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NASA NTRS2024

The Peregrine Ion Trap Mass Spectrometer (PITMS) Investigation Development and Pre-Flight Planning

The Peregrine Ion Trap Mass Spectrometer (PITMS) is a mass spectrometer instrument that operated during the Astrobotic Peregrine Mission-1 as part of the NASA Commercial Lunar Payload Services (CLPS) initiative. This paper describes the instrument and investigation design, development, and planning conducted by the PITMS team consisting of a successful partnership between NASA Goddard Space Flight Center (GSFC), The Open University (OU), NASA, and ESA. PITMS was designed to measure the abundance and temporal variability of volatile species in the near-surface lunar exosphere from a landed platform on the lunar surface. The PITMS instrument consisted of an ESA-provided Exospheric Mass Spectrometer (EMS; including sensor, electronics, controller, power supply boards) and a GSFC wrapper that provided structural elements, thermal control, and a deployable dust cover. PITMS was designed to operate as a passive sampler, where ambient gases would enter PITMS through an aperture, diffuse around the mass analyzer cavity, become ionized by electron impact and trapped in a radiofrequency field, then sequentially released to a detector to build a mass spectrum. PITMS was capable of measuring species with a massto-charge ratio (m/z) from 10 to 150 Da, with a mass resolution of approximately 0.5 amu. The PITMS science investigation was planned to be operated by GSFC with an international team of scientists. Though the mission did not achieve its lunar landing, information about the PITMS instrument and planning is provided to be able to understand and effectively use data that will be forthcoming from the investigation.

Barbara Cohen↗
NASA NTRS2009

Low-Pressure, Field-Ionizing Mass Spectrometer

A small mass spectrometer utilizing a miniature field ionization source is now undergoing development. It is designed for use in a variety of applications in which there are requirements for a lightweight, low-power-consumption instrument that can analyze the masses of a wide variety of molecules and ions. The device can operate without need for a high-vacuum, carrier-gas feed radioactive ionizing source, or thermal ionizer. This mass spectrometer can operate either in the natural vacuum of outer space or on Earth at any ambient pressure below 50 torr (below about 6.7 kPa) - a partial vacuum that can easily be reached by use of a small sampling pump. This mass spectrometer also has a large dynamic range - from singly charged small gas ions to deoxyribonucleic acid (DNA) fragments larger than 104 atomic mass units - with sensitivity adequate for detecting some molecules and ions at relative abundances of less than one part per billion. This instrument (see figure) includes a field ionizer integrated with a rotating-field mass spectrometer (RFMS). The field ionizer effects ionization of a type characterized as "soft" in the art because it does not fragment molecules or initiate avalanche arcing. What makes the "soft" ionization mode possible is that the distance between the ionizing electrodes is less than mean free path for ions at the maximum anticipated operating pressure, so that the ionizer always operates on the non-breakdown side of the applicable Paschen curve (a standard plot of breakdown potential on the ordinate and pressure electrode separation on the abscissa). The field ionizer in this instrument is fabricated by micromachining a submicron-thick membrane out of an electrically nonconductive substrate, coating the membrane on both sides to form electrodes, then micromachining small holes through the electrodes and membrane. Because of the submicron electrode separation, even a potential of only 1 V applied between the electrodes gives rise to an electric field with a strength of in excess of a megavolt per meter strong enough to ionize any gas molecules passing through the holes. An accelerator grid and an electrostatic deflector focus the ions from the field ionizer into the rotating-field cell of the RFMS. The potentials applied to the electrodes of the cell to generate the rotating electric field typically range from 1 to 13 V. The ions travel in well-defined helices within this cell, after which they are collected in a Faraday cup. The mass of most of the molecules reaching the Faraday cup decreases with increasing frequency of rotation of the electric field in the cell. Therefore, the frequency of rotation of the electric field is made to vary in order to scan through a desired range of ion masses: For example, lightweight gas molecules are scanned at frequencies in the megahertz range, while DNA and other large organic molecules are scanned at kilohertz frequencies.

