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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 91 records · Page 5
All sourcesNASA NTRSDOE OSTI
NASA NTRS1980

High Temperature Resin Matrix Composites for Aerospace Structures

Accomplishments and the outlook for graphite-polyimide composite structures are briefly outlined. Laminates, skin-stiffened and honeycomb sandwich panels, chopped fiber moldings, and structural components were fabricated with Celion/LARC-160 and Celion/PMR-15 composite materials. Interlaminar shear and flexure strength data obtained on as-fabricated specimens and specimens that were exposed for 125 hours at 589 K indicate that epoxy sized and polyimide sized Celion graphite fibers exhibit essentially the same behavior in a PMR-15 matrix composite. Analyses and tests of graphite-polyimide compression and shear panels indicate that utilization in moderately loaded applications offers the potential for achieving a 30 to 50 percent reduction in structural mass compared to conventional aluminum panels. Data on effects of moisture, temperature, thermal cycling, and shuttle fluids on mechanical properties indicate that both LARC-160 and PMR-15 are suitable matrix materials for a graphite-polyimide aft body flap. No technical road blocks to building a graphite-polyimide composite aft body flap are identified.

Davis, J. G., Jr.↗
NASA NTRS1972

Comparison of NASTRAN and STARDYNE static analysis of a graphite fiber reinforced plastic truss structure

A static and buckling analysis of the ATS-F&G spacecraft reflector support truss (RST) and bridge truss assembly using NASTRAN was conducted. The RST is fabricated from a new material, graphite fiber reinforced plastic. A comparison is made with the NASTRAN results and the results of a similar analysis conducted using the stardyne program. The results of an actual static load test are also compared.

Honeycutt, G. H.↗
NASA NTRS1975

Environmental effects on the torsion and flexure fatigue properties of graphite-epoxy composites

Effects of torsional and flexural fatigue on the long-time integrity of advanced graphite-epoxy structural composites have been investigated. Reversed (R = - 1) and unidirectional (R = 0) torsional fatigue tests were made on unidirectional, cross-plied and woven graphite fiber materials in air and water at room temperature and at 74 C. Flexural fatigue tests (4-point bending) with R = - 1 were run in air and water at room temperature, and at R = 0 in air. Results show that in torsional cycling, both water environment and higher test temperature contribute to significant degradation of torsional stiffness. The degradation of stiffness from torsional stress cycling was observed to be much greater with R = - 1 than with simple R = 0 cycling. The effect of environment is also greater in the fully reversed cycling.

Sumsion, H. T.↗
NASA NTRS1984

New innovations in composites

Procedures for manufacturing metal clad graphite resin structural elements applicable to optical systems requiring precisely controlled thermal and mechanical properties are described. Analytical estimates were made of the material properties that can be obtained for various ratios of graphite epoxy and aluminum cladding. Three graphite fiber systems were evaluated. Two manufacturing processes are described. One method is a procedure for manufacturing long tubes by wrapping aluminum foil over dry graphite fiber. Resin was applied by spreading before applying the aluminum wrap. A second approach, offering the opportunity for precise tuning of the coefficient of expansion, is by die flattening metal tubing through which a measured amount of fiber has been drawn. Prior to flattening, resin is injected, and after flattening or shaping the part is cured. This latter procedure offers the opportunity to fine tune the structure to achieve a CTE with a precision equal to that of the measuring systems-by modifying the number of fiber tows prior to manufacturing or by etching the metal after manufacturing. Experimental verification and demonstration data are presented for Gr/E bars with aluminum and steel skins.

Bluck, R. M.↗
NASA NTRS1976

Environmental Effects on Graphite-Epoxy Fatigue Properties

Effects of torsional and flexural fatigue on the long-time Integrity of advanced graphite-epoxy structural composites have been investigated. Torsional fatigue tests were run at stress ratios of R = 0 (zero to maximum, repeated) and R = -1 (zero mean stress) on unidirectional, angleply, and woven graphite fiber materials in air and water at room temperature and at 74 C. Flexural fatigue tests (four-point bending) with R = -1 were run in air and water at room temperature, and with R = 0 in air. Results show that, in torsional cycling, both water environment and higher test temperature contribute to significant degradation of torsional stiffness. The degradation of stiffness from torsional stress cycling was observed to be much greater with R = -1 than with simple R = 0 cycling. The effect of environment also is greater in the fully reversed cycling. Flexural fatigue results on +/- 30 deg material show a large fatigue effect, with fatigue limits of less than 50% and 30% of the static failure strength for specimens tested under stress ratios of R = 0 and R = -1, respectively. Compliance measurements indicate that the final failures are preceded by damage initiation and accumulation, which begins at about 1% of the specimen life.

