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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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DOE OSTI2018

Effect of the Plasma Functionalization of Carbon Nanotubes on the Formation of a Carbon Nanotube–Nickel Oxide Composite Electrode Material

The unique properties of carbon nanotubes (CNTs) make these systems promising for the production of composite electrode materials based on a combination of CNTs and transition metal oxides. The effect the parameters of the functionalization of vertically aligned CNT arrays in mixed argon–oxygen high-frequency plasma have on the structural characteristics of CNTs is studied by Raman spectroscopy. The effect the duration of treatment at higher partial argon consumption and low total gas consumption of the working mixture has on the distribution of nickel oxide over a CNT array deposited via SILAR is determined. Results from scanning electron microscopy show that lengthening the duration of functionalization from 30 to 1200 s allows the depth of coating a CNT surface with a nickel oxide layer to be increased from 300 nm to 2.5 μm. Composite structures produced in this work can be used as electrodes of supercapacitors.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

NASA NTRS1986

Solid state imagers and their applications; Proceedings of the Meeting, Cannes, France, November 26, 27, 1985

Topics treated include the use of semiconductor imagers in high energy particle physics, an X-ray image sensor based on an optical TDI-CCD imager, and an electron-sensitive CCD readout array for a circular-scan streak tube. Papers are presented on the pan-imager, high resolution linear arrays, the reduction of reflection losses in solid-state image sensors, a high resolution CCD imager module with swing operation, large area CCD image sensors for scientific applications, and new readout techniques for frame transfer CCDs. Consideration is given to advanced optoelectronical sensors for autonomous rendezvous/docking and proximity operations in space, the testing and characterization of CCDs for the Rosat star sensors, an advanced radial camera for the Hubble Space Telescope, and scanning or staring infrared imagers.

Declerck, Gilbert J.↗

NASA NTRS1992

Proton aurora and substorm intensifications

Ground based measurements from the CANOPUS array of meridian scanning photometers and precipitating ion and electron data from the DMSP F9 satellite show that the electron arc which brightens to initiate substorms intensifications is formed within a region of intense proton precipitation that is well equatorward (about 4-6 deg) of the nightside open-closed field line boundary. The precipitating protons are from a population that is energized via Earthward convection from the magnetotail into the dipolar region of the magnetosphere and may play an important role in the formation of the electron arcs leading to substorm intensifications on dipolelike field lines.

Samson, J. C.↗

NASA NTRS1993

Proton aurora and substorm intensifications

Ground based measurements from the CANOPUS array of meridian scanning photometers and precipitating ion and electron data from the DMSP F9 satellite show that the electron arc which brightens to initiate substorm intensifications is formed within a region of intense proton precipitation that is well equatorward (approximately four to six degrees) of the nightside open-closed field line boundary. The precipitating protons are from a population that is energized via earthward convection from the magnetotail into the dipolar region of the magnetosphere and may play an important role in the formation of the electron arcs leading to substorm intensifications on dipole-like field lines.

Samson, J. C.↗

NASA NTRS1979

Remote sensing using solid-state array technology

The paper describes the design features and capabilities of a remote sensor that uses solid-state linear arrays and operates in a 'pushbroom' scan mode to provide the required performance. Pushbroom scanning is a term describing the technique of using the forward motion of a satellite platform to sweep a linear array of detectors oriented perpendicular to the ground track across a scene being imaged. One array is typically used for each spectral channel. Satellite motion provides one direction of scan and electronic sampling of the detectors in the crosstrack dimension provides the orthogonal scan component to form an image. The detector array is sampled at the appropriate rate so that contiguous lines are produced. The performance of a pushbroom system is discussed relative to radiometric sensitivity, detector array geometric fidelity, and radiometric correction. System advantages are precision geometric positioning of the detectors, very high sensitivity and favorable SNR, low power consumption, and no moving optics.