Hartley, Frank↗
NASA NTRS1993

The Beta Pictoris circumstellar disk. XV - Highly ionized species near Beta Pictoris

Temporal variations of the Fe II, Mg II, and Al III circumstellar lines towards Beta Pictoris have been detected and monitored since 1985. However, the unusual presence of Al III ions is still puzzling, since the UV stellar flux from an A5V star such as Beta Pic is insufficient to produce such an ion. In order to better define the origin of such a phenomenon, new observations have been carried out to detect faint signatures of other highly ionized species in the short UV wavelength range, where the stellar continuum flux is low. These observations reveal variations not only near the C IV doublet lines, but also in C I and Al II lines, two weakly ionized species, not clearly detectable until now. In the framework of an infalling body scenario, highly ionized species would be created in the tail, far from the comet head, by collisions with ambient gas surrounding the star, or a weak stellar wind. Spectral changes have also been detected near a CO molecular band location, which, if confirmed, would provide the first molecular signature around Beta Pictoris.

Deleuil, M.↗
NASA NTRS1996

Three-Dimensional Electromagnetic Monte Carlo Particle-in-Cell Simulations of Critical Ionization Velocity Experiments in Space

Although the existence of the critical ionization velocity (CIV) is known from laboratory experiments, no agreement has been reached as to whether CIV exists in the natural space environment. In this paper we move towards more realistic models of CIV and present the first fully three-dimensional, electromagnetic particle-in-cell Monte-Carlo collision (PIC-MCC) simulations of typical space-based CIV experiments. In our model, the released neutral gas is taken to be a spherical cloud traveling across a magnetized ambient plasma. Simulations are performed for neutral clouds with various sizes and densities. The effects of the cloud parameters on ionization yield, wave energy growth, electron heating, momentum coupling, and the three-dimensional structure of the newly ionized plasma are discussed. The simulations suggest that the quantitative characteristics of momentum transfers among the ion beam, neutral cloud, and plasma waves is the key indicator of whether CIV can occur in space. The missing factors in space-based CIV experiments may be the conditions necessary for a continuous enhancement of the beam ion momentum. For a typical shaped charge release experiment, favorable CIV conditions may exist only in a very narrow, intermediate spatial region some distance from the release point due to the effects of the cloud density and size. When CIV does occur, the newly ionized plasma from the cloud forms a very complex structure due to the combined forces from the geomagnetic field, the motion induced emf, and the polarization. Hence the detection of CIV also critically depends on the sensor location.

Wang, J.↗
NASA NTRS1960

Ionospheric Measurements Using Environmental Sampling Techniques

Two rockets were flown to peak altitudes of 220 km in September 1959 to test various methods planned for future measurements of ionization parameters in the ionosphere, exosphere, and interplanetary plasma. The experiments used techniques which sample the ambient environment in the immediate vicinity of the research vehicle. Direct methods were chosen since indirect propagation techniques do not provide the temperatures of charged particles, are insensitive to ion densities, and cannot measure local electron densities under all conditions. Very encouraging results have been obtained from a preliminary analysis of data provided by one of the two flights. A new rf probe technique was successfully used to determine the electron density profile. This was indicated by its agreement with the results of a companion cw propagation experiment, particularly when the probe data were corrected for the effects of the ion sheath which surrounds the vehicle. The characteristics of this sheath were determined directly in flight by an electric field meter which provided the sheath field, and by a Langmuir probe which measured the total potential across the sheath. The electron temperatures deduced from the Langmuir probe data are greater than the neutral gas temperatures previously measured for the same location and season, but these measurements possibly were taken under different atmospheric conditions. Ion densities were calculated from the ion trap data for several altitudes ranging from 130 to 210 km and were found to be within 20 percent of the measured electron densities.