Sumsion, H. T.↗
NASA NTRS1976

Magnetic field generated resistivity maximum in graphite

In a zero magnetic field, the electrical resistivity of highly oriented pyrolytic (polycrystalline) graphite drops smoothly with decreasing temperature, becoming constant below 4 K. However, in a fixed applied magnetic field, the resistivity goes through a maximum as a function of temperature, with a larger maximum for a larger field intensity. The temperature of the maximum increases with field intensity, but saturates to a constant value near 25 K (the exact temperature depends on the sample) at high intensity. In single-crystal graphite, a maximum in resistivity as a function of temperature is also present, but has the effects of Landau level quantization superimposed. Several possible explanations for the resistivity maximum are proposed, but a complete explanation awaits detailed calculations involving the energy band structure of graphite, and the particular scattering mechanisms involved.

Woollam, J. A.↗
NASA NTRS1976

Magnetic field generated resistivity maximum in graphite

In zero magnetic field, B, the electrical resistivity, rho(O,T) of highly oriented pyrolytic (polycrystalline) graphite drops smoothly with decreasing T, becoming constant below 4 K. However, in a fixed applied magnetic field B, the resistivity rho(B,T) goes through a maximum as a function of T, with larger maximum for larger B. The temperature of the maximum increases with B, but saturates to a constant value near 25 K (exact T depends on sample) at high B. In single crystal graphite a maximum in rho(B,T) as a function of T is also present, but has the effects of Landau level quantization superimposed. Several possible explanations for the rho(B,T) maximum are proposed, but a complete explanation awaits detailed calculations involving the energy band structure of graphite, and the particular scattering mechanisms involved.

Wollam, J. A.↗
NASA NTRS1973

Production of circular polymer-glass fabric composites

Potentially automated pultrusion technique has been provided for production of curved, glass-reinforced polyimide, epoxy, and graphite reinforced structures. Specially designed apparatus has been manufactured for production of curved structures.

Hardesty, E. E.↗
NASA NTRS1978

A perspective on composites

The development of composites in the United States in the 1960s and 1970s is briefly reviewed with emphasis on aerospace applications. Consideration is given to such highlights as the manufacture of boron filaments, the use of boron-epoxy composites for aerospace structures, graphite-epoxy composites, and current graphite R & D work.

Lovelace, A. M.↗
NASA NTRS1979

SEP solar array development testing

This paper describes the test program of a lightweight 25 kW solar array for solar electric propulsion. A full-scale development wing was made of aluminum with the containment box cover of graphite-epoxy, while the flight design array wing uses a graphite-epoxy structure. The full-scale continuous longeron array extension mast was tested for performance on a water table, and the full scale wing was functionally tested to demonstrate automatic containment box unlocking, wing extension, and retraction, blanket tensioning, and automatic application of blanket preload. The wing was then tested to the Shuttle acoustic environment, followed by a thermal/vacuum test in which the wing was extended and retracted at high and low temperature. Finally, the wing was tested in vibration with sine and random vibration environments.

Elms, R. V., Jr.↗
NASA NTRS1979

Manufacturing processes for fabricating graphite/PMR 15 polyimide structural elements

Investigations were conducted to obtain commercially available graphite/PMR-15 polyimide prepreg, develop an autoclave manufacturing process, and demonstrate the process by manufacturing structural elements. Controls were established on polymer, prepreg, composite fabrication, and quality assurance, Successful material quality control and processes were demonstrated by fabricating major structural elements including flat laminates, hat sections, I beam sections, honeycomb sandwich structures, and molded graphite reinforced fittings. Successful fabrication of structural elements and simulated section of the space shuttle aft body flap shows that the graphite/PMR-15 polyimide system and the developed processes are ready for further evaluation in flight test hardware.

Sheppard, C. H.↗
NASA NTRS1979

The structural behavior of a graphite-polymide honeycomb sandwich panel with quasi-isotropic face sheets and an orthotropic core

The results of a series of tests of graphite-polyimide honeycomb sandwich panels are presented. The panels were 1.22 m long, 0.508 m wide, and approximately 13.3 m thick. The face sheets were a T-300/PMR-15 fabric in a quasi-isotropic layup and were 0.279 mm thick. The core was Hexcel HRH 327-3/16 - 4.0 glass reinforced polyimide honeycomb, 12.7 mm thick. Three panels were used in the test: one was cut into smaller pieces for testing as beam, compression, and shear specimens; a second panel was used for plate bending tests; the third panel was used for in-plane stability tests. Presented are the experimental results of four point bending tests, short block compression tests, core transverse shear modulus, three point bending tests, vibration tests, plate bending tests, and panel stability tests. The results of the first three tests are used to predict the results of some of the other tests. The predictions and experimental results are compared, and the agreement is quite good.