Thompson, L. L.↗

NASA NTRS2010

Phased Array Radiometer Calibration Using a Radiated Noise Source

Electronic beam steering capability of phased array antenna systems offer significant advantages when used in real aperture imaging radiometers. The sensitivity of such systems is limited by the ability to accurately calibrate variations in the antenna circuit characteristics. Passive antenna systems, which require mechanical rotation to scan the beam, have stable characteristics and the noise figure of the antenna can be characterized with knowledge of its physical temperature [1],[2]. Phased array antenna systems provide the ability to electronically steer the beam in any desired direction. Such antennas make use of active components (amplifiers, phase shifters) to provide electronic scanning capability while maintaining a low antenna noise figure. The gain fluctuations in the active components can be significant, resulting in substantial calibration difficulties [3]. In this paper, we introduce two novel calibration techniques that provide an end-to-end calibration of a real-aperture, phased array radiometer system. Empirical data will be shown to illustrate the performance of both methods.

Srinivasan, Karthik↗

DOE OSTI2019

The 4D Camera: Very High Speed Electron Counting for 4D-STEM

A vast array of new experimental modalities have been enabled in the past several years through the development of pixelated detectors synchronized to probe scanning electronics. Such camera systems can then acquire the rich information present in the central portion of the convergent beam electron diffraction pattern as a function of probe position (4D-STEM). Here, we present the development, installation, and characterization of the 4D Camera, a CMOS Active Pixel Sensor that consists of a 576 x 576 array of 10 μm pixels of a design related to the original TEAM detector and an outer HAADF detector with 16 concentric quadrant diodes.

47 OTHER INSTRUMENTATION↗

DOE OSTI2021

Revealing the Chemical Bonding in Adatom Arrays via Machine Learning of Hyperspectral Scanning Tunneling Spectroscopy Data

The adatom arrays on surfaces offer an ideal playground to explore the mechanisms of chemical bonding via changes in the local electronic tunneling spectra. While this information is readily available in hyperspectral scanning tunneling spectroscopy data, its analysis has been considerably impeded by a lack of suitable analytical tools. Here we develop a machine learning based workflow combining supervised feature identification in the spatial domain and unsupervised clustering in the energy domain to reveal the details of structure-dependent changes of the electronic structure in adatom arrays on the Co 3 Sn 2 S 2 cleaved surface. This approach, in combination with first-principles calculations, provides insight for using artificial neural networks to detect adatoms and classifies each based on their local neighborhood comprised of other adatoms. These structurally classified adatoms are further spectrally deconvolved. The unexpected inhomogeneity of electronic structures among adatoms in similar configurations is unveiled using this method, suggesting there is not a single atomic species of adatoms, but rather multiple types of adatoms on the Co 3 Sn 2 S 2 surface. This is further supported by a slight contrast difference in the images (or slight size variation) of the topography of the adatoms.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2021

Hyperspectral X-ray Imaging: Progress Towards Chemical Analysis in the SEM

The Hyperspectral X-ray Imaging (HXI) project will enable non-destructive chemical-state determination of nano-scale samples in the electron microscope for nuclear safeguards applications. To efficiently measure chemical state through electron-excited X-ray emission requires a combination of wide spectral bandwidth, high resolution, and high count rate capability. We are building a next-generation X-ray detector based on an array of transition edge sensors (TESs) to make these measurements possible and routine in the scanning electron microscope (SEM). Leveraging the large pixel densities afforded by microwave multiplexing readout and continuous, uninterrupted operation of a cryogen-free dilution refrigerator, this instrument will have efficiency to allow chemical species identification of nano-scale samples in hours instead of days to weeks. We describe prototype pixel designs for this HXI instrument, comprising three pixel types that will make up the hybrid TES array. Engineering design of the integrated HXI cryostat and SEM system is in progress, with full detector commissioning expected in Spring 2021 followed closely by full-scale integration with the SEM. Furthermore, we also report on the commissioning of a complementary TES-based X-ray emission spectroscopy platform for bulk samples to build a spectral library for HXI sample identification.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2020