Bourdeau, R. E.↗
NASA NTRS1981

Extended adiabatic blast waves and a model of the soft X-ray background

An analytical approximation is generated which follows the development of an adiabatic spherical blast wave in a homogeneous ambient medium of finite pressure. An analytical approximation is also presented for the electron temperature distribution resulting from coulomb collisional heating. The dynamical, thermal, ionization, and spectral structures are calculated for blast waves of energy E sub 0 = 5 x 10 to the 50th power ergs in a hot low-density interstellar environment. A formula is presented for estimating the luminosity evolution of such explosions. The B and C bands of the soft X-ray background, it is shown, are reproduced by such a model explosion if the ambient density is about .000004 cm, the blast radius is roughly 100 pc, and the solar system is located inside the shocked region. Evolution in a pre-existing cavity with a strong density gradient may, it is suggested, remove both the M band and OVI discrepancies.

Cox, D. P.↗
NASA NTRS1991

Supernova remnants in dense clouds. I - Blast-wave dynamics and X-ray irradiation

Simplified models of cooling SNRs in uniform media together with an idealized emission spectrum are used to investigate the X-ray irradiation of the surrounding gas. The radiative transfer of the emitted X-rays through both the dense cooling shell and the unshocked cloud is calculated, with a simplified treatment to allow for an ionized zone surrounding the SNR. Numerical results are presented for SN energy of 10 exp 51 ergs and ambient densities ranging from 100 to 1,000,000 cu cm. It is found that an appreciable fraction of the X-ray energy is absorbed in regions where the X-ray energy deposited per H nucleon is between 1 and 30 eV; if the gas is initially molecular, the X-ray irradiation will result in warm molecular gas in which endothermic chemical reactions may proceed, and from which there may be strong emission in rotation-vibration transitions of H2 and other molecular species.

Draine, B. T.↗
NASA NTRS1977

A rocket-borne airglow photometer

The design of a rocket-borne photometer to measure the airglow emission of ionized molecular nitrogen in the 391.4 nm band is presented. This airglow is a well known and often observed phenomenon of auroras, where the principal source of ionization is energetic electrons. It is believed that at some midlatitude locations energetic electrons are also a source of nighttime ionization in the E region of the ionosphere. If this is so, then significant levels of 391.4 nm airglow should be present. The intensity of this airglow will be measured in a rocket payload which also contains instrumentation to measured in a rocket payload which also contains instrumentation to measure energetic electron differential flux and the ambient electron density. An intercomparison of the 3 experiments in a nightime launch will allow a test of the importance of energetic electrons as a nighttime source of ionization in the upper E region.

Paarmann, L. D.↗
NASA NTRS1985

Study of photon emission by electron capture during solar nuclei acceleration, 1: Temperature-dependent cross section for charge changing processes

The study of charge changing cross sections of fast ions colliding with matter provides the fundamental basis for the analysis of the charge states produced in such interactions. Given the high degree of complexity of the phenomena, there is no theoretical treatment able to give a comprehensive description. In fact, the involved processes are very dependent on the basic parameters of the projectile, such as velocity charge state, and atomic number, and on the target parameters, the physical state (molecular, atomic or ionized matter) and density. The target velocity, may have also incidence on the process, through the temperature of the traversed medium. In addition, multiple electron transfer in single collisions intrincates more the phenomena. Though, in simplified cases, such as protons moving through atomic hydrogen, considerable agreement has been obtained between theory and experiments However, in general the available theoretical approaches have only limited validity in restricted regions of the basic parameters. Since most measurements of charge changing cross sections are performed in atomic matter at ambient temperature, models are commonly based on the assumption of targets at rest, however at Astrophysical scales, temperature displays a wide range in atomic and ionized matter. Therefore, due to the lack of experimental data , an attempt is made here to quantify temperature dependent cross sections on basis to somewhat arbitrary, but physically reasonable assumptions.

Perez-Peraza, J.↗
NASA NTRS1971

Cosmic ray effects in the Gum Nebula

Ionization of Gum nebula by energetic charged particles from supernova Vela X with estimate of gamma ray line emission from ambient gas, energetic nuclei interaction

Boldt, E. A.↗
NASA NTRS1985

A field gas chromatograph using technology developed for solar system exploration

Trace gas analysis is an integral part of biospheric studies. Analytical instruments, primarily gas chromatographs (GC), are capable of measuring gases and volatiles to the ppb-level in real time. Trace gases significant in the study of biocycles include nitrous oxide, hydrogen sulfide, other nitrogen and sulfur species, as well as methane and ethylene. The concept of a field gas chromatograph is derived from technology being pursued in the design of ultra-compact instruments for solar system exploration. The instrument breadboard incorporates the specialized porous column packings and the highly sensitive metastable ionization detector developed by the Solar System Exploration Office. These parts ensure a broad capability for which the analysis of ambient N2O is one example. A commercial, portable gas chromatograph is currently being extensively modified to incorporate analytical concepts and components derived from flight GC technology. Data storage devices suitable for field use are presently being studied.

