyl, gem-dimethyl, and carbonyl radicals were interpreted as a combining of the radicals to form crosslinking. This crosslinking is the probable cause of the major reduction in the elongation of the tensile specimens after irradiation. Subsequent classical solubility tests indicate that the irradiation caused massive crosslinking.

Long, E. R., Jr.↗

Tensile properties of textile composites

The importance of textile composite materials in aerospace structural applications has been gaining momentum in recent years. With a view to better understand the suitability of these materials in aerospace applications, an experimental program was undertaken to assess the mechanical properties of these materials. Specifically, the braided textile preforms were infiltrated with suitable polymeric matrices leading to the fabrication of composite test coupons. Evaluation of the tensile properties and the analyses of the results in the form of strength moduli, Poisson's ratio, etc., for the braided composites are presented. Based on our past experience with the textile coupons, the fabrication techniques have been modified (by incorporating glass microballoons in the matrix and/or by stabilizing the braid angle along the length of the specimen with axial fibers) to achieve enhanced mechanical properties of the textile composites. This paper outlines the preliminary experimental results obtained from testing these composites.

Avva, V. Sarma↗

The effects of specimen width on tensile properties of triaxially braided textile composites

The objective of this study was to examine the effect of the unit cell architecture on the mechanical response of textile reinforced composite materials. Specifically, the study investigated the effect of unit cell size on the tensile properties of 2D triaxially braided graphite epoxy laminates. The figures contained in this paper reflect the presentation given at the conference. They may be divided into four sections: (1) a short definition of the material system tested; (2) a statement of the problem and a review of the experimental results; (3) experimental results consist of a Moire interferometry study of the strain distribution in the material plus modulus and strength measurements; and (4) a short summary and a description of future work will close the paper.

Masters, John E.↗

Effect of boron on tensile properties of B2 BeAl

Small additions of boron were shown to improve the room temperature ductility of the intermetallic compound Ni3Al. Boron is believed to segregate to the gain boundaries and strengthen them, allowing the inheret ductility of the grains to be achieved. The present study was undertaken to see if boron has a similar effect on the low temperature tensile properties of the equiatomic intermetallic compound FeAl. A binary alloy without boron is compared with an alloy containing 0.78 at % B (0.2 wt %) B, by tensile testing over the temperature range of 300 K to 640 K. Both alloys were processed by powder metallurgy. Results showed that 0.78 at % B addition to FeAl does indeed change the room temperature fracture mode from intergranular to transgranular, suggesting a strengthening of grain boundaries. The alloy containing boron is, however, still brittle at room temperature. A slight decrease in the ductile to brittle transition temperature is, nevertheless, observed. In addition a significant increase in strength of the alloy is observed with boron addition.

Crimp, M.↗

Tensile properties of PRD-49 fiber in epoxy matrix.

Recently a high-modulus and high-strength organic fiber, identified as PRD-49-III by the manufacturer, became commercially available. To assess the fiber performance and its potential as a reinforcement for fiber composites, the tensile properties of the fiber in an epoxy matrix were determined. During this study over 6000 fiber/epoxy strands were made using the filament winding process; these strands were representative samples taken from over 60 lb of single-end fiber. The fiber uniformity, its strength distribution at room and LN2 temperature, stress-strain characteristics, and the strain rate effect on the fiber strength were evaluated.

Chiao, T. T.↗

Tensile Properties of 7075-T6 and 2024-T3 Aluminum-alloy Sheet Heated at Uniform Temperature Rates Under Constant Load

Results are presented of tests to determine the effect of heating at uniform temperature rates from 0.2 degrees to 100 degrees F. per second on the tensile properties of 7075-T6 d(75s-T6) and 2024-T3 (24s-T3) aluminum-alloy sheet under constant-load conditions. Yield and rupture stresses, obtained under rapid-heating conditions, are compared with results of elevated-temperature stress-strain tests for 1/2-hour exposure. Master yield-and-rupture-stress curves based on linear temperature-rate parameter are presented. Yield and rupture stresses and temperatures may be predicted by means of master curves and the parameter.