Hyer, M. W.↗
NASA NTRS1980

Design of a high precision microwave reflector

Development of a high accuracy spherical microwave reflector to support contour RMS and pointing requirements for a new series of space instruments is reported. The reflector system is composed of precision machined aluminum tile reflectors supported from a eutectic coated graphite epoxy structure by flexures. Several basic technologies have been integrated into a manufacturing process that accommodates fabrication techniques of both optical and composite constraints. The optical figure and its change due to thermal gradient was measured in a thermal vacuum environment with a Ronchi system. The radiometer system is in support of the Microwave Limb Sounder, an experiment to measure emissions from earth's atmospheric limb thus obtaining wind, temperature, pressure and chemical composition measurements.

Noller, E. W.↗
NASA NTRS1982

A preliminary assessment of the self-induced environment and contamination of the Space Telescope

Preliminary estimates for the internal pressures and surface contamination of the Space Telescope were made. The calculations for the transient pressures in the aft-shroud and telescope compartments considered two large communicating volumes that contain gaseous sources and sinks. The outgassing sources in the aft shroud consist of several scientific instruments, paints, insulations, and graphite-epoxy structures. With the exception of the instruments, these sources also exist in the telescope compartment. the outgassing functions were generated from ample test results at various temperatures and from internal pressure measurements in a vacuum test of one of the instruments. The venting occurs through combinations of series and parallel passages in both compartments. The calculated time constant of the two volumes and their respective passages, with the telescope protective door closed, is a few seconds, which is slightly less than that of the shuttle bay volume with the bay doors closed. With the telescope door closed, the pressures in the two compartments should decay to about 1OE-5 torr in about 200 hours. The contaminant deposits were assessed on the basis of expected partial pressures of the contaminant fraction of the outgassing. These pressures and the activation energies of the source materials were used to calculate the adsorbed and condensed deposits on the surfaces as a function of time.

Scialdone, J. J.↗
NASA NTRS1983

Development of new and improved polymer matrix resin systems, phase 1

Vinystilbazole (vinylstryrylpyridine) and vinylpolystyrulpyridine were prepared for the purpose of modifying bismaleimide composite resins. Cure studies of resins systems were investigated by differential scanning calorimetry. The vinylstyrylpyridine-modified bismaleimide composite resins were found to have lower cure and gel temperatures, and shorter cure times than the corresponding unmodified composite resins. The resin systems were reinforced with commercially avialable satin-weave carbon cloth. Prepregs were fabricated by solvent or hot melt techniques. Thermal stability, flammability, moisture absorption, and mechanical properties of the composites (such as flexural strength, modulus, tensile and short beam shear strength) were determined. Composite laminates showed substantial improvements in both processability and mechanical properties compared to he bismaleimide control systems. The vinylstyrylpyridine modified bismaleimide resins can be used as advanced matrix resins for graphite secondary structures where ease of processing, fireworthiness, and high temperature stability are required for aerospace applications.

Hsu, M. S.↗
NASA NTRS1985

Bismaleimides and related maleimido polymers as matrix resins

Significant processing and property improvements can be achieved by copolymerization of state-of-the-art bisimides with various vinyl stilbazole derivatives to give both fire resistance and high-temperature properties from hot-melt compositions. Significant improvement in mechanical properties is achieved through these modifications, which may make these new matrix resins ideal candidates for fireworthy secondary graphite composite structures. Phosphorous modifications of maleimido polymers through phosphonate structure and tricyclophosphazene derivatives provide families of new matrix resins for short-time applications in severe thermo-oxidative environments. With further research these may provide matrix resins for long-term thermo-oxidative stability of advanced composites at temperatures up to 400 to 500 C.

Parker, J. A.↗
NASA NTRS1988

Novel polyamide-imines

An account is given of tough, thermally stable linear polyimides containing amide linkages that recommend themselves for use in high temperature-resistant films and coatings as well as matrix resins for graphite-reinforced structures. Four such polymers were synthesized from unsubstituted amide diamines, and two others from N-substituted amide diamines. High inherent viscosities and glass transition temperatures were obtained. The films exhibit good resistance to organic solvents. Films of the 4,4-prime-isomer polyamide-imide yielded exceptionally high modulus and toughness during impact evaluation.

Dezern, James F.↗
NASA NTRS1988

A precision pointing system for space telescope class optical trackers

This paper reports on the results of a study effort whose main objective was to develop a conceptual design for a space based, large-payload (3000 kg) pointing system capable of both rapid slew maneuvers (0.35 rad/sec-squared) and very stable tracking (1 microrad, 1 sigma, each axis). The key features of the resulting solution are: (1) cross elevation over elevation gimbal system, (2) closed cross elevation gimbal ring, (3) graphite-epoxy structure, (4) two-motor reactionless joint torquers, (5) payload mounted vernier reaction wheel, and (6) gyrostabilized model following control system.

Sevaston, George E.↗