Domain-Matching Epitaxy of Ferroelectric Hf 0.5 Zr 0.5 O 2 (111) on La 2/3 Sr 1/3 MnO 3 (001)

Epitaxial ferroelectric HfO2 films are the most suitable to investigate intrinsic properties of the material and for prototyping emerging devices. Ferroelectric Hf 0.5 Zr 0.5 O 2 (111) films were epitaxially stabilized on La 2/3 Sr 1/3 MnO 3 (001) electrodes. This epitaxy, considering the symmetry dissimilarity and the huge lattice mismatch, is not compatible with conventional mechanisms of epitaxy. In this work, to gain insight into the epitaxy mechanism, scanning transmission electron microscopy characterization of the interface was performed, revealing arrays of dislocations with short periodicities. Additionally, these observed periodicities agree with those expected for domain matching epitaxy, indicating that this unconventional mechanism could be the prevailing factor in the stabilization of ferroelectric Hf0.5Zr0.5O2 with (111) orientation in the epitaxial Hf 0.5 Zr 0.5 O 2 (111)/La 2/3 Sr 1/3 MnO 3 (001)heterostructure.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Novel Applications of Scanning Ultrafast Electron Microscopy (SUEM)

The Scanning Ultrafast Electron Microscope (SUEM) was used to image a wide array samples using a variety of standard and non-standard operating conditions on a custom system built in Org. 8942. The ability of this technique to produce high-quality images was assessed during this one year LDRD. To obtain details about the devices imaged, as well as the experimental details, please refer to the classified report from the project manager, Rich Dondero, or the NSP IA lead, Kristina Czuchlewski.

47 OTHER INSTRUMENTATION↗

NASA NTRS2014

Phased Array-Fed Reflector (PAFR) Antenna Architectures for Space-Based Sensors

Communication link and target ranges for satellite communications (SATCOM) and space-based sensors (e.g. radars) vary from approximately 1000 km (for LEO satellites) to 35,800 km (for GEO satellites). At these long ranges, large antenna gains are required and legacy payloads have usually employed large reflectors with single beams that are either fixed or mechanically steered. For many applications, there are inherent limitations that are associated with the use of these legacy antennas/payloads. Hybrid antenna designs using Phased Array Fed Reflectors (PAFRs) provide a compromise between reflectors and Direct Radiating phased Arrays (DRAs). PAFRs provide many of the performance benefits of DRAs while utilizing much smaller, lower cost (feed) arrays. The primary limitation associated with hybrid PAFR architectures is electronic scan range; approximately +/-5 to +/- 10 degrees is typical, but this range depends on many factors. For LEO applications, the earth FOV is approximately +/-55 degrees which is well beyond the range of electronic scanning for PAFRs. However, for some LEO missions, limited scanning is sufficient or the CONOPS and space vehicle designs can be developed to incorporate a combination mechanical slewing and electronic scanning. In this paper, we review, compare and contrast various PAFR architectures with a focus on their general applicability to space missions. We compare the RF performance of various PAFR architectures and describe key hardware design and implementation trades. Space-based PAFR designs are highly multi-disciplinary and we briefly address key hardware engineering design areas. Finally, we briefly describe two PAFR antenna architectures that have been developed at Northrop Grumman.

antenna↗

NASA NTRS2021

A 1-D Submm-wave Leaky-Wave Phased Array using MEMS Phase Shifters

Beam-scanning of submillimeter-wave spectrometers and radiometers have traditionally been implemented using mechanical scanning mechanisms due to the absence of lowloss electronic phase shifters. Recently developed waveguideintegrated MEMS phase shifters are paving the way to realize electronic beam-steering using submm-wave phased arrays. In this work, two phased array demonstrators are presented that operate from 500GHz to 600GHz. A 20 dB directivity 8 ? 1 leaky-wave antenna array will be demonstrated, using fixed waveguide feeding networks, to be capable of ?20? scanning with a scan loss less than 1:7 dB. Secondly, an equivalent but smaller 17 dB directivity 4 ? 1 array will be integrated with MEMS phase shifters to demonstrate a dynamic scanning capability over a ?9:5? range. The antenna array is based on closely sampled square waveguides, terminated with a double-iris, in close proximity of a low permittivity superstrate in order to reduce the grating lobes at larger scanning angles. Measurements are expected to be presented at the conference.