Heimerl, George J↗

Tensile Properties of Hydrogels and of Snake Skin

Stimulus-responsive or 'smart' gels are of potential interest as sensors and actuators, in industrial separations, and as permeable delivery systems. In most applications, a certain degree of mechanical strength and toughness will be required, yet the large-strain behavior of gels has not been widely reported. Some exceptions include work on gelatin and other food gels, some characterization of soft gels applicable for in-vitro cell growth studies, and toughness determinations on commercial contact lens materials. In general, it can be anticipated that the gel stiffness will increase with increasing degree of crosslinking, but the tensile strength may go through a maximum. Gel properties can be tailored by varying not only the degree of crosslinking, but also the polymer concentration and the nature of the polymer backbone (e.g. its stiffness or solubility). Polypeptides provide an especially interesting case, where secondary structure affects trends in moduli and conformational transitions may accompany phase changes. A few papers on the tensile properties of responsive gels have begun to appear. The responsive hydrogel chosen for the present study, crosslinked hydroxypropylcellulose, shrinks over a rather narrow temperature range near 44 C. Some vertebrate skin is also subject to substantial strain. Among reptiles, the morphologies of the skin and scales show wide variations. Bauer et al. described the mechanical properties and histology of gecko skin; longitudinal tensile properties of snake skin were examined by Jayne with reference to locomotion. The present measurements focus on adaptations related to feeding, including the response of the skin to circumferential tension. Tensile properties will be related to interspecific and regional variation in skin structure and folding.

Hinkley, Jeffrey A.↗

High Temperature Tensile Properties and Fatigue Behavior of a Melt-Infiltrated SiC/SiC Composite

High temperature fatigue behavior of a woven, SiC/SiC ceramic matrix composite (CMC) was investigated in air at two temperatures. The reinforcement for the CMC consisted of 5HS Sylramic(Trademark) fabric with a [0deg/90deg]4s lay-up. The SiC matrix material was infiltrated into the fiber-preform with a slurry-cast, melt-infiltration process. Tensile and fatigue test specimens were machined from the CMC plates. Initially tensile tests were conducted to obtain the average values of tensile properties at 1038 and 1204 C. Subsequently, low-cycle fatigue (LCF) tests with zero and two-hour hold-times at the maximum stress were conducted at the same two temperatures. Fatigue life data generated in the LCF tests were used to determine the geometric mean fatigue lives. In this paper, the tensile behavior and the fatigue durability of the CMC determined under different loading conditions are documented. In addition, reductions observed in the cyclic lives of the composite due to the two hour hold-time at maximum tensile stress are discussed.

Kalluri, Sreeramesh↗

Effect of prior creep at 1365 K on the room temperature tensile properties of several oxide dispersion strengthened alloys

An experimental study was conducted to determine whether oxide dispersion-strengthened (ODS) Ni-base alloys in wrought bar form are subject to creep degradation effects similar to those found in thin-gage sheet. The bar products evaluated included ODS-Ni, ODS-NiCr, and advanced ODS-NiCrAl types; the alloys included microstructures ranging from an essentially perfect single crystal to a structure consisting of very small elongated grains. Tensile test specimens were exposed to creep at various stress levels at 1365 K and then tensile tested at room temperature. Low residual tensile properties, change in fracture mode, appearance of dispersoid free bands, grain boundary cavitation, and/or internal oxidation are interpreted as creep degradation effects. The amount of degradation depends on creep strain, and degradation appears to be due to diffusional creep which produces dispersoid free bands around grain boundaries acting as vacancy sources.

Whittenberger, J. D.↗

Effects of Intermittent Versus Continuous Heating upon the Tensile Properties of 2024-T4, 6061-T6 and 7075-T6 Alloys

In some applications, aluminum alloys are subjected to intermittent heating at elevated temperature. It is generally considered that the effects of such intermittent heating are cumulative, and therefore are the same as if the heating had been continuous for the same total length of time. The object of these tests was to determine the effects of intermittent and continuous heating at 300 and 400 F, for total periods of 100 and 200 hr, upon the tensile properties of 2024-T4 and 6061-T6 alloy rolled-and-drawn rod and 7075-T6 alloy extrusions, at room temperature and at the temperature of heating.