Woeller, F. H.↗
NASA NTRS1991

Model of electron collecting plasma contactors

In laboratory experiments, plasma contactors are observed to collect ampere-level electron currents with low impedance. In order to extend the laboratory experience to the low-earth-orbit environment, a model of plasma contactors is being developed. Laboratory results are being used to support and validate the model development. The important physical processes observed in the laboratory are that the source plasma is separated from the background plasma by a double layer and that ionization of the expellant gas by the collected electrons creates the bulk of the ions that leave the source plasma. The model, which uses Poisson's equation with a physical charge density that includes the ion and electron components of both the source and the ambient plasmas, reproduces this phenomenon for typical experimental parameters. The calculations, in agreement with the laboratory results, show little convergence of the accelerated electrons. The angular momentum of the incoming electrons dramatically reduces the peak electron density. These electrons ionize enough gas to generate the source plasma. Calculations show that the increase in ionization rate with potential produces a steep rise in collected current with increasing potential as seen in the laboratory.

Davis, V. A.↗
NASA NTRS1995

Coronal abundances determined from energetic particles

Solar energetic particles (SEPs) provide a measurement of coronal element abundances that is highly independent of the ionization states and temperature of the ions in the source plasma. The most complete measurements come from large 'gradual' events where ambient coronal plasma is swept up by the expanding shock wave from a coronal mass ejection. Particles from 'impulsive' flares have a pattern of acceleration-induced enhancements superimposed on the coronal abundances. Particles accelerated from high-speed solar wind streams at corotating shocks show a different abundance pattern corresponding to material from coronal holes. Large variations in He/O in coronal material are seen for both gradual and impulsive-flare events but other abundance ratios, such as Mg/Ne, are remarkably constant. SEP measurements now include hundreds of events spanning 15 years of high-quality measurement.

Reames, D. V.↗
NASA NTRS1978

Electron beam injection experiments - The beam-plasma discharge at low pressures and magnetic field strengths

The paper describes electron beam injection experiments which clarify observational results obtained in rocket flights. A column of enhanced density plasma, exceeding the density expected from ionization by primary beam electrons, was observed in a large vacuum system at low magnetic fields (1 to 1.5 G) and low ambient pressures (10 to the minus 6 to 10 to the minus 5 torr). The peak luminosity of the discharge was about 10 times that of the beam alone, and the radius increased by a factor of three. In the absence of the discharge, RF emission is observed at 1.1 to 1.2 times the cyclotron frequency, and a strong band of RF noise with upper frequency cutoff at about the cyclotron frequency is observed in the discharge mode, along with higher frequency noise at or near the plasma frequency. The onset of the plasma discharge is critically dependent on beam current. The described results agree with observations obtained at much higher densities and magnetic fields in fusion research studies.

Bernstein, W.↗
NASA NTRS1987

Magnetic field and remanent magnetization effects of basin-forming impacts on the moon

Maps of the distribution of lunar surface magnetic fields produced by the electron reflection method have shown that the largest observed concentrations of lunar crustal magnetization occur antipodal (diametrically opposite) to four relatively young large impact basins: Imbrium, Orientale, Serenitatis, and Crisium. A model is proposed here for the formation of these magnetization concentrations (or 'magcons') in which the partially ionized vapor cloud produced in a hypervelocity (greater than 10 km/s) basin-forming impact expands around the moon forcing a preexisting ambient magnetic field to be concentrated for a brief (less than 1 day) time period in the antipodal zone. Acquisition of magnetic remanence during the period of compressed field amplification may occur by one of several mechanisms, such as shock remanence by impact of solid secondaries ejected from the basin-forming event. The model implies that basin-forming impacts have played a major role in determining the large-scale distribution of crustal magnetization detectable from lunar orbit.