Chattopadhyay, Goutam↗

NASA NTRS2003

Phased Array Antenna Testbed Development at the NASA Glenn Research Center

Ideal phased array antennas offer advantages for communication systems, such as wide-angle scanning and multibeam operation, which can be utilized in certain NASA applications. However, physically realizable, electronically steered, phased array antennas introduce additional system performance parameters, which must be included in the evaluation of the system. The NASA Glenn Research Center (GRC) is currently conducting research to identify these parameters and to develop the tools necessary to measure them. One of these tools is a testbed where phased array antennas may be operated in an environment that simulates their use. This paper describes the development of the testbed and its use in characterizing a particular K-Band, phased array antenna.

Lambert, Kevin M.↗

NASA NTRS2021

Demonstration of a 1-D Submillimeter-Wave Phased Array with MEMS Phase Shifters

At submillimeter-wave frequencies, due to the nonavailability of low-loss phase shifters, electronic antenna beam scanning is difficult to realize. Traditionally, power-hungry and bulky motors are used to mechanically scan the antenna beam. At lower-frequencies, phased array antennas are most commonly used where low-loss phase shifters are used with the array elements to accomplish beam steering. However, development of similar phased array antennas at submillimeter-waves has been challenging. Recently, we have developed a low-loss microelectromechanical systems (MEMS) based phased shifter in the 500-750 GHz band. In this work, we present a submillimeter-wave phased array antenna system with a cavity-backed double slot antenna architecture using the MEMS-based phase shifters. To demonstrate the concept, we developed two arrays: first one is a 8×1 linear antenna array with a fixed waveguide feeding network that achieved ±20◦ beam scanning, 18 dB directivity, and less than 1 dB scan loss over the design frequency of 500–570 GHz. The second one is a 4 × 1 linear antenna array with integrated MEMS-based phase shifters on each array element, achieving 15 dB directivity and capable of dynamic beam scanning over a range of ±9 ◦ . All the plots presented are simulated results since the parts are currently being fabricated. We hope to have access to our assembly and measurement facilities over the next few months and present measured performances at the conference.

Chattopadhyay, G.↗

NASA NTRS1982

A photon-counting photodiode array detector for far ultraviolet (FUV) astronomy

A compact, stable, single-stage intensified photodiode array detector designed for photon-counting, far ultraviolet astronomy applications employs a saturable, 'C'-type MCP (Galileo S. MCP 25-25) to produce high gain pulses with a narrowly peaked pulse height distribution. The P-20 output phosphor exhibits a very short decay time, due to the high current density of the electron pulses. This intensifier is being coupled to a self-scanning linear photodiode array which has a fiber optic input window which allows direct, rigid mechanical coupling with minimal light loss. The array was scanned at a 250 KHz pixel rate. The detector exhibits more than adequate signal-to-noise ratio for pulse counting and event location.

Hartig, G. F.↗

NASA NTRS1982

Photon counting photodiode array detector for far ultraviolet (FUV) astronomy

Hartig, G. F.↗

NASA NTRS1982

Highly versatile computer-controlled television detector system

A description is presented of a television detector system which has been designed to accommodate a wide range of applications. It is currently being developed for use in X-ray diffraction, X-ray astrophysics, and electron microscopy, but it is also well suited for astronomical observations. The image can be integrated in a large, high-speed memory system, in the memory of a computer system, or the target of the TV tube or CCD array. The detector system consists of a continuously scanned, intensified SIT vidicon with scan and processing electronics which generate a digital image that is integrated in the detector memory. Attention is given to details regarding the camera system, scan control and image processing electronics, the memory system, and aspects of detector performance.

Kalata, K.↗