Stickley, G. W.↗

Tensile properties of HA 230 and HA 188 after 400 and 2500 hour exposures to LiF-22CaF2 and vacuum at 1093 K

The solid-to-liquid phase transformation of the nominal LiF-20CaF2 eutectic at 1043 K is considered to be an ideal candidate thermal energy storage mechanism for a space based low temperature Brayton cycle solar dynamic system. Although Co, Fe, and Ni superalloys are thought to be suitable containment materials for LiF based salts, long term containment is of concern because molten fluorides are usually corrosive and Cr can be lost into space through evaporation. Two examples of commercially available superalloys in sheet form, the Ni-base material HA 230 and the Co-base material Ha 88, have been exposed to molten LiF-22CaF2, its vapor, and vacuum, at 1093 K, for 400 and 2500 hr. Triplicate tensile testing of specimens subjected to all three environments have been undertaken between 77 to 1200 K. Comparison of the weight gain data, microstructure, and tensile properties indicate that little, if any, difference in behavior can be ascribed to the exposure environment.

Whittenberger, J. Daniel↗

In-Plane Tensile Properties, Creep Behavior and Failure Mechanisms of CVI and PIP SiC/SiC Composites at Temperatures to 1,650⁰C in Air

The in-plane tensile and creep properties of 2D woven CVI and PIP SiC/SiC composites with SylramicTM-iBN SiC fibers were measured at temperatures to 16500C in air and the data compared with the literature. Batch-to-batch variations in the tensile and creep properties, influence of thermal treatment on creep, creep parameters, damage mechanisms and failure modes for these composites were studied. Under the tested conditions, the CVI SiC/SiC composites exhibited both matrix and fiber dominated creep depending on stress, whereas the PIP SiC/SiC composites displayed only fiber dominated creep. Creep durability in both composite systems is controlled by the most creep resistant phase as well as oxidation of the fibers via cracked matrix. The Larson-Miller parameter and Monkman-Grant relationship were used wherever applicable for analyzing and predicting creep durability.

SiC-SiC Composites, CVI, PIP, Creep, In-plane tens↗

Effect of Test Specimen Shape and Size on Interlaminar Tensile Properties of Advanced Carbon-Carbon Composites

The interlaminar tensile strength of 1000-tow T-300 fiber ACC-6 carbon-carbon composites was measured using the method of bonding the coupons to adherends at room temperature. The size, 0.70 to 1.963 inches maximum width or radius, and shape, round or square, of the test coupons were varied to determine if the test method was sensitive to these variables. Sixteen total variations were investigated and the results modeled.

Vaughn, Wallace L.↗

Tensile properties of HK31XA-H24 magnesium-alloy sheet under rapid-heating conditions and constant elevated temperatures

Specimens of HK31XA-H24 magnesium-alloy sheet from an experimental batch were heated to failure at nominal temperature rates from 0.2 F to 100 F per second under constant-load conditions. Rapid-heating yield and rupture stresses are presented and compared with the yield and ultimate stresses from elevated-temperature tensile stress-strain tests for 1/2-hour exposure. Linear temperature-rate parameters were used to correlate rapid-heating results by constructing master curves which can be used for predicting yield stresses and temperatures and for estimating rupture stresses and temperatures.

MATERIALS, PROPERTIES - THERMAL↗

Tensile properties of impact ices

A special test apparatus was developed to measure the tensile strength of impact ices perpendicular to the direction of growth. The apparatus consists of a split tube carefully machined to minimize the effect of the joint on impact ice strength. The tube is supported in the wind tunnel by two carefully aligned bearings. During accretion the tube is turned slowly in the icing cloud to form a uniform coating of ice on the split tube specimen. The two halves of the split tube are secured firmly by a longitudinal bolt to prevent relative motion between the two halves during ice accretion and handling. Tensile test strength results for a variety of icing conditions were obtained. Both glaze and rime ice conditions were investigated. In general, the tensile strength of impact ice was significantly less than refrigerator ice. Based on the limited data taken, the median strength of rime ice was less than glaze ice. However, the mean values were similar.

Chu, M. L.↗