Search NASA⌕ Search

SEARCH · Search NASA

Results for “Tetroxide”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 91 records · Page 5

Propellant saturation test, 2 February - 3 May 1966

The objective of this test program was to determine the behavior of gas-saturated water and nitrogen tetroxide under various flow and pressure drop conditions. A second part of the test program is to be conducted at a later time to determine the rate of gas diffusion into propellants. The test program was conducted by the Fluid Systems Test Section of the Thermochemical Test Branch for the Auxiliary Propulsion and Pyrotechnics Branch, Propulsion and Power Division. Testing was accomplished at the Fluid Systems Test Facility during the period from February 2, 1966, to May 3, 1966.

Nitrogen compound↗

Synchrotron‐source micro‐x‐ray computed tomography for examining butterfly eyes

Comparative anatomy is an important tool for investigating evolutionary relationships among species, but the lack of scalable imaging tools and stains for rapidly mapping the microscale anatomies of related species poses a major impediment to using comparative anatomy approaches for identifying evolutionary adaptations. We describe a method using synchrotron source micro-x-ray computed tomography (syn-μXCT) combined with machine learning algorithms for high-throughput imaging of Lepidoptera (i.e., butterfly and moth) eyes. Our pipeline allows for imaging at rates of ~15 min/mm 3 at 600 nm 3 resolution. Image contrast is generated using standard electron microscopy labeling approaches (e.g., osmium tetroxide) that unbiasedly labels all cellular membranes in a species-independent manner thus removing any barrier to imaging any species of interest. To demonstrate the power of the method, we analyzed the 3D morphologies of butterfly crystalline cones, a part of the visual system associated with acuity and sensitivity and found significant variation within six butterfly individuals. Despite this variation, a classic measure of optimization, the ratio of interommatidial angle to resolving power of ommatidia, largely agrees with early work on eye geometry across species. We show that this method can successfully be used to determine compound eye organization and crystalline cone morphology. Our novel pipeline provides for fast, scalable visualization and analysis of eye anatomies that can be applied to any arthropod species, enabling new questions about evolutionary adaptations of compound eyes and beyond.

59 BASIC BIOLOGICAL SCIENCES↗

Insights into Chemical Prelithiation of SiO x /Graphite Composite Anodes through Scanning Electron Microscope Imaging

Initial Coulombic efficiency (ICE) is critical for determining the energy density of lithium-ion batteries (LIBs) used for practical applications; however, it is typically disregarded in anode research. We used SiO x and graphite composite anodes for commercial lithium-ion batteries in our preliminary research to achieve a balance between ICE, capacity, and cycling life. ICE reached 88%; however, it needs further improvement for commercial applications. Prelithiation is a process that involves the introduction of extra lithium ions into LIBs during their manufacturing to enhance the overall performance of the LIBs. We applied a chemical prelithiation method on our SiO x /graphite composite anodes, which comprised 95 wt % of the active material mass loading on the electrode. The ICE increased from 88% to 98% using an aryllithium reagent impregnation method within 2 min of prelithiation. The anode’s specific capacity density, rate, and cycle performance also significantly improved. Scanning electron microscopy (SEM) imaging enhanced by an osmium tetroxide staining method indicated that the P-anode contained a stable solid electrolyte interface (SEI) layer after the prelithiation process and cycling electrochemical test. The P-anode’s stable charge differential peak over 500 cycles also showcases a robust artificial SEI layer that was generated by the prelithiation procedure. Here, this prelithiation process has significant potential for adoption in the LIB industry’s current electrode manufacturing process.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DEVELOPMENT OF A LIGHT-WEIGHT REGENERATIVELY COOLED THRUST CHAMBER WITH BRAZED RIBS AND BRAZED OUTER WIRE TRAP

Design and fabrication procedures are discussed of a brazed-ribtype thrust chamber fabricated from stainless steel or inconel for a Sooo-lb thrust 20: 1 expansion-area-ratio regeneratively cooled liquidpropellant rocket engine which is designated as the JPL 6K Engine and operates at a chamber pressure of 150 psia. Hydrazine is used as the fuel and regenerative coolant and nitrogen tetroxide as the oxidizer. The nozzle-throat diameter is 5.42 in. The thrust chamber consists of a sheet-metal gas-side liner with longitudinal ribs spotwelded and brazed to the outer surface. Wire is wrapped over the ribs circumferentially, spot-welded to the ribs, and brazed. The liner, ribs, and wire form the coolant-passage walls. There are three basic advantages to this type of thrust chamber: light weight, ease of fabrication, and comparatively low cost. The total dry weight of a thrust chamber of this type and size made of 347 stainless steel is 46.2 lb, and the wet weight is 56.3 Ib. A total of 87 static engine tests were made on 19 of 23 thrust chambers fabricated by this technique. Four of the chambers tested had an expansion-area ratio of 20:1, and 15, which were shorter but had the same throat diameter, had an expansion-area ratio of 3.5:l. Accumulated test time was 1926 sec, including 558 sec regenerative cooling with hydrazine and 1368 sec cooling with water. One 20:l thrust chamber was subjected to 16 separate engine tests, with an accumulated test time of 399 sec, and was still in very good operating condition after the tests were completed. With water flowing through the coolant passages at 10 lb/sec, the measured nominal pressure drop between coolant manifolds of a 20:l thrust chamber wrapped with flat wire was 17.2 psi.

Thrust Chamber↗

Glass bead shot peening retards stress corrosion failure of titanium tanks

Rigidly controlled shot peening retards the incompatibility between titanium alloys and nitrogen tetroxide in rocket-propellant storage tanks. This sets up a residual compressive stress in the surface of a material which reduces tensile stresses in the material fibers, alleviating stress corrosion.

Bales, T. T.↗