Hood, L. L.↗
NASA NTRS1992

Coordinated Radio, Electron, and Waves Experiment (CREWE) for the NASA Comet Rendezvous and Asteroid Flyby (CRAF) instrument

The Coordinated Radio, Electron, and Waves Experiment (CREWE) was designed to determine density, bulk velocity and temperature of the electrons for the NASA Comet Rendezvous and Asteroid Flyby Spacecraft, to define the MHD-SW IMF flow configuration; to clarify the role of impact ionization processes, to comment on the importance of anomalous ionization phenomena (via wave particle processes), to quantify the importance of wave turbulence in the cometary interaction, to establish the importance of photoionization via the presence of characteristic lines in a structured energy spectrum, to infer the presence and grain size of significant ambient dust column density, to search for the theoretically suggested 'impenetrable' contact surface, and to quantify the flow of heat (in the likelihood that no surface exists) that will penetrate very deep into the atmosphere supplying a good deal of heat via impact and charge exchange ionization. This final report provides an instrument description, instrument test plans, list of deliverables/schedule, flight and support equipment and software schedule, CREWE accommodation issues, resource requirements, status of major contracts, an explanation of the non-NASA funded efforts, status of EIP and IM plan, descope options, and Brinton questions.

Scudder, Jack D.↗
NASA NTRS1999

Ionized Outflows in 3-D Insights from Herbig-Haro Objects and Applications to Nearby AGN

HST shows that the gas distributions of these objects are complex and clump at the limit of resolution. HST spectra have lumpy emission-line profiles, indicating unresolved sub-structure. The advantages of 3D over slits on gas so distributed are: robust flux estimates of various dynamical systems projected along lines of sight, sensitivity to fainter spectral lines that are physical diagnostics (reddening-gas density, T, excitation mechanisms, abundances), and improved prospects for recovery of unobserved dimensions of phase-space. These advantages al- low more confident modeling for more profound inquiry into underlying dynamics. The main complication is the effort required to link multi- frequency datasets that optimally track the energy flow through various phases of the ISM. This tedium has limited the number of objects that have been thoroughly analyzed to the a priori most spectacular systems. For HHO'S, proper-motions constrain the ambient B-field, shock velocity, gas abundances, mass-loss rates, source duty-cycle, and tie-ins with molecular flows. If the shock speed, hence ionization fraction, is indeed small then the ionized gas is a significant part of the flow energetics. For AGN'S, nuclear beaming is a source of ionization ambiguity. Establishing the energetics of the outflow is critical to determining how the accretion disk loses its energy. CXO will provide new constraints (especially spectral) on AGN outflows, and STIS UV-spectroscopy is also constraining cloud properties (although limited by extinction). HHO's show some of the things that we will find around AGN'S. I illustrate these points with results from ground-based and HST programs being pursued with collaborators.

Cecil, Gerald↗
NASA NTRS2015

Ice Chemistry in Interstellar Dense Molecular Clouds, Protostellar Disks, and Comets

Despite the low temperatures (T less than 20K), low pressures, and low molecular densities found in much of the cosmos, considerable chemistry is expected to occur in many astronomical environments. Much of this chemistry happens in icy grain mantles on dust grains and is driven by ionizing radiation. This ionizing radiation breaks chemical bonds of molecules in the ices and creates a host of ions and radicals that can react at the ambient temperature or when the parent ice is subsequently warmed. Experiments that similar these conditions have demonstrated a rich chemistry associated with these environments that leads to a wide variety of organic products. Many of these products are of considerable interest to astrobiology. For example, the irradiation of simple ices has been shown to abiotically produce amino acids, nucleobases, quinones, and amphiphiles, all compounds that play key roles in modern biochemistry. This suggests extraterrestrial chemistry could have played a role in the origin of life on Earth and, by extension, do so on planets in other stellar systems.

Ice Irradiation↗